Structural and morphological characterizations of glass based composites in thin films form

By using a low-cost sol gel method, neat and loaded phosphate glass containing Cr, Co, Ni, and Zn was synthesized and then placed on a silica glass substrate. Cr, Ni, Co, and Zn loading amounts were diluted inside the matrix using rates varying from 0 wt% to 16 wt% in order to study the impact of lo...

Full description

Bibliographic Details
Main Authors: Maryama Hammi, Amine El Haimeur
Format: Article
Language:English
Published: Elsevier 2023-04-01
Series:Heliyon
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2405844023021746
_version_ 1797837052656484352
author Maryama Hammi
Amine El Haimeur
author_facet Maryama Hammi
Amine El Haimeur
author_sort Maryama Hammi
collection DOAJ
description By using a low-cost sol gel method, neat and loaded phosphate glass containing Cr, Co, Ni, and Zn was synthesized and then placed on a silica glass substrate. Cr, Ni, Co, and Zn loading amounts were diluted inside the matrix using rates varying from 0 wt% to 16 wt% in order to study the impact of loading elements on glass characteristics. By using XRD and SEM, it was determined how loading factors affected the structural and morphological characteristics of glass thin layers. When the annealing temperature was maintained at 250 °C, X-ray diffractograms revealed that the deposited glass films had an amorphous nature, whilst also X-ray pattern results revealed that the loaded films had a low crystalline nature. Morphology studies indicated the homogeneity and the edge of crystallinity of the obtained thin films. All results were described in detail and they indicated that the films prepared in this study can be used in many nanotechnology applications.
first_indexed 2024-04-09T15:18:38Z
format Article
id doaj.art-bdbcf1afe2d242369715206a86bc8499
institution Directory Open Access Journal
issn 2405-8440
language English
last_indexed 2024-04-09T15:18:38Z
publishDate 2023-04-01
publisher Elsevier
record_format Article
series Heliyon
spelling doaj.art-bdbcf1afe2d242369715206a86bc84992023-04-29T14:52:21ZengElsevierHeliyon2405-84402023-04-0194e14967Structural and morphological characterizations of glass based composites in thin films formMaryama Hammi0Amine El Haimeur1Faculty of Sciences, University of Mohammed V-Rabat, BP1014, Rabat, Morocco; Corresponding author.Laboratory of Materials Physics and Subatomic, Faculty of Science, University Ibn Tofail, BP.133-14000, Kénitra, MoroccoBy using a low-cost sol gel method, neat and loaded phosphate glass containing Cr, Co, Ni, and Zn was synthesized and then placed on a silica glass substrate. Cr, Ni, Co, and Zn loading amounts were diluted inside the matrix using rates varying from 0 wt% to 16 wt% in order to study the impact of loading elements on glass characteristics. By using XRD and SEM, it was determined how loading factors affected the structural and morphological characteristics of glass thin layers. When the annealing temperature was maintained at 250 °C, X-ray diffractograms revealed that the deposited glass films had an amorphous nature, whilst also X-ray pattern results revealed that the loaded films had a low crystalline nature. Morphology studies indicated the homogeneity and the edge of crystallinity of the obtained thin films. All results were described in detail and they indicated that the films prepared in this study can be used in many nanotechnology applications.http://www.sciencedirect.com/science/article/pii/S2405844023021746Sol gel techniqueUnloadedLoadedXRDSEM
spellingShingle Maryama Hammi
Amine El Haimeur
Structural and morphological characterizations of glass based composites in thin films form
Heliyon
Sol gel technique
Unloaded
Loaded
XRD
SEM
title Structural and morphological characterizations of glass based composites in thin films form
title_full Structural and morphological characterizations of glass based composites in thin films form
title_fullStr Structural and morphological characterizations of glass based composites in thin films form
title_full_unstemmed Structural and morphological characterizations of glass based composites in thin films form
title_short Structural and morphological characterizations of glass based composites in thin films form
title_sort structural and morphological characterizations of glass based composites in thin films form
topic Sol gel technique
Unloaded
Loaded
XRD
SEM
url http://www.sciencedirect.com/science/article/pii/S2405844023021746
work_keys_str_mv AT maryamahammi structuralandmorphologicalcharacterizationsofglassbasedcompositesinthinfilmsform
AT amineelhaimeur structuralandmorphologicalcharacterizationsofglassbasedcompositesinthinfilmsform