Wet Relaxation of Electrospun Nanofiber Mats

Electrospinning can be used to produce nanofiber mats. One of the often used polymers for electrospinning is polyacrylonitrile (PAN), especially for the production of carbon nanofibers, but also for a diverse number of other applications. For some of these applications—e.g., creation of na...

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Main Authors: Timo Grothe, Lilia Sabantina, Michaela Klöcker, Irén Juhász Junger, Christoph Döpke, Andrea Ehrmann
Format: Article
Language:English
Published: MDPI AG 2019-02-01
Series:Technologies
Subjects:
Online Access:https://www.mdpi.com/2227-7080/7/1/23
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author Timo Grothe
Lilia Sabantina
Michaela Klöcker
Irén Juhász Junger
Christoph Döpke
Andrea Ehrmann
author_facet Timo Grothe
Lilia Sabantina
Michaela Klöcker
Irén Juhász Junger
Christoph Döpke
Andrea Ehrmann
author_sort Timo Grothe
collection DOAJ
description Electrospinning can be used to produce nanofiber mats. One of the often used polymers for electrospinning is polyacrylonitrile (PAN), especially for the production of carbon nanofibers, but also for a diverse number of other applications. For some of these applications—e.g., creation of nano-filters—the dimensional stability of the nanofiber mats is crucial. While relaxation processes—especially dry, wet and washing relaxation—are well-known and often investigated for knitted fabrics, the dimensional stability of nanofiber mats has not yet been investigated. Here we report on the wet relaxation of PAN nanofiber mats, which are dependent on spinning and solution parameters such as: voltage, electrode distance, nanofiber mat thickness, and solid content in the solution. Our results show that wet relaxation has a significant effect on the samples, resulting in a dimensional change that has to be taken into account for nanofiber mats in wet applications. While the first and second soaking in pure water resulted in an increase of the nanofiber mat area up to approximately 5%, the dried sample, after the second soaking, conversely showed an area reduced by a maximum of 5%. For soaking in soap water, small areal decreases between approximately 1⁻4% were measured.
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spelling doaj.art-c5f973962ae94453896da70a286cc0bd2022-12-21T22:27:51ZengMDPI AGTechnologies2227-70802019-02-01712310.3390/technologies7010023technologies7010023Wet Relaxation of Electrospun Nanofiber MatsTimo Grothe0Lilia Sabantina1Michaela Klöcker2Irén Juhász Junger3Christoph Döpke4Andrea Ehrmann5Faculty of Engineering and Mathematics, ITES, Bielefeld University of Applied Sciences, 33619 Bielefeld, GermanyFaculty of Engineering and Mathematics, ITES, Bielefeld University of Applied Sciences, 33619 Bielefeld, GermanyFaculty of Engineering and Mathematics, ITES, Bielefeld University of Applied Sciences, 33619 Bielefeld, GermanyFaculty of Engineering and Mathematics, ITES, Bielefeld University of Applied Sciences, 33619 Bielefeld, GermanyFaculty of Engineering and Mathematics, ITES, Bielefeld University of Applied Sciences, 33619 Bielefeld, GermanyFaculty of Engineering and Mathematics, ITES, Bielefeld University of Applied Sciences, 33619 Bielefeld, GermanyElectrospinning can be used to produce nanofiber mats. One of the often used polymers for electrospinning is polyacrylonitrile (PAN), especially for the production of carbon nanofibers, but also for a diverse number of other applications. For some of these applications—e.g., creation of nano-filters—the dimensional stability of the nanofiber mats is crucial. While relaxation processes—especially dry, wet and washing relaxation—are well-known and often investigated for knitted fabrics, the dimensional stability of nanofiber mats has not yet been investigated. Here we report on the wet relaxation of PAN nanofiber mats, which are dependent on spinning and solution parameters such as: voltage, electrode distance, nanofiber mat thickness, and solid content in the solution. Our results show that wet relaxation has a significant effect on the samples, resulting in a dimensional change that has to be taken into account for nanofiber mats in wet applications. While the first and second soaking in pure water resulted in an increase of the nanofiber mat area up to approximately 5%, the dried sample, after the second soaking, conversely showed an area reduced by a maximum of 5%. For soaking in soap water, small areal decreases between approximately 1⁻4% were measured.https://www.mdpi.com/2227-7080/7/1/23electrospinningfilterwet relaxationdimensionspolyacrylonitrile (PAN)
spellingShingle Timo Grothe
Lilia Sabantina
Michaela Klöcker
Irén Juhász Junger
Christoph Döpke
Andrea Ehrmann
Wet Relaxation of Electrospun Nanofiber Mats
Technologies
electrospinning
filter
wet relaxation
dimensions
polyacrylonitrile (PAN)
title Wet Relaxation of Electrospun Nanofiber Mats
title_full Wet Relaxation of Electrospun Nanofiber Mats
title_fullStr Wet Relaxation of Electrospun Nanofiber Mats
title_full_unstemmed Wet Relaxation of Electrospun Nanofiber Mats
title_short Wet Relaxation of Electrospun Nanofiber Mats
title_sort wet relaxation of electrospun nanofiber mats
topic electrospinning
filter
wet relaxation
dimensions
polyacrylonitrile (PAN)
url https://www.mdpi.com/2227-7080/7/1/23
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