On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and Aging

A Cu-1Cr-0.1Zr alloy has been subjected to ECAP processing via route Bc and aging at 250-800°C. Electron BackScatter diffraction (EBSD), Transmission Electron Microscopy (TEM) and X-Ray Diffraction Line Profile Analysis (XRDLPA) techniques have been used to unveil some peculiarities of the grain and...

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Main Authors: K. Abib, B. Alili, T. Baudin, A.-L. Helbert, F. Brisset, L. Litynska-Dobrzynska, P. Zieba, D. Bradai
Format: Article
Language:English
Published: Polish Academy of Sciences 2024-04-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:https://journals.pan.pl/Content/130873/PDF/AMM-2024-1-02-Abib.pdf
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author K. Abib
B. Alili
T. Baudin
A.-L. Helbert
F. Brisset
L. Litynska-Dobrzynska
P. Zieba
D. Bradai
author_facet K. Abib
B. Alili
T. Baudin
A.-L. Helbert
F. Brisset
L. Litynska-Dobrzynska
P. Zieba
D. Bradai
author_sort K. Abib
collection DOAJ
description A Cu-1Cr-0.1Zr alloy has been subjected to ECAP processing via route Bc and aging at 250-800°C. Electron BackScatter diffraction (EBSD), Transmission Electron Microscopy (TEM) and X-Ray Diffraction Line Profile Analysis (XRDLPA) techniques have been used to unveil some peculiarities of the grain and subgrain structure with a special emphasis on the comparison of the grain size estimated by the three techniques. For the alloy ECAP processed and aged up to 16 passes, the grain size (from EBSD, 0.2 < d < 5 μm), subgrain size (from TEM, d ~ 0.75 μm) and “apparent” average crystallite size (from XRDLPA, d < 0.25 μm) are manifestly different. The results were compared to the published data and analyzed based on the fundamental aspects of these techniques.
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spelling doaj.art-c1db3096f5394e01b5a20de262dc68e22024-04-12T15:34:22ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092024-04-01vol. 69No 1916https://doi.org/10.24425/amm.2024.147776On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and AgingK. Abib0https://orcid.org/0000-0001-7651-3134B. Alili1https://orcid.org/0000-0001-8749-248XT. Baudin2https://orcid.org/0000-0002-6765-360XA.-L. Helbert3https://orcid.org/0000-0003-1679-9569F. Brisset4https://orcid.org/0000-0003-0952-2748L. Litynska-Dobrzynska5https://orcid.org/0000-0001-8786-3586P. Zieba6https://orcid.org/0000-0002-7696-3124D. Bradai7https://orcid.org/0000-0003-0213-2405University Of Sciences And Technology Houari Boumediene, Faculty Of Physics, Bp 32 El Alia, Bab Ezzouar, Algiers, AlgeriaUniversity Of Sciences And Technology Houari Boumediene, Faculty Of Physics, Bp 32 El Alia, Bab Ezzouar, Algiers, AlgeriaUniversity Paris-Saclay, Icmmo, 91405, Orsay, FranceUniversity Paris-Saclay, Icmmo, 91405, Orsay, FranceUniversity Paris-Saclay, Icmmo, 91405, Orsay, FranceInstitute Of Meta llurgy And Mat erials Science, Polish Academy Of Sciences, 25 Reymonta Str., 30-059 Krakow, PolandInstitute Of Meta llurgy And Mat erials Science, Polish Academy Of Sciences, 25 Reymonta Str., 30-059 Krakow, PolandUniversity Of Sciences And Technology Houari Boumediene, Faculty Of Physics, Bp 32 El Alia, Bab Ezzouar, Algiers, AlgeriaA Cu-1Cr-0.1Zr alloy has been subjected to ECAP processing via route Bc and aging at 250-800°C. Electron BackScatter diffraction (EBSD), Transmission Electron Microscopy (TEM) and X-Ray Diffraction Line Profile Analysis (XRDLPA) techniques have been used to unveil some peculiarities of the grain and subgrain structure with a special emphasis on the comparison of the grain size estimated by the three techniques. For the alloy ECAP processed and aged up to 16 passes, the grain size (from EBSD, 0.2 < d < 5 μm), subgrain size (from TEM, d ~ 0.75 μm) and “apparent” average crystallite size (from XRDLPA, d < 0.25 μm) are manifestly different. The results were compared to the published data and analyzed based on the fundamental aspects of these techniques.https://journals.pan.pl/Content/130873/PDF/AMM-2024-1-02-Abib.pdfcu-cr-zrecapebsdxrdlpatem
spellingShingle K. Abib
B. Alili
T. Baudin
A.-L. Helbert
F. Brisset
L. Litynska-Dobrzynska
P. Zieba
D. Bradai
On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and Aging
Archives of Metallurgy and Materials
cu-cr-zr
ecap
ebsd
xrdlpa
tem
title On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and Aging
title_full On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and Aging
title_fullStr On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and Aging
title_full_unstemmed On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and Aging
title_short On some Features of the Grain and Subgrain Size in a Cu-Cr-Zr Alloy After ECAP Processing and Aging
title_sort on some features of the grain and subgrain size in a cu cr zr alloy after ecap processing and aging
topic cu-cr-zr
ecap
ebsd
xrdlpa
tem
url https://journals.pan.pl/Content/130873/PDF/AMM-2024-1-02-Abib.pdf
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