Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics
In the current work, we focused on the impact of Indium oxide partial substitution at the (Hg) site on the structural characteristics of the (HgBa2Ca2Cu2.85La0.15O8+δ) compound with (0,0.05,0.1,0.15,0.2 and 0.25). Samples were prepared by the (SSR) method. The combined powder was crushed with...
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| Format: | Article |
| Language: | English |
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University of Kufa
2023-06-01
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| Series: | Journal of Kufa-Physics |
| Subjects: | |
| Online Access: | https://www.journal.uokufa.edu.iq/index.php/jkp/article/view/10917 |
| _version_ | 1797651631358083072 |
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| author | EKHLAS HASSAN Haider M.J. Haider |
| author_facet | EKHLAS HASSAN Haider M.J. Haider |
| author_sort | EKHLAS HASSAN |
| collection | DOAJ |
| description |
In the current work, we focused on the impact of Indium oxide partial substitution at the (Hg) site on the structural characteristics of the (HgBa2Ca2Cu2.85La0.15O8+δ) compound with (0,0.05,0.1,0.15,0.2 and 0.25). Samples were prepared by the (SSR) method. The combined powder was crushed with a pressure of 7 tons per square centimeter to create a disc with a thickness of (0.2 cm) and a diameter of (1.5 cm). The samples sintered for 24 hours at a rate that was changed from ambient temperature to 820 °C. For the samples which were doped with (In=0.05) in comparison to other samples, the highest value of the c-axis lattice parameter and a pseudo-tetragonal structure were discovered using (XRD) analysis. It was discovered that altering the In concentrations in all of the results of our sample changes the volume fraction VPh(1223), mass density dm, and c/a. It was also determined that the change in lattice parameters, degree of crystallinity, crystal size, and strain (in different ways) resulted from a change in the indium oxide concentrations for all samples.
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| first_indexed | 2024-03-11T16:17:38Z |
| format | Article |
| id | doaj.art-c3717870705349daa8824a013637b837 |
| institution | Directory Open Access Journal |
| issn | 2077-5830 2312-6671 |
| language | English |
| last_indexed | 2024-03-11T16:17:38Z |
| publishDate | 2023-06-01 |
| publisher | University of Kufa |
| record_format | Article |
| series | Journal of Kufa-Physics |
| spelling | doaj.art-c3717870705349daa8824a013637b8372023-10-24T14:15:20ZengUniversity of KufaJournal of Kufa-Physics2077-58302312-66712023-06-01150110.31257/2018/JKP/2023/v15.i01.10917Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics EKHLAS HASSAN0Haider M.J. Haider1University of KufaUniversity of Kufa In the current work, we focused on the impact of Indium oxide partial substitution at the (Hg) site on the structural characteristics of the (HgBa2Ca2Cu2.85La0.15O8+δ) compound with (0,0.05,0.1,0.15,0.2 and 0.25). Samples were prepared by the (SSR) method. The combined powder was crushed with a pressure of 7 tons per square centimeter to create a disc with a thickness of (0.2 cm) and a diameter of (1.5 cm). The samples sintered for 24 hours at a rate that was changed from ambient temperature to 820 °C. For the samples which were doped with (In=0.05) in comparison to other samples, the highest value of the c-axis lattice parameter and a pseudo-tetragonal structure were discovered using (XRD) analysis. It was discovered that altering the In concentrations in all of the results of our sample changes the volume fraction VPh(1223), mass density dm, and c/a. It was also determined that the change in lattice parameters, degree of crystallinity, crystal size, and strain (in different ways) resulted from a change in the indium oxide concentrations for all samples. https://www.journal.uokufa.edu.iq/index.php/jkp/article/view/10917partial substitutionthe (SSR) method(XRD) analysisdegree of crystallinitycrystallite sizestrain |
| spellingShingle | EKHLAS HASSAN Haider M.J. Haider Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics Journal of Kufa-Physics partial substitution the (SSR) method (XRD) analysis degree of crystallinity crystallite size strain |
| title | Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics |
| title_full | Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics |
| title_fullStr | Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics |
| title_full_unstemmed | Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics |
| title_short | Preparation (HgBa2Ca2Cu2.85La0.15O8+δ) compound and Study of the impact of partial substitution of mercury with (In2O3)on the structural characteristics |
| title_sort | preparation hgba2ca2cu2 85la0 15o8 δ compound and study of the impact of partial substitution of mercury with in2o3 on the structural characteristics |
| topic | partial substitution the (SSR) method (XRD) analysis degree of crystallinity crystallite size strain |
| url | https://www.journal.uokufa.edu.iq/index.php/jkp/article/view/10917 |
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