Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste Electrode
In the presented work, the properties of carbon materials obtained in the reaction of sodium bicarbonate (C-SB) and ammonium oxalate (C-AO) with magnesium by combustion synthesis were investigated. For the materials obtained in this way, the influence of the type of precursor on their properties was...
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MDPI AG
2021-05-01
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| Series: | Materials |
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| Online Access: | https://www.mdpi.com/1996-1944/14/10/2480 |
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| author | Katarzyna Skrzypczyńska Andrzej Świątkowski Ryszard Diduszko Lidia Dąbek |
| author_facet | Katarzyna Skrzypczyńska Andrzej Świątkowski Ryszard Diduszko Lidia Dąbek |
| author_sort | Katarzyna Skrzypczyńska |
| collection | DOAJ |
| description | In the presented work, the properties of carbon materials obtained in the reaction of sodium bicarbonate (C-SB) and ammonium oxalate (C-AO) with magnesium by combustion synthesis were investigated. For the materials obtained in this way, the influence of the type of precursor on their properties was analyzed, including: Degree of crystallinity, porous structure, surface topography, and electrochemical properties. It has been shown that the products obtained in magnesiothermic process were found to contain largely the turbostratic carbon forming a petal-like graphene material. Both materials were used as modifiers of carbon paste electrodes, which were then used to determine the concentration of chlorophenol solutions by voltammetric method. It was shown that the peak current determined from the registered differential pulse voltammograms was mainly influenced by the volume of mesopores and the adsorption capacity of 4-chlorophenol for both obtained carbons. |
| first_indexed | 2024-03-10T11:32:05Z |
| format | Article |
| id | doaj.art-c45eab201a3646a5b539d06ad0f038d1 |
| institution | Directory Open Access Journal |
| issn | 1996-1944 |
| language | English |
| last_indexed | 2024-03-10T11:32:05Z |
| publishDate | 2021-05-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Materials |
| spelling | doaj.art-c45eab201a3646a5b539d06ad0f038d12023-11-21T19:09:58ZengMDPI AGMaterials1996-19442021-05-011410248010.3390/ma14102480Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste ElectrodeKatarzyna Skrzypczyńska0Andrzej Świątkowski1Ryszard Diduszko2Lidia Dąbek3Łukasiewicz Research Network—Industrial Chemistry Institute, 01-793 Warsaw, PolandInstitute of Chemistry, Military University of Technology, 00-908 Warsaw, PolandŁukasiewicz Research Network—Institute of Microelectronics and Photonics, 01-919 Warsaw, PolandFaculty of Environmental, Geomatic and Energy Engineering, Kielce University of Technology, 25-314 Kielce, PolandIn the presented work, the properties of carbon materials obtained in the reaction of sodium bicarbonate (C-SB) and ammonium oxalate (C-AO) with magnesium by combustion synthesis were investigated. For the materials obtained in this way, the influence of the type of precursor on their properties was analyzed, including: Degree of crystallinity, porous structure, surface topography, and electrochemical properties. It has been shown that the products obtained in magnesiothermic process were found to contain largely the turbostratic carbon forming a petal-like graphene material. Both materials were used as modifiers of carbon paste electrodes, which were then used to determine the concentration of chlorophenol solutions by voltammetric method. It was shown that the peak current determined from the registered differential pulse voltammograms was mainly influenced by the volume of mesopores and the adsorption capacity of 4-chlorophenol for both obtained carbons.https://www.mdpi.com/1996-1944/14/10/2480combustion synthesissalts with carbon in moleculecarbon materialsmodified CPEs |
| spellingShingle | Katarzyna Skrzypczyńska Andrzej Świątkowski Ryszard Diduszko Lidia Dąbek Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste Electrode Materials combustion synthesis salts with carbon in molecule carbon materials modified CPEs |
| title | Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste Electrode |
| title_full | Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste Electrode |
| title_fullStr | Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste Electrode |
| title_full_unstemmed | Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste Electrode |
| title_short | Studies on Carbon Materials Produced from Salts with Anions Containing Carbon Atoms for Carbon Paste Electrode |
| title_sort | studies on carbon materials produced from salts with anions containing carbon atoms for carbon paste electrode |
| topic | combustion synthesis salts with carbon in molecule carbon materials modified CPEs |
| url | https://www.mdpi.com/1996-1944/14/10/2480 |
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