1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide
In the title molecule, C10H13N3O3S, the thiosemicarbazide =N—NH—C(=S)—NH– fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)°]. A weak N—H...S hydrogen bond [3.480&#...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2010-05-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810014078 |
| _version_ | 1818913482450403328 |
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| author | Hana Bashir Shawish M. Jamil Maah Seik Weng Ng |
| author_facet | Hana Bashir Shawish M. Jamil Maah Seik Weng Ng |
| author_sort | Hana Bashir Shawish |
| collection | DOAJ |
| description | In the title molecule, C10H13N3O3S, the thiosemicarbazide =N—NH—C(=S)—NH– fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)°]. A weak N—H...S hydrogen bond [3.480 (1) Å] links two molecules about a center of inversion to generate a ring. The hydroxy groups are engaged in intermolecular hydrogen bonding; the O—H...O and O—H...S hydrogen bonds generate a layer motif. |
| first_indexed | 2024-12-19T23:31:11Z |
| format | Article |
| id | doaj.art-be12193dcda14ca7b76d1aa3194cf40b |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-19T23:31:11Z |
| publishDate | 2010-05-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-be12193dcda14ca7b76d1aa3194cf40b2022-12-21T20:01:44ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-05-01665o1151o115110.1107/S16005368100140781-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazideHana Bashir ShawishM. Jamil MaahSeik Weng NgIn the title molecule, C10H13N3O3S, the thiosemicarbazide =N—NH—C(=S)—NH– fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)°]. A weak N—H...S hydrogen bond [3.480 (1) Å] links two molecules about a center of inversion to generate a ring. The hydroxy groups are engaged in intermolecular hydrogen bonding; the O—H...O and O—H...S hydrogen bonds generate a layer motif.http://scripts.iucr.org/cgi-bin/paper?S1600536810014078 |
| spellingShingle | Hana Bashir Shawish M. Jamil Maah Seik Weng Ng 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide Acta Crystallographica Section E |
| title | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_full | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_fullStr | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_full_unstemmed | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_short | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_sort | 1 2 3 4 trihydroxybenzylidene 4 ethylthiosemicarbazide |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810014078 |
| work_keys_str_mv | AT hanabashirshawish 1234trihydroxybenzylidene4ethylthiosemicarbazide AT mjamilmaah 1234trihydroxybenzylidene4ethylthiosemicarbazide AT seikwengng 1234trihydroxybenzylidene4ethylthiosemicarbazide |