Electrolytic Synthesis and Characterization of Silver Nanopowder

This work reports a simple, novel, cost effective and eco-friendly electrolytic synthesis of silver nanoparticles using AgNO3 as metal precursor. The synthesis rate is much faster than other methods and this approach is suitable for large scale production. They are characterized by XRD, SEM and FT-I...

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Main Authors: T. Theivasanthi, M. Alagar
Format: Article
Language:English
Published: Tsinghua University Press 2012-06-01
Series:Nano Biomedicine and Engineering
Subjects:
Online Access:https://www.sciopen.com/article/10.5101/nbe.v4i2.p58-65
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author T. Theivasanthi
M. Alagar
author_facet T. Theivasanthi
M. Alagar
author_sort T. Theivasanthi
collection DOAJ
description This work reports a simple, novel, cost effective and eco-friendly electrolytic synthesis of silver nanoparticles using AgNO3 as metal precursor. The synthesis rate is much faster than other methods and this approach is suitable for large scale production. They are characterized by XRD, SEM and FT-IR techniques to analyze size, morphology and functional groups. XRD studies reveal a high degree of crystallinity and monophasic Ag nanoparticles. Their particle size is found to be 24 nm and specific surface area (SSA) is 24 m2 g-1. Analysis of Ag nanoparticles SSA reports that increasing their SSA improves their antibacterial actions. Microbiology assay founds that Ag nanoparticles are effective against E.coli and B.megaterium bacteria. SSA of bacteria analysis reveals that it plays a major role while reacting with antimicrobial agents.
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spelling doaj.art-c715989a28de46e2a10659c5e32991962023-09-26T10:12:41ZengTsinghua University PressNano Biomedicine and Engineering2150-55782012-06-0142586510.5101/nbe.v4i2.p58-65Electrolytic Synthesis and Characterization of Silver NanopowderT. Theivasanthi0M. Alagar1Centre for Research and Post Graduate Department of Physics, Ayya Nadar Janaki Ammal College, Sivakasi-626124, Tamilnadu, IndiaCentre for Research and Post Graduate Department of Physics, Ayya Nadar Janaki Ammal College, Sivakasi-626124, Tamilnadu, IndiaThis work reports a simple, novel, cost effective and eco-friendly electrolytic synthesis of silver nanoparticles using AgNO3 as metal precursor. The synthesis rate is much faster than other methods and this approach is suitable for large scale production. They are characterized by XRD, SEM and FT-IR techniques to analyze size, morphology and functional groups. XRD studies reveal a high degree of crystallinity and monophasic Ag nanoparticles. Their particle size is found to be 24 nm and specific surface area (SSA) is 24 m2 g-1. Analysis of Ag nanoparticles SSA reports that increasing their SSA improves their antibacterial actions. Microbiology assay founds that Ag nanoparticles are effective against E.coli and B.megaterium bacteria. SSA of bacteria analysis reveals that it plays a major role while reacting with antimicrobial agents.https://www.sciopen.com/article/10.5101/nbe.v4i2.p58-65xrdsilver nanopowderwilliamson hall plotelectrolysisdebye-scherrer
spellingShingle T. Theivasanthi
M. Alagar
Electrolytic Synthesis and Characterization of Silver Nanopowder
Nano Biomedicine and Engineering
xrd
silver nanopowder
williamson hall plot
electrolysis
debye-scherrer
title Electrolytic Synthesis and Characterization of Silver Nanopowder
title_full Electrolytic Synthesis and Characterization of Silver Nanopowder
title_fullStr Electrolytic Synthesis and Characterization of Silver Nanopowder
title_full_unstemmed Electrolytic Synthesis and Characterization of Silver Nanopowder
title_short Electrolytic Synthesis and Characterization of Silver Nanopowder
title_sort electrolytic synthesis and characterization of silver nanopowder
topic xrd
silver nanopowder
williamson hall plot
electrolysis
debye-scherrer
url https://www.sciopen.com/article/10.5101/nbe.v4i2.p58-65
work_keys_str_mv AT ttheivasanthi electrolyticsynthesisandcharacterizationofsilvernanopowder
AT malagar electrolyticsynthesisandcharacterizationofsilvernanopowder