Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious Systems

Capsule-based self-sealing in cementitious systems is an advantageous methodology which has the potential to decrease water ingress and thus enhance a system’s durability and extend its lifespan. If capsule-based self-sealing is to be considered as an industrial solution, production must be scaled w...

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Main Authors: Riordan Claire, Palmer Dave, Al-Tabbaa Abir
Format: Article
Language:English
Published: EDP Sciences 2023-01-01
Series:MATEC Web of Conferences
Online Access:https://www.matec-conferences.org/articles/matecconf/pdf/2023/05/matecconf_smartincs2023_02010.pdf
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author Riordan Claire
Palmer Dave
Al-Tabbaa Abir
author_facet Riordan Claire
Palmer Dave
Al-Tabbaa Abir
author_sort Riordan Claire
collection DOAJ
description Capsule-based self-sealing in cementitious systems is an advantageous methodology which has the potential to decrease water ingress and thus enhance a system’s durability and extend its lifespan. If capsule-based self-sealing is to be considered as an industrial solution, production must be scaled while capsule quality and batch reproducibility are maintained. In this study, polyurethane-shelled microcapsules containing a commercially available water repellent agent were produced using membrane emulsification equipment, supplied by Micropore Technologies, followed by interfacial polymerisation. Production was scaled across three different cross-flow membrane emulsification devices, the AXF-1, the AXF-3, and the AXF-4, increasing production output to a maximum of 850 L/hr of capsule suspension. Following production, capsules were characterised, measuring average size and size distribution, as well as integrated into a cementitious matrix. The results highlight the key parameters that govern capsule size, the versatility of the equipment, and the consistent quality of capsules produced. It is hoped that this scaled production of capsules will help to develop the commercial viability of capsule-based self-sealing cementitious systems.
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spelling doaj.art-c221695ea5474c81886213623c84cb952023-05-02T09:34:12ZengEDP SciencesMATEC Web of Conferences2261-236X2023-01-013780201010.1051/matecconf/202337802010matecconf_smartincs2023_02010Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious SystemsRiordan Claire0Palmer Dave1Al-Tabbaa Abir2Department of Engineering, University of CambridgeMicropore Technologies, Wilton CentreDepartment of Engineering, University of CambridgeCapsule-based self-sealing in cementitious systems is an advantageous methodology which has the potential to decrease water ingress and thus enhance a system’s durability and extend its lifespan. If capsule-based self-sealing is to be considered as an industrial solution, production must be scaled while capsule quality and batch reproducibility are maintained. In this study, polyurethane-shelled microcapsules containing a commercially available water repellent agent were produced using membrane emulsification equipment, supplied by Micropore Technologies, followed by interfacial polymerisation. Production was scaled across three different cross-flow membrane emulsification devices, the AXF-1, the AXF-3, and the AXF-4, increasing production output to a maximum of 850 L/hr of capsule suspension. Following production, capsules were characterised, measuring average size and size distribution, as well as integrated into a cementitious matrix. The results highlight the key parameters that govern capsule size, the versatility of the equipment, and the consistent quality of capsules produced. It is hoped that this scaled production of capsules will help to develop the commercial viability of capsule-based self-sealing cementitious systems.https://www.matec-conferences.org/articles/matecconf/pdf/2023/05/matecconf_smartincs2023_02010.pdf
spellingShingle Riordan Claire
Palmer Dave
Al-Tabbaa Abir
Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious Systems
MATEC Web of Conferences
title Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious Systems
title_full Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious Systems
title_fullStr Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious Systems
title_full_unstemmed Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious Systems
title_short Investigation of Membrane Emulsification for the Scaled Production of Microcapsules for Self-sealing Cementitious Systems
title_sort investigation of membrane emulsification for the scaled production of microcapsules for self sealing cementitious systems
url https://www.matec-conferences.org/articles/matecconf/pdf/2023/05/matecconf_smartincs2023_02010.pdf
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AT altabbaaabir investigationofmembraneemulsificationforthescaledproductionofmicrocapsulesforselfsealingcementitioussystems