Tin dioxide nanoparticles for waste water treatment: facile synthesis and characterization

Tin dioxide nanoparticles (SnO2 NPs) are synthesized by using Buxus wallichiana ( B. Wallichiana ) leaf extract. To determine the surface area (138.2 m ^2 g ^−1 ) and pore size of the SnO2 NPs, the nitrogen adsorption-desorption method used. The average crystallite size was determined to be 38 nm us...

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Main Authors: Rimsha Ehsan, Sirajul Haq, Nadia Shahzad, Manel Ben Ali, Fethi Ben Abdallah, Montasser M Hassan, Amor Hedfi, Salah Ud Din, Muhammad Imran Shahzad
Format: Article
Language:English
Published: IOP Publishing 2022-01-01
Series:Materials Research Express
Subjects:
Online Access:https://doi.org/10.1088/2053-1591/ac6cce
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author Rimsha Ehsan
Sirajul Haq
Nadia Shahzad
Manel Ben Ali
Fethi Ben Abdallah
Montasser M Hassan
Amor Hedfi
Salah Ud Din
Muhammad Imran Shahzad
author_facet Rimsha Ehsan
Sirajul Haq
Nadia Shahzad
Manel Ben Ali
Fethi Ben Abdallah
Montasser M Hassan
Amor Hedfi
Salah Ud Din
Muhammad Imran Shahzad
author_sort Rimsha Ehsan
collection DOAJ
description Tin dioxide nanoparticles (SnO2 NPs) are synthesized by using Buxus wallichiana ( B. Wallichiana ) leaf extract. To determine the surface area (138.2 m ^2 g ^−1 ) and pore size of the SnO2 NPs, the nitrogen adsorption-desorption method used. The average crystallite size was determined to be 38 nm using x-ray diffraction (XRD). Scanning electron microscopy (SEM), diffuse reflectance spectroscopy (DRS), were used to investigate the structural and optical properties of SnO _2 NPs with a band gap of 3.69 eV. Fourier transform infrared (FTIR) spectroscopy was used for the chemical analysis. In this experiment, methyl orange (MO) was deteriorated in the presence of artificial sun light for 140 min, where 97.50 percent of the dye decolorized. A 15 ppm solution of MO with the pH 6, was treated in the presence of 20 mg of the catalyst, resulting in the highest photocatalytic activity.
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spelling doaj.art-bdaf721d52a74eff8625596355fc17f22023-08-09T16:14:07ZengIOP PublishingMaterials Research Express2053-15912022-01-019505500610.1088/2053-1591/ac6cceTin dioxide nanoparticles for waste water treatment: facile synthesis and characterizationRimsha Ehsan0Sirajul Haq1https://orcid.org/0000-0002-9424-2531Nadia Shahzad2https://orcid.org/0000-0002-1414-772XManel Ben Ali3Fethi Ben Abdallah4Montasser M Hassan5Amor Hedfi6Salah Ud Din7Muhammad Imran Shahzad8https://orcid.org/0000-0002-5687-8889Department of Chemistry, University of Azad Jammu and Kashmir , Muzaffarabad, 13100, PakistanDepartment of Chemistry, University of Azad Jammu and Kashmir , Muzaffarabad, 13100, PakistanUS-Pakistan Centre for Advanced Studies in Energy, National University of Science and Technology (NUST) , 44000 Islamabad, PakistanDepartment of Biology, College of Sciences, Taif University , PO Box 11099, Taif 21944, Saudi ArabiaDepartment of Biology, College of Sciences, Taif University , PO Box 11099, Taif 21944, Saudi ArabiaDepartment of Biology, College of Sciences, Taif University , PO Box 11099, Taif 21944, Saudi ArabiaDepartment of Biology, College of Sciences, Taif University , PO Box 11099, Taif 21944, Saudi ArabiaDepartment of Chemistry, University of Azad Jammu and Kashmir , Muzaffarabad, 13100, PakistanNanosciences and Technology Department (NS & TD), National Center for Physics (NCP), 44000 Islamabad, PakistanTin dioxide nanoparticles (SnO2 NPs) are synthesized by using Buxus wallichiana ( B. Wallichiana ) leaf extract. To determine the surface area (138.2 m ^2 g ^−1 ) and pore size of the SnO2 NPs, the nitrogen adsorption-desorption method used. The average crystallite size was determined to be 38 nm using x-ray diffraction (XRD). Scanning electron microscopy (SEM), diffuse reflectance spectroscopy (DRS), were used to investigate the structural and optical properties of SnO _2 NPs with a band gap of 3.69 eV. Fourier transform infrared (FTIR) spectroscopy was used for the chemical analysis. In this experiment, methyl orange (MO) was deteriorated in the presence of artificial sun light for 140 min, where 97.50 percent of the dye decolorized. A 15 ppm solution of MO with the pH 6, was treated in the presence of 20 mg of the catalyst, resulting in the highest photocatalytic activity.https://doi.org/10.1088/2053-1591/ac6ccetin dioxidebuxus wallichianaphotocatalytic activity
spellingShingle Rimsha Ehsan
Sirajul Haq
Nadia Shahzad
Manel Ben Ali
Fethi Ben Abdallah
Montasser M Hassan
Amor Hedfi
Salah Ud Din
Muhammad Imran Shahzad
Tin dioxide nanoparticles for waste water treatment: facile synthesis and characterization
Materials Research Express
tin dioxide
buxus wallichiana
photocatalytic activity
title Tin dioxide nanoparticles for waste water treatment: facile synthesis and characterization
title_full Tin dioxide nanoparticles for waste water treatment: facile synthesis and characterization
title_fullStr Tin dioxide nanoparticles for waste water treatment: facile synthesis and characterization
title_full_unstemmed Tin dioxide nanoparticles for waste water treatment: facile synthesis and characterization
title_short Tin dioxide nanoparticles for waste water treatment: facile synthesis and characterization
title_sort tin dioxide nanoparticles for waste water treatment facile synthesis and characterization
topic tin dioxide
buxus wallichiana
photocatalytic activity
url https://doi.org/10.1088/2053-1591/ac6cce
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