Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal Method
Carbon microsphere was successfully synthesized from waste office paper via hydrothermal method and high temperature treatment in nitrogen atmosphere. The process of carbon microsphere synthesis from waste office paper fiber using concentrated sulfuric acid was studied, and the influence of H2SO4 co...
| Main Authors: | , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
North Carolina State University
2022-11-01
|
| Series: | BioResources |
| Subjects: | |
| Online Access: | https://ojs.cnr.ncsu.edu/index.php/BRJ/article/view/22020 |
| _version_ | 1797794864637673472 |
|---|---|
| author | Mannan Yang Changqing Fang Jian Su Qi Zhang Ming Liu |
| author_facet | Mannan Yang Changqing Fang Jian Su Qi Zhang Ming Liu |
| author_sort | Mannan Yang |
| collection | DOAJ |
| description | Carbon microsphere was successfully synthesized from waste office paper via hydrothermal method and high temperature treatment in nitrogen atmosphere. The process of carbon microsphere synthesis from waste office paper fiber using concentrated sulfuric acid was studied, and the influence of H2SO4 concentration and reaction time on the hydrolysis reaction was considered. To investigate the mechanism of conversion of waste office paper to carbon microsphere, Fourier transform infrared spectrometry was used to analyze the chemical composition of the supernatant liquid product and the non-carbonized carbon microsphere. The weight loss of the non-carbonized carbon microsphere was assessed through thermogravimetry. Scanning electron microscopy was used to analyze the morphology. The hydrolysis reaction of waste office paper fiber and synthesis mechanism of carbon microsphere under different conditions were evaluated. The results showed that when the reaction time reached 24 h, the product had uniform particle size and was well dispersed, and the more sulfuric acid present led to the waste office paper fiber being more thoroughly hydrolyzed. |
| first_indexed | 2024-03-13T03:09:09Z |
| format | Article |
| id | doaj.art-ba6c6855643041a49d573453df3acee4 |
| institution | Directory Open Access Journal |
| issn | 1930-2126 |
| language | English |
| last_indexed | 2024-03-13T03:09:09Z |
| publishDate | 2022-11-01 |
| publisher | North Carolina State University |
| record_format | Article |
| series | BioResources |
| spelling | doaj.art-ba6c6855643041a49d573453df3acee42023-06-26T18:28:23ZengNorth Carolina State UniversityBioResources1930-21262022-11-011745568557722Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal MethodMannan Yang0Changqing Fang1Jian Su2Qi Zhang3Ming Liu4School of Mechanical and Precision Instrument Engineering, Xi'an University of TechnologyFaculty of Printing, Packaging Engineering and Digital Media Technology, Xi'an University of TechnologyFaculty of Printing, Packaging Engineering and Digital Media Technology, Xi'an University of TechnologyFaculty of Printing, Packaging Engineering and Digital Media Technology, Xi'an University of TechnologyJiangsu Weixing New Materials Co., Ltd., Carbon microsphere was successfully synthesized from waste office paper via hydrothermal method and high temperature treatment in nitrogen atmosphere. The process of carbon microsphere synthesis from waste office paper fiber using concentrated sulfuric acid was studied, and the influence of H2SO4 concentration and reaction time on the hydrolysis reaction was considered. To investigate the mechanism of conversion of waste office paper to carbon microsphere, Fourier transform infrared spectrometry was used to analyze the chemical composition of the supernatant liquid product and the non-carbonized carbon microsphere. The weight loss of the non-carbonized carbon microsphere was assessed through thermogravimetry. Scanning electron microscopy was used to analyze the morphology. The hydrolysis reaction of waste office paper fiber and synthesis mechanism of carbon microsphere under different conditions were evaluated. The results showed that when the reaction time reached 24 h, the product had uniform particle size and was well dispersed, and the more sulfuric acid present led to the waste office paper fiber being more thoroughly hydrolyzed.https://ojs.cnr.ncsu.edu/index.php/BRJ/article/view/22020waste office papercarbon microspherehydrolysishydrothermal method |
| spellingShingle | Mannan Yang Changqing Fang Jian Su Qi Zhang Ming Liu Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal Method BioResources waste office paper carbon microsphere hydrolysis hydrothermal method |
| title | Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal Method |
| title_full | Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal Method |
| title_fullStr | Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal Method |
| title_full_unstemmed | Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal Method |
| title_short | Synthesis Mechanism of Carbon Microsphere from Waste Office Paper via Hydrothermal Method |
| title_sort | synthesis mechanism of carbon microsphere from waste office paper via hydrothermal method |
| topic | waste office paper carbon microsphere hydrolysis hydrothermal method |
| url | https://ojs.cnr.ncsu.edu/index.php/BRJ/article/view/22020 |
| work_keys_str_mv | AT mannanyang synthesismechanismofcarbonmicrospherefromwasteofficepaperviahydrothermalmethod AT changqingfang synthesismechanismofcarbonmicrospherefromwasteofficepaperviahydrothermalmethod AT jiansu synthesismechanismofcarbonmicrospherefromwasteofficepaperviahydrothermalmethod AT qizhang synthesismechanismofcarbonmicrospherefromwasteofficepaperviahydrothermalmethod AT mingliu synthesismechanismofcarbonmicrospherefromwasteofficepaperviahydrothermalmethod |