Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)

Electrochemical impedance spectroscopy (EIS) was used to detect stress corrosion cracking (SCC) in stainless steel 304 alloy exposed to an aqueous environment at 120 °C. Stainless steel 304 alloy as u-bend was tested in the solution that contains 40 weight percent of magnesium chloride. U-bended sam...

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Main Authors: J. Neshati, B. Adib, A. Sardashti
Format: Article
Language:English
Published: Reaserch Institute of Petroleum Industry 2012-01-01
Series:Journal of Petroleum Science and Technology
Subjects:
Online Access:https://jpst.ripi.ir/article_94_79ee9fa4546b595c2ad22d37b9e23a10.pdf
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author J. Neshati
B. Adib
A. Sardashti
author_facet J. Neshati
B. Adib
A. Sardashti
author_sort J. Neshati
collection DOAJ
description Electrochemical impedance spectroscopy (EIS) was used to detect stress corrosion cracking (SCC) in stainless steel 304 alloy exposed to an aqueous environment at 120 °C. Stainless steel 304 alloy as u-bend was tested in the solution that contains 40 weight percent of magnesium chloride. U-bended samples were prepared according to ASTM G30. EIS measurements were always performed simultaneously on u-bend samples under stress and non-stress conditions. The results indicate that changes in phase shift versus time could be related to the stress corrosion cracking process. Stress corrosion cracking is detectable at a frequency of 23.95 Hz. EIS measurement can be used for SCC monitoring in u-bend samples. Finally, analysis of the fracture surface by using metallographic and SEM techniques confirmed the EIS results.
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spelling doaj.art-bed3c0a648b348abbfb246018cf5114e2022-12-22T01:12:38ZengReaserch Institute of Petroleum IndustryJournal of Petroleum Science and Technology2251-659X2645-33122012-01-0121556010.22078/jpst.2012.9494Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)J. Neshati0B. Adib1A. Sardashti2Corrosion Department, Research Institute of Petroleum Industry (RIPI)Department of Chemistry, Islamic Azad University, North Tehran BranchDepartment of Chemistry, Islamic Azad University, North Tehran BranchElectrochemical impedance spectroscopy (EIS) was used to detect stress corrosion cracking (SCC) in stainless steel 304 alloy exposed to an aqueous environment at 120 °C. Stainless steel 304 alloy as u-bend was tested in the solution that contains 40 weight percent of magnesium chloride. U-bended samples were prepared according to ASTM G30. EIS measurements were always performed simultaneously on u-bend samples under stress and non-stress conditions. The results indicate that changes in phase shift versus time could be related to the stress corrosion cracking process. Stress corrosion cracking is detectable at a frequency of 23.95 Hz. EIS measurement can be used for SCC monitoring in u-bend samples. Finally, analysis of the fracture surface by using metallographic and SEM techniques confirmed the EIS results.https://jpst.ripi.ir/article_94_79ee9fa4546b595c2ad22d37b9e23a10.pdfstress corrosion crackingstainless steel 304u-bendmonitoringeis
spellingShingle J. Neshati
B. Adib
A. Sardashti
Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)
Journal of Petroleum Science and Technology
stress corrosion cracking
stainless steel 304
u-bend
monitoring
eis
title Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)
title_full Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)
title_fullStr Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)
title_full_unstemmed Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)
title_short Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)
title_sort stress corrosion cracking detection of sensitized stainless steel 304 in chloride media by using electrochemical impedance spectroscopy eis
topic stress corrosion cracking
stainless steel 304
u-bend
monitoring
eis
url https://jpst.ripi.ir/article_94_79ee9fa4546b595c2ad22d37b9e23a10.pdf
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