Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications
A method of wet chemical synthesis suitable for high throughput and combinatorial applications has been developed for the synthesis of porous resistive thick-film gas sensors. This method is based on the robot-controlled application of unstable metal oxide suspensions on an array of 64 inter-digital...
Main Authors: | , , , , |
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Format: | Article |
Language: | English |
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MDPI AG
2006-11-01
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Series: | Sensors |
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Online Access: | http://www.mdpi.com/1424-8220/6/11/1568/ |
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author | Wilhelm F. Maier Ulrich Simon Daniel Sanders Andreas Frantzen Gerald Frenzer |
author_facet | Wilhelm F. Maier Ulrich Simon Daniel Sanders Andreas Frantzen Gerald Frenzer |
author_sort | Wilhelm F. Maier |
collection | DOAJ |
description | A method of wet chemical synthesis suitable for high throughput and combinatorial applications has been developed for the synthesis of porous resistive thick-film gas sensors. This method is based on the robot-controlled application of unstable metal oxide suspensions on an array of 64 inter-digital electrodes positioned on an Al2O3 substrate. SnO2, WO3, ZrO2, TiO2, CeO2, In2O3 and Bi2O3 were chosen as base oxides, and were optimised by doping or mixed oxide formation. The parallel synthesis of mixed oxide sensors is illustrated by representative examples. The electrical characteristics and the sensor performance of the films were measured by high-throughput impedance spectroscopy while supplying various test gases (H2, CO, NO, NO2, propene). Data collection, data mining techniques applied and the best potential sensor materials discovered are presented. |
first_indexed | 2024-04-11T18:38:56Z |
format | Article |
id | doaj.art-bb4d9b3dad7a43ce894c71d1144bf112 |
institution | Directory Open Access Journal |
issn | 1424-8220 |
language | English |
last_indexed | 2024-04-11T18:38:56Z |
publishDate | 2006-11-01 |
publisher | MDPI AG |
record_format | Article |
series | Sensors |
spelling | doaj.art-bb4d9b3dad7a43ce894c71d1144bf1122022-12-22T04:09:04ZengMDPI AGSensors1424-82202006-11-016111568158610.3390/s6111568Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing ApplicationsWilhelm F. MaierUlrich SimonDaniel SandersAndreas FrantzenGerald FrenzerA method of wet chemical synthesis suitable for high throughput and combinatorial applications has been developed for the synthesis of porous resistive thick-film gas sensors. This method is based on the robot-controlled application of unstable metal oxide suspensions on an array of 64 inter-digital electrodes positioned on an Al2O3 substrate. SnO2, WO3, ZrO2, TiO2, CeO2, In2O3 and Bi2O3 were chosen as base oxides, and were optimised by doping or mixed oxide formation. The parallel synthesis of mixed oxide sensors is illustrated by representative examples. The electrical characteristics and the sensor performance of the films were measured by high-throughput impedance spectroscopy while supplying various test gases (H2, CO, NO, NO2, propene). Data collection, data mining techniques applied and the best potential sensor materials discovered are presented.http://www.mdpi.com/1424-8220/6/11/1568/Combinatorial ChemistryHigh ThroughputThick FilmSol-GelSensorMaterials Science. |
spellingShingle | Wilhelm F. Maier Ulrich Simon Daniel Sanders Andreas Frantzen Gerald Frenzer Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications Sensors Combinatorial Chemistry High Throughput Thick Film Sol-Gel Sensor Materials Science. |
title | Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications |
title_full | Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications |
title_fullStr | Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications |
title_full_unstemmed | Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications |
title_short | Wet Chemical Synthesis and Screening of Thick Porous Oxide Films for Resistive Gas Sensing Applications |
title_sort | wet chemical synthesis and screening of thick porous oxide films for resistive gas sensing applications |
topic | Combinatorial Chemistry High Throughput Thick Film Sol-Gel Sensor Materials Science. |
url | http://www.mdpi.com/1424-8220/6/11/1568/ |
work_keys_str_mv | AT wilhelmfmaier wetchemicalsynthesisandscreeningofthickporousoxidefilmsforresistivegassensingapplications AT ulrichsimon wetchemicalsynthesisandscreeningofthickporousoxidefilmsforresistivegassensingapplications AT danielsanders wetchemicalsynthesisandscreeningofthickporousoxidefilmsforresistivegassensingapplications AT andreasfrantzen wetchemicalsynthesisandscreeningofthickporousoxidefilmsforresistivegassensingapplications AT geraldfrenzer wetchemicalsynthesisandscreeningofthickporousoxidefilmsforresistivegassensingapplications |