Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ions
This paper describes the synthesis of a new derivative 3-(1,3- benzothiazol-2-yl)- /4H- spiro[indole2,3-[1,3]thiazolidine]-2,/4(1H) dion [L], which have been obtained from the cyclization of 3-(benzo [d] thiazol-2- ylimino) indolin -2-one[AB] through the addition of á-mercapto acetic acid. The produ...
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| Format: | Article |
| Language: | English |
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Unviversity of Technology- Iraq
2011-11-01
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| Series: | Engineering and Technology Journal |
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| Online Access: | https://etj.uotechnology.edu.iq/article_33233_a01e8f6644c8311d987c840f93b36783.pdf |
| _version_ | 1827358373447729152 |
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| author | Rehab A.M. Al-Hasani Sinan M.M. Al-byatti Sarab M.S. Al Azawi |
| author_facet | Rehab A.M. Al-Hasani Sinan M.M. Al-byatti Sarab M.S. Al Azawi |
| author_sort | Rehab A.M. Al-Hasani |
| collection | DOAJ |
| description | This paper describes the synthesis of a new derivative 3-(1,3- benzothiazol-2-yl)- /4H- spiro[indole2,3-[1,3]thiazolidine]-2,/4(1H) dion [L], which have been obtained from the cyclization of 3-(benzo [d] thiazol-2- ylimino) indolin -2-one[AB] through the addition of á-mercapto acetic acid. The product [L] was characterized by (FT.IR) and (U.Vis) spectroscopy and in addition to element analysis (C.H.N.S.). A number of metal complexes were synthesized from the reaction of the ligand [L] with ions Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) . The prepared complexes were isolated and characterized by using (FT.IR) and (U.Vis) spectroscopy in addition to element analysis (C.H.N.S.), flame atomic absorption technique, in addition to magnetic susceptibility and conductivity measurement. The antibacterial activity of the ligand [L] and its complexes were studied against two selected micro-organisms (Pseudonomous aerugionosa) as gram negative and (Bacillus subtitis) as gram positive. |
| first_indexed | 2024-03-08T06:09:51Z |
| format | Article |
| id | doaj.art-c40a1148c71846128fd76339bf30631c |
| institution | Directory Open Access Journal |
| issn | 1681-6900 2412-0758 |
| language | English |
| last_indexed | 2024-03-08T06:09:51Z |
| publishDate | 2011-11-01 |
| publisher | Unviversity of Technology- Iraq |
| record_format | Article |
| series | Engineering and Technology Journal |
| spelling | doaj.art-c40a1148c71846128fd76339bf30631c2024-02-04T17:42:43ZengUnviversity of Technology- IraqEngineering and Technology Journal1681-69002412-07582011-11-0129153067307810.30684/etj.29.15.333233Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ionsRehab A.M. Al-HasaniSinan M.M. Al-byattiSarab M.S. Al AzawiThis paper describes the synthesis of a new derivative 3-(1,3- benzothiazol-2-yl)- /4H- spiro[indole2,3-[1,3]thiazolidine]-2,/4(1H) dion [L], which have been obtained from the cyclization of 3-(benzo [d] thiazol-2- ylimino) indolin -2-one[AB] through the addition of á-mercapto acetic acid. The product [L] was characterized by (FT.IR) and (U.Vis) spectroscopy and in addition to element analysis (C.H.N.S.). A number of metal complexes were synthesized from the reaction of the ligand [L] with ions Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) . The prepared complexes were isolated and characterized by using (FT.IR) and (U.Vis) spectroscopy in addition to element analysis (C.H.N.S.), flame atomic absorption technique, in addition to magnetic susceptibility and conductivity measurement. The antibacterial activity of the ligand [L] and its complexes were studied against two selected micro-organisms (Pseudonomous aerugionosa) as gram negative and (Bacillus subtitis) as gram positive.https://etj.uotechnology.edu.iq/article_33233_a01e8f6644c8311d987c840f93b36783.pdfthiazoliddioncomplexes of thiazolidin derivativesbiological studies |
| spellingShingle | Rehab A.M. Al-Hasani Sinan M.M. Al-byatti Sarab M.S. Al Azawi Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ions Engineering and Technology Journal thiazolid dion complexes of thiazolidin derivatives biological studies |
| title | Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ions |
| title_full | Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ions |
| title_fullStr | Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ions |
| title_full_unstemmed | Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ions |
| title_short | Synthesis, Structural and Biological Studies of /3-(1, 3- benzothiazol-2-yl) - /4H- spiro[indole2,3-[1,3]thiazolidine]- 2,/4(1H) dion with Cr (III), Mn (II), Co (II), Ni (II), Cu (II), and Zn (II) ions |
| title_sort | synthesis structural and biological studies of 3 1 3 benzothiazol 2 yl 4h spiro indole2 3 1 3 thiazolidine 2 4 1h dion with cr iii mn ii co ii ni ii cu ii and zn ii ions |
| topic | thiazolid dion complexes of thiazolidin derivatives biological studies |
| url | https://etj.uotechnology.edu.iq/article_33233_a01e8f6644c8311d987c840f93b36783.pdf |
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