Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn Steel

This paper presents the results of martensite tempering resistance in 4% Mn steel. The material was quenched and tempered at 350 °C for 15, 30, and 60 min. The analysis of the quenching and tempering was carried out using dilatometric and microstructural approaches. The phase composition was assesse...

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Main Authors: Adam Grajcar, Mateusz Morawiec, Jose Antonio Jimenez, Carlos Garcia-Mateo
Format: Article
Language:English
Published: MDPI AG 2020-10-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/13/19/4442
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author Adam Grajcar
Mateusz Morawiec
Jose Antonio Jimenez
Carlos Garcia-Mateo
author_facet Adam Grajcar
Mateusz Morawiec
Jose Antonio Jimenez
Carlos Garcia-Mateo
author_sort Adam Grajcar
collection DOAJ
description This paper presents the results of martensite tempering resistance in 4% Mn steel. The material was quenched and tempered at 350 °C for 15, 30, and 60 min. The analysis of the quenching and tempering was carried out using dilatometric and microstructural approaches. The phase composition was assessed using X-ray diffraction. The M<sub>s</sub> temperature and tempering progress were simulated using JMatPro software. The dilatometric analysis revealed a small decrease in the relative change in length (RCL) during tempering. This decrease was connected to the precipitation kinetics of cementite within the martensite laths. The microstructure investigation using a scanning electron microscope showed a very small amount of carbides, even for the longest tempering time. This showed the high tempering resistance of the martensite in medium-Mn steels. The hardness results showed an insignificant decrease in the hardness depending on the tempering time, which confirmed the high tempering resistance of martensite.
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spelling doaj.art-bfbee9d44aa24bdeb1a0a7f81ebf7a072023-11-20T16:16:15ZengMDPI AGMaterials1996-19442020-10-011319444210.3390/ma13194442Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn SteelAdam Grajcar0Mateusz Morawiec1Jose Antonio Jimenez2Carlos Garcia-Mateo3Department of Engineering Materials and Biomaterials, Silesian University of Technology, 44-100 Gliwice, PolandDepartment of Engineering Materials and Biomaterials, Silesian University of Technology, 44-100 Gliwice, PolandDepartment of Physical Metallurgy, National Center for Metallurgical Research, 28040 Madrid, SpainDepartment of Physical Metallurgy, National Center for Metallurgical Research, 28040 Madrid, SpainThis paper presents the results of martensite tempering resistance in 4% Mn steel. The material was quenched and tempered at 350 °C for 15, 30, and 60 min. The analysis of the quenching and tempering was carried out using dilatometric and microstructural approaches. The phase composition was assessed using X-ray diffraction. The M<sub>s</sub> temperature and tempering progress were simulated using JMatPro software. The dilatometric analysis revealed a small decrease in the relative change in length (RCL) during tempering. This decrease was connected to the precipitation kinetics of cementite within the martensite laths. The microstructure investigation using a scanning electron microscope showed a very small amount of carbides, even for the longest tempering time. This showed the high tempering resistance of the martensite in medium-Mn steels. The hardness results showed an insignificant decrease in the hardness depending on the tempering time, which confirmed the high tempering resistance of martensite.https://www.mdpi.com/1996-1944/13/19/4442quenchingtemperingmedium-Mn steelmartensitic transformationdilatometrycementite precipitation
spellingShingle Adam Grajcar
Mateusz Morawiec
Jose Antonio Jimenez
Carlos Garcia-Mateo
Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn Steel
Materials
quenching
tempering
medium-Mn steel
martensitic transformation
dilatometry
cementite precipitation
title Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn Steel
title_full Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn Steel
title_fullStr Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn Steel
title_full_unstemmed Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn Steel
title_short Dilatometric and Microstructural Study of Martensite Tempering in 4% Mn Steel
title_sort dilatometric and microstructural study of martensite tempering in 4 mn steel
topic quenching
tempering
medium-Mn steel
martensitic transformation
dilatometry
cementite precipitation
url https://www.mdpi.com/1996-1944/13/19/4442
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AT carlosgarciamateo dilatometricandmicrostructuralstudyofmartensitetemperingin4mnsteel