N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazide
A novel synthetic methodology for preparation of thiocarbohydrazone by reacting thiocarbohydrazide with 1-acetyl-5-chloroisatin is described. The title compound was prepared by condensation of thiocarbohydrazide and substituted isatin in aqueous ethanol. The newly synthesized compound was characteri...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
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MDPI AG
2013-04-01
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| Series: | Molbank |
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| Online Access: | http://www.mdpi.com/1422-8599/2013/2/M798 |
| _version_ | 1818485951137054720 |
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| author | Marina Stefova Frosa Anastasova Nataša Ristovska |
| author_facet | Marina Stefova Frosa Anastasova Nataša Ristovska |
| author_sort | Marina Stefova |
| collection | DOAJ |
| description | A novel synthetic methodology for preparation of thiocarbohydrazone by reacting thiocarbohydrazide with 1-acetyl-5-chloroisatin is described. The title compound was prepared by condensation of thiocarbohydrazide and substituted isatin in aqueous ethanol. The newly synthesized compound was characterized using 1H-NMR, 13C-NMR, FT-IR and mass spectrometry. |
| first_indexed | 2024-12-10T16:16:22Z |
| format | Article |
| id | doaj.art-c53a1eb1ebef49a4a899c176b06154a7 |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-12-10T16:16:22Z |
| publishDate | 2013-04-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-c53a1eb1ebef49a4a899c176b06154a72022-12-22T01:41:57ZengMDPI AGMolbank1422-85992013-04-0120132M79810.3390/M798N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazideMarina StefovaFrosa AnastasovaNataša RistovskaA novel synthetic methodology for preparation of thiocarbohydrazone by reacting thiocarbohydrazide with 1-acetyl-5-chloroisatin is described. The title compound was prepared by condensation of thiocarbohydrazide and substituted isatin in aqueous ethanol. The newly synthesized compound was characterized using 1H-NMR, 13C-NMR, FT-IR and mass spectrometry.http://www.mdpi.com/1422-8599/2013/2/M798chloroisatinthiocarbohydrazidecarbonyl-amine condensation |
| spellingShingle | Marina Stefova Frosa Anastasova Nataša Ristovska N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazide Molbank chloroisatin thiocarbohydrazide carbonyl-amine condensation |
| title | N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazide |
| title_full | N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazide |
| title_fullStr | N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazide |
| title_full_unstemmed | N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazide |
| title_short | N"-[(3Z)-1-Acetyl-5-chloro-2-oxo-1,2-dihydro-3H-indol-3-ylidene]thiocarbonohydrazide |
| title_sort | n 3z 1 acetyl 5 chloro 2 oxo 1 2 dihydro 3h indol 3 ylidene thiocarbonohydrazide |
| topic | chloroisatin thiocarbohydrazide carbonyl-amine condensation |
| url | http://www.mdpi.com/1422-8599/2013/2/M798 |
| work_keys_str_mv | AT marinastefova n3z1acetyl5chloro2oxo12dihydro3hindol3ylidenethiocarbonohydrazide AT frosaanastasova n3z1acetyl5chloro2oxo12dihydro3hindol3ylidenethiocarbonohydrazide AT natasaristovska n3z1acetyl5chloro2oxo12dihydro3hindol3ylidenethiocarbonohydrazide |