Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants
Fe-based scaffolds are of particular interest in the technology of biodegradable implants due to their high mechanical properties and biocompatibility. In the present work, using an electroexplosive Fe nanopowder and NaCl particles 100–200 µm in size as a porogen, scaffolds with a porosity of about...
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2022-07-01
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author | Aleksandr S. Lozhkomoev Ales S. Buyakov Sergey O. Kazantsev Elena I. Senkina Maksim G. Krinitcyn Valeria A. Ivanyuk Aliya F. Sharipova Marat I. Lerner |
author_facet | Aleksandr S. Lozhkomoev Ales S. Buyakov Sergey O. Kazantsev Elena I. Senkina Maksim G. Krinitcyn Valeria A. Ivanyuk Aliya F. Sharipova Marat I. Lerner |
author_sort | Aleksandr S. Lozhkomoev |
collection | DOAJ |
description | Fe-based scaffolds are of particular interest in the technology of biodegradable implants due to their high mechanical properties and biocompatibility. In the present work, using an electroexplosive Fe nanopowder and NaCl particles 100–200 µm in size as a porogen, scaffolds with a porosity of about 70 ± 0.8% were obtained. The effect of the sintering temperature on the structure, composition, and mechanical characteristics of the scaffolds was considered. The optimum parameters of the sintering process were determined, allowing us to obtain samples characterized by plastic deformation and a yield strength of up to 16.2 MPa. The degradation of the scaffolds sintered at 1000 and 1100 °C in 0.9 wt.% NaCl solution for 28 days resulted in a decrease in their strength by 23% and 17%, respectively. |
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format | Article |
id | doaj.art-bb053dfe515d4add8a22039f5d976cea |
institution | Directory Open Access Journal |
issn | 1996-1944 |
language | English |
last_indexed | 2024-03-09T06:17:03Z |
publishDate | 2022-07-01 |
publisher | MDPI AG |
record_format | Article |
series | Materials |
spelling | doaj.art-bb053dfe515d4add8a22039f5d976cea2023-12-03T11:52:07ZengMDPI AGMaterials1996-19442022-07-011514490010.3390/ma15144900Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable ImplantsAleksandr S. Lozhkomoev0Ales S. Buyakov1Sergey O. Kazantsev2Elena I. Senkina3Maksim G. Krinitcyn4Valeria A. Ivanyuk5Aliya F. Sharipova6Marat I. Lerner7Institute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaResearch School of Chemistry & Applied Biomedical Sciences, National Research Tomsk Polytechnic University, 634050 Tomsk, RussiaDepartment of Materials Science and Engineering, Technion, Haifa 3200003, IsraelInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaFe-based scaffolds are of particular interest in the technology of biodegradable implants due to their high mechanical properties and biocompatibility. In the present work, using an electroexplosive Fe nanopowder and NaCl particles 100–200 µm in size as a porogen, scaffolds with a porosity of about 70 ± 0.8% were obtained. The effect of the sintering temperature on the structure, composition, and mechanical characteristics of the scaffolds was considered. The optimum parameters of the sintering process were determined, allowing us to obtain samples characterized by plastic deformation and a yield strength of up to 16.2 MPa. The degradation of the scaffolds sintered at 1000 and 1100 °C in 0.9 wt.% NaCl solution for 28 days resulted in a decrease in their strength by 23% and 17%, respectively.https://www.mdpi.com/1996-1944/15/14/4900Fe nanopowderscaffoldsinteringdegradationstrength |
spellingShingle | Aleksandr S. Lozhkomoev Ales S. Buyakov Sergey O. Kazantsev Elena I. Senkina Maksim G. Krinitcyn Valeria A. Ivanyuk Aliya F. Sharipova Marat I. Lerner Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants Materials Fe nanopowder scaffold sintering degradation strength |
title | Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants |
title_full | Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants |
title_fullStr | Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants |
title_full_unstemmed | Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants |
title_short | Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants |
title_sort | preparation and properties of iron nanoparticle based macroporous scaffolds for biodegradable implants |
topic | Fe nanopowder scaffold sintering degradation strength |
url | https://www.mdpi.com/1996-1944/15/14/4900 |
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