The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodeposition
<p>CuInSe<sub>2</sub> with chalcopyrite structure has become one of the most promising photoelectric materials for its high optical absorption coefficient and conversion efficiency. Electrodeposition has the advantages of low cost and easy operation. CuInSe<sub>2</sub>...
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Kaunas University of Technology
2017-11-01
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Series: | Medžiagotyra |
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Online Access: | http://matsc.ktu.lt/index.php/MatSc/article/view/17447 |
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author | Kegao LIU Chao XU Hong LIU Yong HU Ludan SHI |
author_facet | Kegao LIU Chao XU Hong LIU Yong HU Ludan SHI |
author_sort | Kegao LIU |
collection | DOAJ |
description | <p>CuInSe<sub>2</sub> with chalcopyrite structure has become one of the most promising photoelectric materials for its high optical absorption coefficient and conversion efficiency. Electrodeposition has the advantages of low cost and easy operation. CuInSe<sub>2</sub> thin films were prepared by one-step electrodeposition with CuC1<sub>2</sub>·2H<sub>2</sub>O, InC1<sub>3</sub>, SeO<sub>2</sub> as raw materials. Cyclic voltammetry curves of the solutions were tested by electrochemical workstation. The phases of product thin films were analyzed by X-ray diffraction (XRD) and the surface morphology was characterized by scanning electron microscope (SEM). Experimental results show that the continuous, uniform and dense CuInSe<sub>2</sub> thin films can be obtained under conditions of deposition potential -0.5 V and sodium citrate as complexing agent with concentration of 5mmol/L. The XRD diffraction peaks of CuInSe<sub>2</sub> thin film are corresponding to the crystal planes of (112), (220) and (312) respectively.</p><p>DOI: <a href="http://dx.doi.org/10.5755/j01.ms.23.4.17447">http://dx.doi.org/10.5755/j01.ms.23.4.17447</a></p> |
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issn | 1392-1320 2029-7289 |
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spelling | doaj.art-c0d55e3ade3a4f4499e73a77a6636e6e2022-12-22T00:16:03ZengKaunas University of TechnologyMedžiagotyra1392-13202029-72892017-11-0123431331610.5755/j01.ms.23.4.174478731The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodepositionKegao LIU0Chao XUHong LIUYong HULudan SHIShandong Jianzhu University<p>CuInSe<sub>2</sub> with chalcopyrite structure has become one of the most promising photoelectric materials for its high optical absorption coefficient and conversion efficiency. Electrodeposition has the advantages of low cost and easy operation. CuInSe<sub>2</sub> thin films were prepared by one-step electrodeposition with CuC1<sub>2</sub>·2H<sub>2</sub>O, InC1<sub>3</sub>, SeO<sub>2</sub> as raw materials. Cyclic voltammetry curves of the solutions were tested by electrochemical workstation. The phases of product thin films were analyzed by X-ray diffraction (XRD) and the surface morphology was characterized by scanning electron microscope (SEM). Experimental results show that the continuous, uniform and dense CuInSe<sub>2</sub> thin films can be obtained under conditions of deposition potential -0.5 V and sodium citrate as complexing agent with concentration of 5mmol/L. The XRD diffraction peaks of CuInSe<sub>2</sub> thin film are corresponding to the crystal planes of (112), (220) and (312) respectively.</p><p>DOI: <a href="http://dx.doi.org/10.5755/j01.ms.23.4.17447">http://dx.doi.org/10.5755/j01.ms.23.4.17447</a></p>http://matsc.ktu.lt/index.php/MatSc/article/view/17447CuInSe2thin filmphotoelectricone-step electrodeposition |
spellingShingle | Kegao LIU Chao XU Hong LIU Yong HU Ludan SHI The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodeposition Medžiagotyra CuInSe2 thin film photoelectric one-step electrodeposition |
title | The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodeposition |
title_full | The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodeposition |
title_fullStr | The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodeposition |
title_full_unstemmed | The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodeposition |
title_short | The Phase and Morphology of CuInSe2 Film Prepared by One-Step electrodeposition |
title_sort | phase and morphology of cuinse2 film prepared by one step electrodeposition |
topic | CuInSe2 thin film photoelectric one-step electrodeposition |
url | http://matsc.ktu.lt/index.php/MatSc/article/view/17447 |
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