Optimisation of ECX permeation barriers towards thicker alumina

The current development with respect to modifying the ECX (electrochemical X-deposition) process towards thicker alumina formed by heat treatment of aluminium electroplated on steel is described. As anticipated, changing the heat treatment atmosphere from argon to air or prolonging holding at high t...

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Bibliographic Details
Main Authors: Carsten Schroer, Julia Lorenz, Olaf Wedemeyer, Aleksandr Skrypnik, Kateryna Khanchych
Format: Article
Language:English
Published: Elsevier 2024-03-01
Series:Nuclear Materials and Energy
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2352179124000036
Description
Summary:The current development with respect to modifying the ECX (electrochemical X-deposition) process towards thicker alumina formed by heat treatment of aluminium electroplated on steel is described. As anticipated, changing the heat treatment atmosphere from argon to air or prolonging holding at high temperature (980 °C) increases the amount of alumina, but exposure to liquid lithium–lead eutectic reveals weak spots present in the alumina layers. The thickness of alumina produced is in the range of 1–2 µm for holding at 980 °C in air for 0.5–2 h.
ISSN:2352-1791