Synthesis and Properties of SBA-15 Modified with Non-Noble Metals

Modification of SBA-15 with non-noble metal leads to functional materials, which can be applied as gas sensors, adsorbents, and catalysts of various reactions. The new materials contain up to four various metals, which are deposited consecutively or simultaneously at various concentrations ranging f...

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Main Authors: Marek Kosmulski, Edward Mączka, Leszek Ruchomski
Format: Article
Language:English
Published: MDPI AG 2018-11-01
Series:Colloids and Interfaces
Subjects:
Online Access:https://www.mdpi.com/2504-5377/2/4/59
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author Marek Kosmulski
Edward Mączka
Leszek Ruchomski
author_facet Marek Kosmulski
Edward Mączka
Leszek Ruchomski
author_sort Marek Kosmulski
collection DOAJ
description Modification of SBA-15 with non-noble metal leads to functional materials, which can be applied as gas sensors, adsorbents, and catalysts of various reactions. The new materials contain up to four various metals, which are deposited consecutively or simultaneously at various concentrations ranging from a fraction of 1% to an amount that is comparable with the mass of silica-support. These materials contain metals at various oxidation levels, usually as oxides, which occur in crystalline form (a typical crystallite size of about 10 nm matches the width of the SBA-15 channels), but in a few other materials, crystalline metal compounds have not been detected. Many researchers have provided detailed physico- chemical characteristics of SBA-15 modified with non-noble metals by the means of various microscopic and spectroscopic techniques.
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spelling doaj.art-bd54d210893849a99b9069bfbf9e77d52022-12-21T23:32:49ZengMDPI AGColloids and Interfaces2504-53772018-11-01245910.3390/colloids2040059colloids2040059Synthesis and Properties of SBA-15 Modified with Non-Noble MetalsMarek Kosmulski0Edward Mączka1Leszek Ruchomski2Laboratory of Electrochemistry, Lublin University of Technology, Nadbystrzycka 38, 20-618 Lublin, PolandLaboratory of Electrochemistry, Lublin University of Technology, Nadbystrzycka 38, 20-618 Lublin, PolandLaboratory of Electrochemistry, Lublin University of Technology, Nadbystrzycka 38, 20-618 Lublin, PolandModification of SBA-15 with non-noble metal leads to functional materials, which can be applied as gas sensors, adsorbents, and catalysts of various reactions. The new materials contain up to four various metals, which are deposited consecutively or simultaneously at various concentrations ranging from a fraction of 1% to an amount that is comparable with the mass of silica-support. These materials contain metals at various oxidation levels, usually as oxides, which occur in crystalline form (a typical crystallite size of about 10 nm matches the width of the SBA-15 channels), but in a few other materials, crystalline metal compounds have not been detected. Many researchers have provided detailed physico- chemical characteristics of SBA-15 modified with non-noble metals by the means of various microscopic and spectroscopic techniques.https://www.mdpi.com/2504-5377/2/4/59BETXRDTEMFTIRTGARaman
spellingShingle Marek Kosmulski
Edward Mączka
Leszek Ruchomski
Synthesis and Properties of SBA-15 Modified with Non-Noble Metals
Colloids and Interfaces
BET
XRD
TEM
FTIR
TGA
Raman
title Synthesis and Properties of SBA-15 Modified with Non-Noble Metals
title_full Synthesis and Properties of SBA-15 Modified with Non-Noble Metals
title_fullStr Synthesis and Properties of SBA-15 Modified with Non-Noble Metals
title_full_unstemmed Synthesis and Properties of SBA-15 Modified with Non-Noble Metals
title_short Synthesis and Properties of SBA-15 Modified with Non-Noble Metals
title_sort synthesis and properties of sba 15 modified with non noble metals
topic BET
XRD
TEM
FTIR
TGA
Raman
url https://www.mdpi.com/2504-5377/2/4/59
work_keys_str_mv AT marekkosmulski synthesisandpropertiesofsba15modifiedwithnonnoblemetals
AT edwardmaczka synthesisandpropertiesofsba15modifiedwithnonnoblemetals
AT leszekruchomski synthesisandpropertiesofsba15modifiedwithnonnoblemetals