Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed Fusion

Hydrogen was doped in austenitic stainless steel (ASS) 316L tensile samples produced by the laser-powder bed fusion (L-PBF) technique. For this aim, an electrochemical method was conducted under a high current density of 100 mA/cm<sup>2</sup> for three days to examine its sustainability...

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Main Authors: Farzaneh Khaleghifar, Khashayar Razeghi, Akbar Heidarzadeh, Reza Taherzadeh Mousavian
Format: Article
Language:English
Published: MDPI AG 2021-04-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/11/4/586
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author Farzaneh Khaleghifar
Khashayar Razeghi
Akbar Heidarzadeh
Reza Taherzadeh Mousavian
author_facet Farzaneh Khaleghifar
Khashayar Razeghi
Akbar Heidarzadeh
Reza Taherzadeh Mousavian
author_sort Farzaneh Khaleghifar
collection DOAJ
description Hydrogen was doped in austenitic stainless steel (ASS) 316L tensile samples produced by the laser-powder bed fusion (L-PBF) technique. For this aim, an electrochemical method was conducted under a high current density of 100 mA/cm<sup>2</sup> for three days to examine its sustainability under extreme hydrogen environments at ambient temperatures. The chemical composition of the starting powders contained a high amount of Ni, approximately 12.9 wt.%, as a strong austenite stabilizer. The tensile tests disclosed that hydrogen charging caused a minor reduction in the elongation to failure (approximately 3.5% on average) and ultimate tensile strength (UTS; approximately 2.1% on average) of the samples, using a low strain rate of 1.2 × 10<sup>−4</sup> s<sup>−1</sup>. It was also found that an increase in the strain rate from 1.2 × 10<sup>−4</sup> s<sup>−1</sup> to 4.8 × 10<sup>−4</sup> s<sup>−1</sup> led to a reduction of approximately 3.6% on average for the elongation to failure and 1.7% on average for UTS in the pre-charged samples. No trace of martensite was detected in the X-ray diffraction (XRD) analysis of the fractured samples thanks to the high Ni content, which caused a minor reduction in UTS × uniform elongation (UE) (GPa%) after the H charging. Considerable surface tearing was observed for the pre-charged sample after the tensile deformation. Additionally, some cracks were observed to be independent of the melt pool boundaries, indicating that such boundaries cannot necessarily act as a suitable area for the crack propagation.
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spelling doaj.art-c14211ba97754335bbff989115bee6352023-11-21T14:07:33ZengMDPI AGMetals2075-47012021-04-0111458610.3390/met11040586Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed FusionFarzaneh Khaleghifar0Khashayar Razeghi1Akbar Heidarzadeh2Reza Taherzadeh Mousavian3Razi Applied Science Foundation, P.O. Box, Tehran 37531-46137, IranRazi Applied Science Foundation, P.O. Box, Tehran 37531-46137, IranDepartment of Materials Engineering, Azarbaijan Shahid Madani University, P.O. Box, Tabriz 53714-161, IranI-Form, Advanced Manufacturing Research Centre & Advanced Processing Technology Research Centre, School of Mechanical & Manufacturing Engineering, Dublin City University, 9 Dublin, IrelandHydrogen was doped in austenitic stainless steel (ASS) 316L tensile samples produced by the laser-powder bed fusion (L-PBF) technique. For this aim, an electrochemical method was conducted under a high current density of 100 mA/cm<sup>2</sup> for three days to examine its sustainability under extreme hydrogen environments at ambient temperatures. The chemical composition of the starting powders contained a high amount of Ni, approximately 12.9 wt.%, as a strong austenite stabilizer. The tensile tests disclosed that hydrogen charging caused a minor reduction in the elongation to failure (approximately 3.5% on average) and ultimate tensile strength (UTS; approximately 2.1% on average) of the samples, using a low strain rate of 1.2 × 10<sup>−4</sup> s<sup>−1</sup>. It was also found that an increase in the strain rate from 1.2 × 10<sup>−4</sup> s<sup>−1</sup> to 4.8 × 10<sup>−4</sup> s<sup>−1</sup> led to a reduction of approximately 3.6% on average for the elongation to failure and 1.7% on average for UTS in the pre-charged samples. No trace of martensite was detected in the X-ray diffraction (XRD) analysis of the fractured samples thanks to the high Ni content, which caused a minor reduction in UTS × uniform elongation (UE) (GPa%) after the H charging. Considerable surface tearing was observed for the pre-charged sample after the tensile deformation. Additionally, some cracks were observed to be independent of the melt pool boundaries, indicating that such boundaries cannot necessarily act as a suitable area for the crack propagation.https://www.mdpi.com/2075-4701/11/4/586laser powder bed fusion (L-PBF)hydrogen embrittlement (HE)austenitic stainless steels (ASSs)tensile properties
spellingShingle Farzaneh Khaleghifar
Khashayar Razeghi
Akbar Heidarzadeh
Reza Taherzadeh Mousavian
Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed Fusion
Metals
laser powder bed fusion (L-PBF)
hydrogen embrittlement (HE)
austenitic stainless steels (ASSs)
tensile properties
title Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed Fusion
title_full Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed Fusion
title_fullStr Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed Fusion
title_full_unstemmed Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed Fusion
title_short Effect of Hydrogen on the Tensile Behavior of Austenitic Stainless Steels 316L Produced by Laser-Powder Bed Fusion
title_sort effect of hydrogen on the tensile behavior of austenitic stainless steels 316l produced by laser powder bed fusion
topic laser powder bed fusion (L-PBF)
hydrogen embrittlement (HE)
austenitic stainless steels (ASSs)
tensile properties
url https://www.mdpi.com/2075-4701/11/4/586
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