Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and Chemometrics

Parmigiano Reggiano is an Italian product with a protected designation of origin (P.D.O.). It is an aged hard cheese made from raw milk. P.D.O. products are protected by European regulations. Approximately 3 million wheels are produced each year, and the product attracts a relevant premium price due...

Full description

Bibliographic Details
Main Authors: Bert Popping, Emiliano De Dominicis, Mario Dante, Marco Nocetti
Format: Article
Language:English
Published: MDPI AG 2017-02-01
Series:Foods
Subjects:
Online Access:http://www.mdpi.com/2304-8158/6/2/13
_version_ 1818319170647883776
author Bert Popping
Emiliano De Dominicis
Mario Dante
Marco Nocetti
author_facet Bert Popping
Emiliano De Dominicis
Mario Dante
Marco Nocetti
author_sort Bert Popping
collection DOAJ
description Parmigiano Reggiano is an Italian product with a protected designation of origin (P.D.O.). It is an aged hard cheese made from raw milk. P.D.O. products are protected by European regulations. Approximately 3 million wheels are produced each year, and the product attracts a relevant premium price due to its quality and all around the world well known typicity. Due to the high demand that exceeds the production, several fraudulent products can be found on the market. The rate of fraud is estimated between 20% and 40%, the latter predominantly in the grated form. We have developed a non-target method based on Liquid Chomatography-High Resolution Mass Spectrometry (LC-HRMS) that allows the discrimination of Parmigiano Reggiano from non-authentic products with milk from different geographical origins or products, where other aspects of the production process do not comply with the rules laid down in the production specifications for Parmeggiano Reggiano. Based on a database created with authentic samples provided by the Consortium of Parmigiano Reggiano Cheese, a reliable classification model was built. The overall classification capabilities of this non-targeted method was verified on 32 grated cheese samples. The classification was 87.5% accurate.
first_indexed 2024-12-13T10:04:52Z
format Article
id doaj.art-c79b67ac8e4a4d838729ad474453cea6
institution Directory Open Access Journal
issn 2304-8158
language English
last_indexed 2024-12-13T10:04:52Z
publishDate 2017-02-01
publisher MDPI AG
record_format Article
series Foods
spelling doaj.art-c79b67ac8e4a4d838729ad474453cea62022-12-21T23:51:33ZengMDPI AGFoods2304-81582017-02-01621310.3390/foods6020013foods6020013Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and ChemometricsBert Popping0Emiliano De Dominicis1Mario Dante2Marco Nocetti3Food Consulting Services, 2 Chemin des Mouilles, 69290 Grezieu la Varenne, FranceR&D Department, Italy Mérieux NutriSciences, via Fratta 25, 31023 Resana, ItalyR&D Department, Italy Mérieux NutriSciences, via Fratta 25, 31023 Resana, ItalyR&D Department, Parmigiano Reggiano Cheese Consortium, Via J. F. Kennedy 18, 42124 Reggio Emilia, ItalyParmigiano Reggiano is an Italian product with a protected designation of origin (P.D.O.). It is an aged hard cheese made from raw milk. P.D.O. products are protected by European regulations. Approximately 3 million wheels are produced each year, and the product attracts a relevant premium price due to its quality and all around the world well known typicity. Due to the high demand that exceeds the production, several fraudulent products can be found on the market. The rate of fraud is estimated between 20% and 40%, the latter predominantly in the grated form. We have developed a non-target method based on Liquid Chomatography-High Resolution Mass Spectrometry (LC-HRMS) that allows the discrimination of Parmigiano Reggiano from non-authentic products with milk from different geographical origins or products, where other aspects of the production process do not comply with the rules laid down in the production specifications for Parmeggiano Reggiano. Based on a database created with authentic samples provided by the Consortium of Parmigiano Reggiano Cheese, a reliable classification model was built. The overall classification capabilities of this non-targeted method was verified on 32 grated cheese samples. The classification was 87.5% accurate.http://www.mdpi.com/2304-8158/6/2/13P.D.O.Parmigiano Reggiano cheesegeographical originnon-targeted mass spectrometrychemometrics
spellingShingle Bert Popping
Emiliano De Dominicis
Mario Dante
Marco Nocetti
Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and Chemometrics
Foods
P.D.O.
Parmigiano Reggiano cheese
geographical origin
non-targeted mass spectrometry
chemometrics
title Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and Chemometrics
title_full Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and Chemometrics
title_fullStr Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and Chemometrics
title_full_unstemmed Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and Chemometrics
title_short Identification of the Geographic Origin of Parmigiano Reggiano (P.D.O.) Cheeses Deploying Non-Targeted Mass Spectrometry and Chemometrics
title_sort identification of the geographic origin of parmigiano reggiano p d o cheeses deploying non targeted mass spectrometry and chemometrics
topic P.D.O.
Parmigiano Reggiano cheese
geographical origin
non-targeted mass spectrometry
chemometrics
url http://www.mdpi.com/2304-8158/6/2/13
work_keys_str_mv AT bertpopping identificationofthegeographicoriginofparmigianoreggianopdocheesesdeployingnontargetedmassspectrometryandchemometrics
AT emilianodedominicis identificationofthegeographicoriginofparmigianoreggianopdocheesesdeployingnontargetedmassspectrometryandchemometrics
AT mariodante identificationofthegeographicoriginofparmigianoreggianopdocheesesdeployingnontargetedmassspectrometryandchemometrics
AT marconocetti identificationofthegeographicoriginofparmigianoreggianopdocheesesdeployingnontargetedmassspectrometryandchemometrics