2,4-Dichloro-N-(4-methylphenyl)benzenesulfonamide
The title compound, C13H11Cl2NO2S, crystallizes with four independent molecules in the asymmetric unit. In each of the four molecules, the conformation of the N—C bond in the C—SO2—NH—C segment is gauche with respect to both S=O bonds. The mole...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2010-01-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536809053707 |
| _version_ | 1819104991411961856 |
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| author | B. Thimme Gowda Sabine Foro P. G. Nirmala Hartmut Fuess |
| author_facet | B. Thimme Gowda Sabine Foro P. G. Nirmala Hartmut Fuess |
| author_sort | B. Thimme Gowda |
| collection | DOAJ |
| description | The title compound, C13H11Cl2NO2S, crystallizes with four independent molecules in the asymmetric unit. In each of the four molecules, the conformation of the N—C bond in the C—SO2—NH—C segment is gauche with respect to both S=O bonds. The molecules are twisted at the S—N bonds with C—SO2—NH—C torsion angles of 60.6 (4), −59.7 (3), 63.9 (4) and 53.0 (4)°. The benzene rings in two of the molecules are disordered with multiple positions resolved in each case. The crystal structure features inversion dimers linked by pairs of N—H...O hydrogen bonds for each of the four molecules. |
| first_indexed | 2024-12-22T02:15:09Z |
| format | Article |
| id | doaj.art-c4520273cf7b4b65bb8cf31c3d45abf2 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-22T02:15:09Z |
| publishDate | 2010-01-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-c4520273cf7b4b65bb8cf31c3d45abf22022-12-21T18:42:18ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-01-01661o190o19010.1107/S16005368090537072,4-Dichloro-N-(4-methylphenyl)benzenesulfonamideB. Thimme GowdaSabine ForoP. G. NirmalaHartmut FuessThe title compound, C13H11Cl2NO2S, crystallizes with four independent molecules in the asymmetric unit. In each of the four molecules, the conformation of the N—C bond in the C—SO2—NH—C segment is gauche with respect to both S=O bonds. The molecules are twisted at the S—N bonds with C—SO2—NH—C torsion angles of 60.6 (4), −59.7 (3), 63.9 (4) and 53.0 (4)°. The benzene rings in two of the molecules are disordered with multiple positions resolved in each case. The crystal structure features inversion dimers linked by pairs of N—H...O hydrogen bonds for each of the four molecules.http://scripts.iucr.org/cgi-bin/paper?S1600536809053707 |
| spellingShingle | B. Thimme Gowda Sabine Foro P. G. Nirmala Hartmut Fuess 2,4-Dichloro-N-(4-methylphenyl)benzenesulfonamide Acta Crystallographica Section E |
| title | 2,4-Dichloro-N-(4-methylphenyl)benzenesulfonamide |
| title_full | 2,4-Dichloro-N-(4-methylphenyl)benzenesulfonamide |
| title_fullStr | 2,4-Dichloro-N-(4-methylphenyl)benzenesulfonamide |
| title_full_unstemmed | 2,4-Dichloro-N-(4-methylphenyl)benzenesulfonamide |
| title_short | 2,4-Dichloro-N-(4-methylphenyl)benzenesulfonamide |
| title_sort | 2 4 dichloro n 4 methylphenyl benzenesulfonamide |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536809053707 |
| work_keys_str_mv | AT bthimmegowda 24dichloron4methylphenylbenzenesulfonamide AT sabineforo 24dichloron4methylphenylbenzenesulfonamide AT pgnirmala 24dichloron4methylphenylbenzenesulfonamide AT hartmutfuess 24dichloron4methylphenylbenzenesulfonamide |