Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particles

Background: Bioactive materials produce a biological reaction such as stimulation of pulpal cells for dentinal repair and induction of the formation of hydroxyapatite. Aim: The study was conducted to evaluate the microhardness of experimental dental composite resins (EDCR) containing nano-hydroxyapa...

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Main Authors: Chaitali Keshav Mirajkar, Jasmin Winnier, Umesh Hambire
Format: Article
Language:English
Published: Wolters Kluwer Medknow Publications 2023-01-01
Series:SRM Journal of Research in Dental Sciences
Subjects:
Online Access:http://www.srmjrds.in/article.asp?issn=0976-433X;year=2023;volume=14;issue=4;spage=172;epage=177;aulast=Mirajkar
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author Chaitali Keshav Mirajkar
Jasmin Winnier
Umesh Hambire
author_facet Chaitali Keshav Mirajkar
Jasmin Winnier
Umesh Hambire
author_sort Chaitali Keshav Mirajkar
collection DOAJ
description Background: Bioactive materials produce a biological reaction such as stimulation of pulpal cells for dentinal repair and induction of the formation of hydroxyapatite. Aim: The study was conducted to evaluate the microhardness of experimental dental composite resins (EDCR) containing nano-hydroxyapatite, zirconia, and glass filler particles. Materials and Methods: The EDCR was prepared with varying concentrations of barium aluminum fluoride glass (5–20 nm), zirconia (4–11 nm), and hydroxyapatite (20–80 nm) filler particles added to the organic matrix. The L9 orthogonal array was used to prepare a sample size of 27 samples. Disc-shaped specimens of 10 mm diameter and 4 mm thickness were prepared using the American Society for Testing and Materials E384 standard for testing the microhardness. The Taguchi's method of optimization was used to obtain a composite with optimum microhardness. A regression model was developed. Results: EDCR with 23.7% of zirconia, 27.5% of nano-hydroxyapatite, and 20% of glass filler particles gave the optimum microhardness of 222.67 HV. The confirmatory experimental test of EDCR gave a microhardness of 225 HV. The model developed with regression equation for the microhardness was 60–123 Z + 114 H + 17.8 G + 2.48 ZH − 0.02 HG + 0.97 Z2 − 3.40 H2. The difference between the R2 (99.9) and adjusted R2 values (99.4) is <0.5, this shows that the model is acceptable. Conclusion: The EDCR developed after using Taguchi's method of optimization had microhardness superior to that of the commercially available composite resins.
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spelling doaj.art-bd756dc3fb8948d19ba92445c83c65ef2024-04-05T08:39:53ZengWolters Kluwer Medknow PublicationsSRM Journal of Research in Dental Sciences2772-52432772-52512023-01-0114417217710.4103/srmjrds.srmjrds_109_23Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particlesChaitali Keshav MirajkarJasmin WinnierUmesh HambireBackground: Bioactive materials produce a biological reaction such as stimulation of pulpal cells for dentinal repair and induction of the formation of hydroxyapatite. Aim: The study was conducted to evaluate the microhardness of experimental dental composite resins (EDCR) containing nano-hydroxyapatite, zirconia, and glass filler particles. Materials and Methods: The EDCR was prepared with varying concentrations of barium aluminum fluoride glass (5–20 nm), zirconia (4–11 nm), and hydroxyapatite (20–80 nm) filler particles added to the organic matrix. The L9 orthogonal array was used to prepare a sample size of 27 samples. Disc-shaped specimens of 10 mm diameter and 4 mm thickness were prepared using the American Society for Testing and Materials E384 standard for testing the microhardness. The Taguchi's method of optimization was used to obtain a composite with optimum microhardness. A regression model was developed. Results: EDCR with 23.7% of zirconia, 27.5% of nano-hydroxyapatite, and 20% of glass filler particles gave the optimum microhardness of 222.67 HV. The confirmatory experimental test of EDCR gave a microhardness of 225 HV. The model developed with regression equation for the microhardness was 60–123 Z + 114 H + 17.8 G + 2.48 ZH − 0.02 HG + 0.97 Z2 − 3.40 H2. The difference between the R2 (99.9) and adjusted R2 values (99.4) is <0.5, this shows that the model is acceptable. Conclusion: The EDCR developed after using Taguchi's method of optimization had microhardness superior to that of the commercially available composite resins.http://www.srmjrds.in/article.asp?issn=0976-433X;year=2023;volume=14;issue=4;spage=172;epage=177;aulast=Mirajkarbiomaterialsdental composite resinsdental materialsglasshydroxyapatitenanofillerszirconia
spellingShingle Chaitali Keshav Mirajkar
Jasmin Winnier
Umesh Hambire
Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particles
SRM Journal of Research in Dental Sciences
biomaterials
dental composite resins
dental materials
glass
hydroxyapatite
nanofillers
zirconia
title Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particles
title_full Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particles
title_fullStr Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particles
title_full_unstemmed Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particles
title_short Optimized regression model for microhardness of experimental dental composite resins with nano-hydroxyapatite filler particles
title_sort optimized regression model for microhardness of experimental dental composite resins with nano hydroxyapatite filler particles
topic biomaterials
dental composite resins
dental materials
glass
hydroxyapatite
nanofillers
zirconia
url http://www.srmjrds.in/article.asp?issn=0976-433X;year=2023;volume=14;issue=4;spage=172;epage=177;aulast=Mirajkar
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AT umeshhambire optimizedregressionmodelformicrohardnessofexperimentaldentalcompositeresinswithnanohydroxyapatitefillerparticles