Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications

A method of wet chemical synthesis suitable for high throughput and combinatorial applications has been developed for the synthesis of porous resistive thick-film gas sensors. This method is based on the robot-controlled application of unstable metal oxide suspensions on an array of 64 inter-digital...

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Main Authors: Wilhelm F. Maier, Ulrich Simon, Daniel Sanders, Andreas Frantzen, Gerald Frenzer
Format: Article
Language:English
Published: MDPI AG 2006-11-01
Series:Sensors
Subjects:
Online Access:http://www.mdpi.com/1424-8220/6/11/1568/
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author Wilhelm F. Maier
Ulrich Simon
Daniel Sanders
Andreas Frantzen
Gerald Frenzer
author_facet Wilhelm F. Maier
Ulrich Simon
Daniel Sanders
Andreas Frantzen
Gerald Frenzer
author_sort Wilhelm F. Maier
collection DOAJ
description A method of wet chemical synthesis suitable for high throughput and combinatorial applications has been developed for the synthesis of porous resistive thick-film gas sensors. This method is based on the robot-controlled application of unstable metal oxide suspensions on an array of 64 inter-digital electrodes positioned on an Al2O3 substrate. SnO2, WO3, ZrO2, TiO2, CeO2, In2O3 and Bi2O3 were chosen as base oxides, and were optimised by doping or mixed oxide formation. The parallel synthesis of mixed oxide sensors is illustrated by representative examples. The electrical characteristics and the sensor performance of the films were measured by high-throughput impedance spectroscopy while supplying various test gases (H2, CO, NO, NO2, propene). Data collection, data mining techniques applied and the best potential sensor materials discovered are presented.
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spelling doaj.art-bb4d9b3dad7a43ce894c71d1144bf1122022-12-22T04:09:04ZengMDPI AGSensors1424-82202006-11-016111568158610.3390/s6111568Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing ApplicationsWilhelm F. MaierUlrich SimonDaniel SandersAndreas FrantzenGerald FrenzerA method of wet chemical synthesis suitable for high throughput and combinatorial applications has been developed for the synthesis of porous resistive thick-film gas sensors. This method is based on the robot-controlled application of unstable metal oxide suspensions on an array of 64 inter-digital electrodes positioned on an Al2O3 substrate. SnO2, WO3, ZrO2, TiO2, CeO2, In2O3 and Bi2O3 were chosen as base oxides, and were optimised by doping or mixed oxide formation. The parallel synthesis of mixed oxide sensors is illustrated by representative examples. The electrical characteristics and the sensor performance of the films were measured by high-throughput impedance spectroscopy while supplying various test gases (H2, CO, NO, NO2, propene). Data collection, data mining techniques applied and the best potential sensor materials discovered are presented.http://www.mdpi.com/1424-8220/6/11/1568/Combinatorial ChemistryHigh ThroughputThick FilmSol-GelSensorMaterials Science.
spellingShingle Wilhelm F. Maier
Ulrich Simon
Daniel Sanders
Andreas Frantzen
Gerald Frenzer
Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications
Sensors
Combinatorial Chemistry
High Throughput
Thick Film
Sol-Gel
Sensor
Materials Science.
title Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications
title_full Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications
title_fullStr Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications
title_full_unstemmed Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications
title_short Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications
title_sort wet chemical synthesis and screening of thick porous oxide films for resistive gas sensing applications
topic Combinatorial Chemistry
High Throughput
Thick Film
Sol-Gel
Sensor
Materials Science.
url http://www.mdpi.com/1424-8220/6/11/1568/
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