Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>

This paper introduces a new spark plasma sintering technique that is able to order crystalline anisotropy by in-series/in situ DC electric coupled magnetic field. The process control parameters have been investigated on the production of anisotropic BaFe<sub>12</sub>O<sub>19</su...

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Main Authors: Haetham G. Mohammed, Thar Mohammed Badri Albarody, Susilawati Susilawati, Soheil Gohari, Aris Doyan, Saiful Prayogi, Muhammad Roil Bilad, Reza Alebrahim, Anwar Ameen Hezam Saeed
Format: Article
Language:English
Published: MDPI AG 2021-05-01
Series:Materials
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Online Access:https://www.mdpi.com/1996-1944/14/10/2650
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author Haetham G. Mohammed
Thar Mohammed Badri Albarody
Susilawati Susilawati
Soheil Gohari
Aris Doyan
Saiful Prayogi
Muhammad Roil Bilad
Reza Alebrahim
Anwar Ameen Hezam Saeed
author_facet Haetham G. Mohammed
Thar Mohammed Badri Albarody
Susilawati Susilawati
Soheil Gohari
Aris Doyan
Saiful Prayogi
Muhammad Roil Bilad
Reza Alebrahim
Anwar Ameen Hezam Saeed
author_sort Haetham G. Mohammed
collection DOAJ
description This paper introduces a new spark plasma sintering technique that is able to order crystalline anisotropy by in-series/in situ DC electric coupled magnetic field. The process control parameters have been investigated on the production of anisotropic BaFe<sub>12</sub>O<sub>19</sub> magnets based on resulted remanence (Mr). Sintering holding time (H.T.), cooling rate (C.R.), pressure (P), and sintering temperature (S.T.) are optimized by Taguchi with L9 orthogonal array (OA). The remanent magnetization of nanocrystalline BaFe<sub>12</sub>O<sub>19</sub> in parallel (Mr<sup>ǁ</sup>) and perpendicular (Mr<sup>Ʇ</sup>) to the applied magnetic field was regarded as a measure of performance. The Taguchi study calculated optimum process parameters, which significantly improved the sintering process based on the confirmation tests of BaFe<sub>12</sub>O<sub>19</sub> anisotropy. The magnetic properties in terms of Mr<sup>ǁ</sup> and Mr<sup>Ʇ</sup> were greatly affected by sintering temperature and pressure according to ANOVA results. In addition, regression models were developed for predicting the Mr<sup>ǁ</sup> as well as Mr<sup>Ʇ</sup> respectively.
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spelling doaj.art-c6b7716c65c74f52a084895fc8aa20c52023-11-21T20:19:35ZengMDPI AGMaterials1996-19442021-05-011410265010.3390/ma14102650Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>Haetham G. Mohammed0Thar Mohammed Badri Albarody1Susilawati Susilawati2Soheil Gohari3Aris Doyan4Saiful Prayogi5Muhammad Roil Bilad6Reza Alebrahim7Anwar Ameen Hezam Saeed8Department of Mechanical Engineering, Universiti Teknologi Petronas, Seri Iskandar 32610, MalaysiaDepartment of Mechanical Engineering, Universiti Teknologi Petronas, Seri Iskandar 32610, MalaysiaMaster of Science Education Program, University of Mataram, Mataram 83125, IndonesiaDepartment of Mechanical Engineering, The University of Melbourne, Parkville, VIC 3010, AustraliaMaster of Science Education Program, University of Mataram, Mataram 83125, IndonesiaFaculty of Applied Science and Enginering, Universitas Pendidikan Mandalika, Mataram 83126, IndonesiaFaculty of Applied Science and Enginering, Universitas Pendidikan Mandalika, Mataram 83126, IndonesiaIndustrial Engineering Department, University of Padova, 35131 Padova, ItalyDepartment of Chemical Engineering, Universiti Teknologi Petronas, Seri Iskandar 32610, MalaysiaThis paper introduces a new spark plasma sintering technique that is able to order crystalline anisotropy by in-series/in situ DC electric coupled magnetic field. The process control parameters have been investigated on the production of anisotropic BaFe<sub>12</sub>O<sub>19</sub> magnets based on resulted remanence (Mr). Sintering holding time (H.T.), cooling rate (C.R.), pressure (P), and sintering temperature (S.T.) are optimized by Taguchi with L9 orthogonal array (OA). The remanent magnetization of nanocrystalline BaFe<sub>12</sub>O<sub>19</sub> in parallel (Mr<sup>ǁ</sup>) and perpendicular (Mr<sup>Ʇ</sup>) to the applied magnetic field was regarded as a measure of performance. The Taguchi study calculated optimum process parameters, which significantly improved the sintering process based on the confirmation tests of BaFe<sub>12</sub>O<sub>19</sub> anisotropy. The magnetic properties in terms of Mr<sup>ǁ</sup> and Mr<sup>Ʇ</sup> were greatly affected by sintering temperature and pressure according to ANOVA results. In addition, regression models were developed for predicting the Mr<sup>ǁ</sup> as well as Mr<sup>Ʇ</sup> respectively.https://www.mdpi.com/1996-1944/14/10/2650spark plasma sinteringsintering parametersremanenceoptimizationmagnetmagnetic properties
spellingShingle Haetham G. Mohammed
Thar Mohammed Badri Albarody
Susilawati Susilawati
Soheil Gohari
Aris Doyan
Saiful Prayogi
Muhammad Roil Bilad
Reza Alebrahim
Anwar Ameen Hezam Saeed
Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>
Materials
spark plasma sintering
sintering parameters
remanence
optimization
magnet
magnetic properties
title Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>
title_full Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>
title_fullStr Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>
title_full_unstemmed Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>
title_short Process Optimization of In Situ Magnetic-Anisotropy Spark Plasma Sintering of M-Type-Based Barium Hexaferrite BaFe<sub>12</sub>O<sub>19</sub>
title_sort process optimization of in situ magnetic anisotropy spark plasma sintering of m type based barium hexaferrite bafe sub 12 sub o sub 19 sub
topic spark plasma sintering
sintering parameters
remanence
optimization
magnet
magnetic properties
url https://www.mdpi.com/1996-1944/14/10/2650
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