Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment Conditions

Herein, anacardic acid was applied for the preparation of nanosized cellulose using three different 11 treatment conditions including ultrasonication, microwave irradiation, and reflux. Physico-chemical 12 characterization was undertaken using FTIR, TEM, SEM, and XRD. FTIR, TEM, and SEM analyses 13...

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Main Authors: Olugbenga O. Oluwasina, Abiodun D. Aderibigbe, Damilola C. Petinrin, Adeyemi S. Adebisi, Olayinka O. Oluwasina, Oluwasegun J. Wahab
Format: Article
Language:English
Published: Nigerian Society of Physical Sciences 2022-11-01
Series:Journal of Nigerian Society of Physical Sciences
Subjects:
Online Access:https://journal.nsps.org.ng/index.php/jnsps/article/view/949
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author Olugbenga O. Oluwasina
Abiodun D. Aderibigbe
Damilola C. Petinrin
Adeyemi S. Adebisi
Olayinka O. Oluwasina
Oluwasegun J. Wahab
author_facet Olugbenga O. Oluwasina
Abiodun D. Aderibigbe
Damilola C. Petinrin
Adeyemi S. Adebisi
Olayinka O. Oluwasina
Oluwasegun J. Wahab
author_sort Olugbenga O. Oluwasina
collection DOAJ
description Herein, anacardic acid was applied for the preparation of nanosized cellulose using three different 11 treatment conditions including ultrasonication, microwave irradiation, and reflux. Physico-chemical 12 characterization was undertaken using FTIR, TEM, SEM, and XRD. FTIR, TEM, and SEM analyses 13 confirm the preparation of nanosized cellulose with similar chemical but different physical properties as 14 the cellulose starting material. In addition, calculated degrees of crystallinities from XRD data revealed 15 crystallinities of 53.9, 54.4, and 54.7 % for the nanosized cellulose prepared by ultrasonication (UNC), 16 microwave irradiation (MNC), and reflux (RNC) respectively, which all are higher than the 53.3 % of the 17 precursor cellulose. Overall, the study shows that anacardic acid holds potential for the preparation of 18 nanosized cellulose.
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spelling doaj.art-bb36f061b25740bb92846dc13db311902022-12-22T04:38:20ZengNigerian Society of Physical SciencesJournal of Nigerian Society of Physical Sciences2714-28172714-47042022-11-014410.46481/jnsps.2022.949Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment ConditionsOlugbenga O. Oluwasina0Abiodun D. Aderibigbe1Damilola C. Petinrin2Adeyemi S. Adebisi3Olayinka O. Oluwasina4Oluwasegun J. Wahab5Department of Chemistry, Federal University of Technology Akure, P.M.B. 704 Akure, Ondo State, NigeriaDepartment of Chemistry, Federal University of Technology AkureDepartment of Chemistry, Federal University of Technology Akure, P.M.B. 704 Akure, Ondo State, NigeriaDepartment of Chemistry, Federal University of Technology Akure, P.M.B. 704 Akure, Ondo State, NigeriaSchool of Chemistry and Physics, University of KwaZulu-Natal, Westville Campus, Private Bag X54001, 4000, 7 South AfricaDepartment of Chemistry, University of Warwick, Coventry CV4 7AL, United Kingdom Herein, anacardic acid was applied for the preparation of nanosized cellulose using three different 11 treatment conditions including ultrasonication, microwave irradiation, and reflux. Physico-chemical 12 characterization was undertaken using FTIR, TEM, SEM, and XRD. FTIR, TEM, and SEM analyses 13 confirm the preparation of nanosized cellulose with similar chemical but different physical properties as 14 the cellulose starting material. In addition, calculated degrees of crystallinities from XRD data revealed 15 crystallinities of 53.9, 54.4, and 54.7 % for the nanosized cellulose prepared by ultrasonication (UNC), 16 microwave irradiation (MNC), and reflux (RNC) respectively, which all are higher than the 53.3 % of the 17 precursor cellulose. Overall, the study shows that anacardic acid holds potential for the preparation of 18 nanosized cellulose. https://journal.nsps.org.ng/index.php/jnsps/article/view/949Anacardic acidCelluloseNanosized celluloseUltrasonicationRefluxMicrowave irradiation
spellingShingle Olugbenga O. Oluwasina
Abiodun D. Aderibigbe
Damilola C. Petinrin
Adeyemi S. Adebisi
Olayinka O. Oluwasina
Oluwasegun J. Wahab
Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment Conditions
Journal of Nigerian Society of Physical Sciences
Anacardic acid
Cellulose
Nanosized cellulose
Ultrasonication
Reflux
Microwave irradiation
title Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment Conditions
title_full Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment Conditions
title_fullStr Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment Conditions
title_full_unstemmed Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment Conditions
title_short Potential of Anacardic Acid for Nanosized Cellulose Preparation Under Different Treatment Conditions
title_sort potential of anacardic acid for nanosized cellulose preparation under different treatment conditions
topic Anacardic acid
Cellulose
Nanosized cellulose
Ultrasonication
Reflux
Microwave irradiation
url https://journal.nsps.org.ng/index.php/jnsps/article/view/949
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