ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action Pressing

ZrC ceramics were prepared by mechanical axial compression of self-propagating high-temperature synthesis/single action pressing (SHS/SAP).The effects of pressure on microstructure and densification of the products,as well as the relationship between displacement/variation of the load curve and SHS...

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Main Authors: CHENG Yong, SU Xun-jia, HOU Gen-liang, SHI Zi-liang, ZHONG Chang-rong, XING Ya-kun
Format: Article
Language:zho
Published: Journal of Materials Engineering 2017-01-01
Series:Cailiao gongcheng
Subjects:
Online Access:http://jme.biam.ac.cn/CN/Y2017/V45/I1/1
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author CHENG Yong
SU Xun-jia
HOU Gen-liang
SHI Zi-liang
ZHONG Chang-rong
XING Ya-kun
author_facet CHENG Yong
SU Xun-jia
HOU Gen-liang
SHI Zi-liang
ZHONG Chang-rong
XING Ya-kun
author_sort CHENG Yong
collection DOAJ
description ZrC ceramics were prepared by mechanical axial compression of self-propagating high-temperature synthesis/single action pressing (SHS/SAP).The effects of pressure on microstructure and densification of the products,as well as the relationship between displacement/variation of the load curve and SHS reaction,were studied.The structure and properties of the products were investigated by XRD and SEM.In addition,the density was measured by the drain away liquid method.Meanwhile,universal testing machine was used to record the displacement and load curve alternations.The results indicate that products are mainly composed of ZrC phase,the process of exhaust are accelerated as the increasing of pressure as well,leading to the smaller size of porosity and crystal particles.Density manifested as an increasing pattern by the elevated pressure with no longer change at 80MPa.Due to the strong attenuation of pressure at the peak of temperature,the density of the production is only 65.7% in 120MPa.The end point of the SHS reaction and the plastic time of the products can be monitored by displacement and load curve.The results provide evidence for the application of self-propagating high-temperature synthesis/pseudo-hot isostatic pressing to further improve the density of ceramics.
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spelling doaj.art-bce568f2227643088f5068742014ba8c2023-01-02T21:47:19ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43811001-43812017-01-014511610.11868/j.issn.1001-4381.2015.00012520170101ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action PressingCHENG Yong0SU Xun-jia1HOU Gen-liang2SHI Zi-liang3ZHONG Chang-rong4XING Ya-kun5Rocket Force University of Engineering, Xi'an 710025, ChinaRocket Force University of Engineering, Xi'an 710025, ChinaRocket Force University of Engineering, Xi'an 710025, ChinaRocket Force University of Engineering, Xi'an 710025, ChinaRocket Force University of Engineering, Xi'an 710025, ChinaChong Qing Communication Constitution, Chongqing 400035, ChinaZrC ceramics were prepared by mechanical axial compression of self-propagating high-temperature synthesis/single action pressing (SHS/SAP).The effects of pressure on microstructure and densification of the products,as well as the relationship between displacement/variation of the load curve and SHS reaction,were studied.The structure and properties of the products were investigated by XRD and SEM.In addition,the density was measured by the drain away liquid method.Meanwhile,universal testing machine was used to record the displacement and load curve alternations.The results indicate that products are mainly composed of ZrC phase,the process of exhaust are accelerated as the increasing of pressure as well,leading to the smaller size of porosity and crystal particles.Density manifested as an increasing pattern by the elevated pressure with no longer change at 80MPa.Due to the strong attenuation of pressure at the peak of temperature,the density of the production is only 65.7% in 120MPa.The end point of the SHS reaction and the plastic time of the products can be monitored by displacement and load curve.The results provide evidence for the application of self-propagating high-temperature synthesis/pseudo-hot isostatic pressing to further improve the density of ceramics.http://jme.biam.ac.cn/CN/Y2017/V45/I1/1SHS/SAPZrCceramicpressure
spellingShingle CHENG Yong
SU Xun-jia
HOU Gen-liang
SHI Zi-liang
ZHONG Chang-rong
XING Ya-kun
ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action Pressing
Cailiao gongcheng
SHS/SAP
ZrC
ceramic
pressure
title ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action Pressing
title_full ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action Pressing
title_fullStr ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action Pressing
title_full_unstemmed ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action Pressing
title_short ZrC Ceramics Prepared by Self-propagating High-temperature Synthesis/Single Action Pressing
title_sort zrc ceramics prepared by self propagating high temperature synthesis single action pressing
topic SHS/SAP
ZrC
ceramic
pressure
url http://jme.biam.ac.cn/CN/Y2017/V45/I1/1
work_keys_str_mv AT chengyong zrcceramicspreparedbyselfpropagatinghightemperaturesynthesissingleactionpressing
AT suxunjia zrcceramicspreparedbyselfpropagatinghightemperaturesynthesissingleactionpressing
AT hougenliang zrcceramicspreparedbyselfpropagatinghightemperaturesynthesissingleactionpressing
AT shiziliang zrcceramicspreparedbyselfpropagatinghightemperaturesynthesissingleactionpressing
AT zhongchangrong zrcceramicspreparedbyselfpropagatinghightemperaturesynthesissingleactionpressing
AT xingyakun zrcceramicspreparedbyselfpropagatinghightemperaturesynthesissingleactionpressing