Study on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coating

A low-frequency composite absorbing material with high permeability and low permittivity in low frequency was prepared after the flaky FeSiAl alloy powder was annealed in N _2 atmosphere and modified with zinc-based phosphate solution. The effects of annealing temperature and phosphating time on the...

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Main Authors: Ze Li, Jianjiang Wang, Fang Zhao
Format: Article
Language:English
Published: IOP Publishing 2021-01-01
Series:Materials Research Express
Subjects:
Online Access:https://doi.org/10.1088/2053-1591/ac0abb
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author Ze Li
Jianjiang Wang
Fang Zhao
author_facet Ze Li
Jianjiang Wang
Fang Zhao
author_sort Ze Li
collection DOAJ
description A low-frequency composite absorbing material with high permeability and low permittivity in low frequency was prepared after the flaky FeSiAl alloy powder was annealed in N _2 atmosphere and modified with zinc-based phosphate solution. The effects of annealing temperature and phosphating time on the phase composition, morphology and static magnetic properties of the flaky FeSiAl alloy were investigated with x-ray diffraction (XRD), scanning electron microscope (SEM) and vibrating sample magnetometer (VSM). With the aid of vector network analyzer (VNA), the electromagnetic properties and absorbing performance of the powder treated in two ways were studied. The results showed that after annealing in N _2 atmosphere, the crystallization degree of FeSiAl powder increased, the crystal type underwent a phase transition of A2-A2/B2-A2/B2/D03, the permittivity decreased, and the permeability was greatly improved. After phosphating, the phosphating reaction products were deposited on the surface of FeSiAl particles, the permittivity was significantly reduced, the low-frequency impedance matching and low-frequency absorption performance were improved. The causes and frequency changes of electromagnetic wave absorption peaks were analyzed with the λ /4 interference cancellation theory, the interface reflection model and the impedance matching principle.
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spelling doaj.art-bf18bf85012c4833a7a592bfb8e11b482023-08-09T15:50:23ZengIOP PublishingMaterials Research Express2053-15912021-01-018606652610.1088/2053-1591/ac0abbStudy on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coatingZe Li0https://orcid.org/0000-0002-3278-241XJianjiang Wang1Fang Zhao2Shijiazhuang Campus, PLA Army Engineering University , Shijiazhuang 050003, People’s Republic of ChinaHebei University of Science And Technology , Shijiazhuang 050003, People’s Republic of ChinaShijiazhuang Campus, PLA Army Engineering University , Shijiazhuang 050003, People’s Republic of ChinaA low-frequency composite absorbing material with high permeability and low permittivity in low frequency was prepared after the flaky FeSiAl alloy powder was annealed in N _2 atmosphere and modified with zinc-based phosphate solution. The effects of annealing temperature and phosphating time on the phase composition, morphology and static magnetic properties of the flaky FeSiAl alloy were investigated with x-ray diffraction (XRD), scanning electron microscope (SEM) and vibrating sample magnetometer (VSM). With the aid of vector network analyzer (VNA), the electromagnetic properties and absorbing performance of the powder treated in two ways were studied. The results showed that after annealing in N _2 atmosphere, the crystallization degree of FeSiAl powder increased, the crystal type underwent a phase transition of A2-A2/B2-A2/B2/D03, the permittivity decreased, and the permeability was greatly improved. After phosphating, the phosphating reaction products were deposited on the surface of FeSiAl particles, the permittivity was significantly reduced, the low-frequency impedance matching and low-frequency absorption performance were improved. The causes and frequency changes of electromagnetic wave absorption peaks were analyzed with the λ /4 interference cancellation theory, the interface reflection model and the impedance matching principle.https://doi.org/10.1088/2053-1591/ac0abbFeSiAllow-frequency absorbing materialsannealingphosphatingelectromagnetic performance
spellingShingle Ze Li
Jianjiang Wang
Fang Zhao
Study on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coating
Materials Research Express
FeSiAl
low-frequency absorbing materials
annealing
phosphating
electromagnetic performance
title Study on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coating
title_full Study on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coating
title_fullStr Study on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coating
title_full_unstemmed Study on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coating
title_short Study on the electromagnetic properties and microwave absorbing mechanism of flaky FeSiAl alloy based on annealing and phosphate coating
title_sort study on the electromagnetic properties and microwave absorbing mechanism of flaky fesial alloy based on annealing and phosphate coating
topic FeSiAl
low-frequency absorbing materials
annealing
phosphating
electromagnetic performance
url https://doi.org/10.1088/2053-1591/ac0abb
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AT jianjiangwang studyontheelectromagneticpropertiesandmicrowaveabsorbingmechanismofflakyfesialalloybasedonannealingandphosphatecoating
AT fangzhao studyontheelectromagneticpropertiesandmicrowaveabsorbingmechanismofflakyfesialalloybasedonannealingandphosphatecoating