XRD investigation of cement pastes incorporating concrete floor polishing waste

Abstract The X-ray diffraction (XRD) technique has been widely used in order to investigate anhydrous and hydrated cement phases. In this study, XRD was used in order to analyze the concrete floor polishing waste (CFPW) and cementitious paste containing CFPW. The diffractograms obtained were compare...

Full description

Bibliographic Details
Main Authors: L. A. Silva, B. O. Nahime, E. C. Lima, J. L. Akasaki, I. C. Reis
Format: Article
Language:English
Published: Associação Brasileira de Cerâmica 2020-10-01
Series:Cerâmica
Subjects:
Online Access:http://www.scielo.br/pdf/ce/v66n380/1678-4553-ce-66-380-373.pdf
_version_ 1819097487262089216
author L. A. Silva
B. O. Nahime
E. C. Lima
J. L. Akasaki
I. C. Reis
author_facet L. A. Silva
B. O. Nahime
E. C. Lima
J. L. Akasaki
I. C. Reis
author_sort L. A. Silva
collection DOAJ
description Abstract The X-ray diffraction (XRD) technique has been widely used in order to investigate anhydrous and hydrated cement phases. In this study, XRD was used in order to analyze the concrete floor polishing waste (CFPW) and cementitious paste containing CFPW. The diffractograms obtained were compared with literature data in order to identify the phases of analyzed materials. Rietveld refinement of XRD pattern of paste containing 12% of CFPW addition was also carried out, in order to analyze calcite and aragonite structures, as these phases are calcium carbonate polymorphs that contribute to matrix filling. XRD pattern of CFPW showed a high concentration of carbonate phases, indicating that the concrete waste was carbonated. The CFPW addition in the cementitious matrix changed the hydrate cement products, as it induced the formation of carboaluminate phases, such as hemicarbonate. Calcite, which is a stable phase, contributed better to the filler effect, as its particles have higher volume than aragonite.
first_indexed 2024-12-22T00:15:52Z
format Article
id doaj.art-bbe900d2c08e46dcafc501856eaea0ce
institution Directory Open Access Journal
issn 1678-4553
language English
last_indexed 2024-12-22T00:15:52Z
publishDate 2020-10-01
publisher Associação Brasileira de Cerâmica
record_format Article
series Cerâmica
spelling doaj.art-bbe900d2c08e46dcafc501856eaea0ce2022-12-21T18:45:18ZengAssociação Brasileira de CerâmicaCerâmica1678-45532020-10-016638037337810.1590/0366-69132020663802956XRD investigation of cement pastes incorporating concrete floor polishing wasteL. A. Silvahttps://orcid.org/0000-0002-8159-7472B. O. NahimeE. C. LimaJ. L. AkasakiI. C. ReisAbstract The X-ray diffraction (XRD) technique has been widely used in order to investigate anhydrous and hydrated cement phases. In this study, XRD was used in order to analyze the concrete floor polishing waste (CFPW) and cementitious paste containing CFPW. The diffractograms obtained were compared with literature data in order to identify the phases of analyzed materials. Rietveld refinement of XRD pattern of paste containing 12% of CFPW addition was also carried out, in order to analyze calcite and aragonite structures, as these phases are calcium carbonate polymorphs that contribute to matrix filling. XRD pattern of CFPW showed a high concentration of carbonate phases, indicating that the concrete waste was carbonated. The CFPW addition in the cementitious matrix changed the hydrate cement products, as it induced the formation of carboaluminate phases, such as hemicarbonate. Calcite, which is a stable phase, contributed better to the filler effect, as its particles have higher volume than aragonite.http://www.scielo.br/pdf/ce/v66n380/1678-4553-ce-66-380-373.pdfcementitious hardened paste wasteXRD qualitative analysisRietveld refinement
spellingShingle L. A. Silva
B. O. Nahime
E. C. Lima
J. L. Akasaki
I. C. Reis
XRD investigation of cement pastes incorporating concrete floor polishing waste
Cerâmica
cementitious hardened paste waste
XRD qualitative analysis
Rietveld refinement
title XRD investigation of cement pastes incorporating concrete floor polishing waste
title_full XRD investigation of cement pastes incorporating concrete floor polishing waste
title_fullStr XRD investigation of cement pastes incorporating concrete floor polishing waste
title_full_unstemmed XRD investigation of cement pastes incorporating concrete floor polishing waste
title_short XRD investigation of cement pastes incorporating concrete floor polishing waste
title_sort xrd investigation of cement pastes incorporating concrete floor polishing waste
topic cementitious hardened paste waste
XRD qualitative analysis
Rietveld refinement
url http://www.scielo.br/pdf/ce/v66n380/1678-4553-ce-66-380-373.pdf
work_keys_str_mv AT lasilva xrdinvestigationofcementpastesincorporatingconcretefloorpolishingwaste
AT bonahime xrdinvestigationofcementpastesincorporatingconcretefloorpolishingwaste
AT eclima xrdinvestigationofcementpastesincorporatingconcretefloorpolishingwaste
AT jlakasaki xrdinvestigationofcementpastesincorporatingconcretefloorpolishingwaste
AT icreis xrdinvestigationofcementpastesincorporatingconcretefloorpolishingwaste