Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods
The aim of this work was to produce a thin SnO2 film by a technique combining the sol-gel method and electrospinning from a solution based on polyvinylpyrrolidone and a tin chloride pentahydrate as a precursor. The spinning solution was subjected to an electrospinning process, and then the obtained...
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Format: | Article |
Language: | English |
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Polish Academy of Sciences
2020-05-01
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Series: | Archives of Metallurgy and Materials |
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Online Access: | https://journals.pan.pl/Content/116054/PDF/AMM-2020-2-31-Matysiak.pdf |
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author | W. Matysiak T. Tański W. Smok S. Polishchuk |
author_facet | W. Matysiak T. Tański W. Smok S. Polishchuk |
author_sort | W. Matysiak |
collection | DOAJ |
description | The aim of this work was to produce a thin SnO2 film by a technique combining the sol-gel method and electrospinning from a solution based on polyvinylpyrrolidone and a tin chloride pentahydrate as a precursor. The spinning solution was subjected to an electrospinning process, and then the obtained nanofiber mats were calcined for 10 h at 500°C. Then, the scanning electron microscopy morphology analysis and chemical composition analysis by X-ray microanalysis of the manufactured thin film was performed. It was shown that an amorphous-crystalline layer formed by the SnO2 nanofiber network was obtained. Based on the UV-Vis spectrum, the width of the energy gap of the obtained layer was determined. |
first_indexed | 2024-04-13T11:20:17Z |
format | Article |
id | doaj.art-c76c5d070e444d929b4529c7e61443b1 |
institution | Directory Open Access Journal |
issn | 2300-1909 |
language | English |
last_indexed | 2024-04-13T11:20:17Z |
publishDate | 2020-05-01 |
publisher | Polish Academy of Sciences |
record_format | Article |
series | Archives of Metallurgy and Materials |
spelling | doaj.art-c76c5d070e444d929b4529c7e61443b12022-12-22T02:48:51ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092020-05-01vol. 65No 2761765https://doi.org/10.24425/amm.2020.132817Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning MethodsW. MatysiakT. TańskiW. SmokS. PolishchukThe aim of this work was to produce a thin SnO2 film by a technique combining the sol-gel method and electrospinning from a solution based on polyvinylpyrrolidone and a tin chloride pentahydrate as a precursor. The spinning solution was subjected to an electrospinning process, and then the obtained nanofiber mats were calcined for 10 h at 500°C. Then, the scanning electron microscopy morphology analysis and chemical composition analysis by X-ray microanalysis of the manufactured thin film was performed. It was shown that an amorphous-crystalline layer formed by the SnO2 nanofiber network was obtained. Based on the UV-Vis spectrum, the width of the energy gap of the obtained layer was determined.https://journals.pan.pl/Content/116054/PDF/AMM-2020-2-31-Matysiak.pdfthin filmsnanofiberstin oxideelectrospinningoptical properties |
spellingShingle | W. Matysiak T. Tański W. Smok S. Polishchuk Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods Archives of Metallurgy and Materials thin films nanofibers tin oxide electrospinning optical properties |
title | Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods |
title_full | Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods |
title_fullStr | Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods |
title_full_unstemmed | Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods |
title_short | Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods |
title_sort | thin sno2 films manufactured via the sol gel and electrospinning methods |
topic | thin films nanofibers tin oxide electrospinning optical properties |
url | https://journals.pan.pl/Content/116054/PDF/AMM-2020-2-31-Matysiak.pdf |
work_keys_str_mv | AT wmatysiak thinsno2filmsmanufacturedviathesolgelandelectrospinningmethods AT ttanski thinsno2filmsmanufacturedviathesolgelandelectrospinningmethods AT wsmok thinsno2filmsmanufacturedviathesolgelandelectrospinningmethods AT spolishchuk thinsno2filmsmanufacturedviathesolgelandelectrospinningmethods |