Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetate
The title imidazo [4,5-b] pyridine derivative, C16H14BrN3O2, crystallizes with two independent molecules (1 and 2) in the asymmetric unit. In molecule 1, the pendant phenyl ring is inclined to the imidazo[4,5-b]pyridine core by 43.10 (4)° while in molecule 2 the corresponding angle is 49.43 (4)°. Th...
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| Format: | Article |
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International Union of Crystallography
2016-12-01
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| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314616019994 |
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| author | Mohammed Yassin Hjouji Joel T. Mague Youssef Kandri Rodi Younes Ouzidan El Mokhtar Essassi |
| author_facet | Mohammed Yassin Hjouji Joel T. Mague Youssef Kandri Rodi Younes Ouzidan El Mokhtar Essassi |
| author_sort | Mohammed Yassin Hjouji |
| collection | DOAJ |
| description | The title imidazo [4,5-b] pyridine derivative, C16H14BrN3O2, crystallizes with two independent molecules (1 and 2) in the asymmetric unit. In molecule 1, the pendant phenyl ring is inclined to the imidazo[4,5-b]pyridine core by 43.10 (4)° while in molecule 2 the corresponding angle is 49.43 (4)°. The two molecules differ primarily in the conformations of the ester substituents. In the crystal, molecules are linked via C—H...N and C—H...O hydrogen bonds, forming sheets parallel to the ab plane. |
| first_indexed | 2024-12-11T00:58:11Z |
| format | Article |
| id | doaj.art-c31f33f3847c4af88126a5ef661c074b |
| institution | Directory Open Access Journal |
| issn | 2414-3146 |
| language | English |
| last_indexed | 2024-12-11T00:58:11Z |
| publishDate | 2016-12-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | IUCrData |
| spelling | doaj.art-c31f33f3847c4af88126a5ef661c074b2022-12-22T01:26:25ZengInternational Union of CrystallographyIUCrData2414-31462016-12-01112x16199910.1107/S2414314616019994su4112Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetateMohammed Yassin Hjouji0Joel T. Mague1Youssef Kandri Rodi2Younes Ouzidan3El Mokhtar Essassi4Laboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoDepartment of Chemistry, Tulane University, New Orleans, LA 70118, USALaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Hétérocyclique URAC 21, Pôle de Compétence Pharmacochimie, Av. Ibn Battouta, BP 1014, Faculté des Sciences, Université Mohammed V, Rabat, MoroccoThe title imidazo [4,5-b] pyridine derivative, C16H14BrN3O2, crystallizes with two independent molecules (1 and 2) in the asymmetric unit. In molecule 1, the pendant phenyl ring is inclined to the imidazo[4,5-b]pyridine core by 43.10 (4)° while in molecule 2 the corresponding angle is 49.43 (4)°. The two molecules differ primarily in the conformations of the ester substituents. In the crystal, molecules are linked via C—H...N and C—H...O hydrogen bonds, forming sheets parallel to the ab plane.http://scripts.iucr.org/cgi-bin/paper?S2414314616019994crystal structureimidazo[4,5-b]pyridinehydrogen bonding |
| spellingShingle | Mohammed Yassin Hjouji Joel T. Mague Youssef Kandri Rodi Younes Ouzidan El Mokhtar Essassi Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetate IUCrData crystal structure imidazo[4,5-b]pyridine hydrogen bonding |
| title | Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetate |
| title_full | Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetate |
| title_fullStr | Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetate |
| title_full_unstemmed | Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetate |
| title_short | Ethyl 2-(6-bromo-2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)acetate |
| title_sort | ethyl 2 6 bromo 2 phenyl 3h imidazo 4 5 b pyridin 3 yl acetate |
| topic | crystal structure imidazo[4,5-b]pyridine hydrogen bonding |
| url | http://scripts.iucr.org/cgi-bin/paper?S2414314616019994 |
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