Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants

Fe-based scaffolds are of particular interest in the technology of biodegradable implants due to their high mechanical properties and biocompatibility. In the present work, using an electroexplosive Fe nanopowder and NaCl particles 100–200 µm in size as a porogen, scaffolds with a porosity of about...

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Main Authors: Aleksandr S. Lozhkomoev, Ales S. Buyakov, Sergey O. Kazantsev, Elena I. Senkina, Maksim G. Krinitcyn, Valeria A. Ivanyuk, Aliya F. Sharipova, Marat I. Lerner
Format: Article
Language:English
Published: MDPI AG 2022-07-01
Series:Materials
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Online Access:https://www.mdpi.com/1996-1944/15/14/4900
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author Aleksandr S. Lozhkomoev
Ales S. Buyakov
Sergey O. Kazantsev
Elena I. Senkina
Maksim G. Krinitcyn
Valeria A. Ivanyuk
Aliya F. Sharipova
Marat I. Lerner
author_facet Aleksandr S. Lozhkomoev
Ales S. Buyakov
Sergey O. Kazantsev
Elena I. Senkina
Maksim G. Krinitcyn
Valeria A. Ivanyuk
Aliya F. Sharipova
Marat I. Lerner
author_sort Aleksandr S. Lozhkomoev
collection DOAJ
description Fe-based scaffolds are of particular interest in the technology of biodegradable implants due to their high mechanical properties and biocompatibility. In the present work, using an electroexplosive Fe nanopowder and NaCl particles 100–200 µm in size as a porogen, scaffolds with a porosity of about 70 ± 0.8% were obtained. The effect of the sintering temperature on the structure, composition, and mechanical characteristics of the scaffolds was considered. The optimum parameters of the sintering process were determined, allowing us to obtain samples characterized by plastic deformation and a yield strength of up to 16.2 MPa. The degradation of the scaffolds sintered at 1000 and 1100 °C in 0.9 wt.% NaCl solution for 28 days resulted in a decrease in their strength by 23% and 17%, respectively.
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spelling doaj.art-bb053dfe515d4add8a22039f5d976cea2023-12-03T11:52:07ZengMDPI AGMaterials1996-19442022-07-011514490010.3390/ma15144900Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable ImplantsAleksandr S. Lozhkomoev0Ales S. Buyakov1Sergey O. Kazantsev2Elena I. Senkina3Maksim G. Krinitcyn4Valeria A. Ivanyuk5Aliya F. Sharipova6Marat I. Lerner7Institute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaResearch School of Chemistry & Applied Biomedical Sciences, National Research Tomsk Polytechnic University, 634050 Tomsk, RussiaDepartment of Materials Science and Engineering, Technion, Haifa 3200003, IsraelInstitute of Strength Physics and Materials Science of the Siberian Branch of the Russian Academy of Sciences (ISPMS SB RAS), 634021 Tomsk, RussiaFe-based scaffolds are of particular interest in the technology of biodegradable implants due to their high mechanical properties and biocompatibility. In the present work, using an electroexplosive Fe nanopowder and NaCl particles 100–200 µm in size as a porogen, scaffolds with a porosity of about 70 ± 0.8% were obtained. The effect of the sintering temperature on the structure, composition, and mechanical characteristics of the scaffolds was considered. The optimum parameters of the sintering process were determined, allowing us to obtain samples characterized by plastic deformation and a yield strength of up to 16.2 MPa. The degradation of the scaffolds sintered at 1000 and 1100 °C in 0.9 wt.% NaCl solution for 28 days resulted in a decrease in their strength by 23% and 17%, respectively.https://www.mdpi.com/1996-1944/15/14/4900Fe nanopowderscaffoldsinteringdegradationstrength
spellingShingle Aleksandr S. Lozhkomoev
Ales S. Buyakov
Sergey O. Kazantsev
Elena I. Senkina
Maksim G. Krinitcyn
Valeria A. Ivanyuk
Aliya F. Sharipova
Marat I. Lerner
Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants
Materials
Fe nanopowder
scaffold
sintering
degradation
strength
title Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants
title_full Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants
title_fullStr Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants
title_full_unstemmed Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants
title_short Preparation and Properties of Iron Nanoparticle-Based Macroporous Scaffolds for Biodegradable Implants
title_sort preparation and properties of iron nanoparticle based macroporous scaffolds for biodegradable implants
topic Fe nanopowder
scaffold
sintering
degradation
strength
url https://www.mdpi.com/1996-1944/15/14/4900
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