Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder Metallurgy

With the huge demands of an aging society, it is urgent to develop a new generation of non-toxic titanium alloy to match the modulus of human bone. Here, we prepared bulk Ti2448 alloys by powder metallurgy technology, and focused on the influence of the sintering process on the porosity, phase compo...

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Main Authors: Amy X. Y. Guo, Bin Cao, Zihan Wang, Xiao Ma, Shan Cecilia Cao
Format: Article
Language:English
Published: MDPI AG 2023-05-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/10/3845
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author Amy X. Y. Guo
Bin Cao
Zihan Wang
Xiao Ma
Shan Cecilia Cao
author_facet Amy X. Y. Guo
Bin Cao
Zihan Wang
Xiao Ma
Shan Cecilia Cao
author_sort Amy X. Y. Guo
collection DOAJ
description With the huge demands of an aging society, it is urgent to develop a new generation of non-toxic titanium alloy to match the modulus of human bone. Here, we prepared bulk Ti2448 alloys by powder metallurgy technology, and focused on the influence of the sintering process on the porosity, phase composition, and mechanical properties of the initial sintered samples. Furthermore, we performed solution treatment on the samples under different sintering parameters to further adjust the microstructure and phase composition, so as to achieve strength enhancement and reduction of Young’s modulus. Solution treatment can effectively inhibit the continuous α phase precipitated along the grain boundaries of the β matrix, which is beneficial to the fracture resistance. Therefore, the water-quenched sample exhibits good mechanical properties due to the absence of acicular α-phase. Samples sintered at 1400 °C and subsequently water quenched have excellent comprehensive mechanical properties, which benefit from high porosity and the smaller feature size of microstructure. To be specific, the compressive yield stress is 1100 MPa, the strain at fracture is 17.5%, and the Young’s modulus is 44 GPa, which are more applicable to orthopedic implants. Finally, the relatively mature sintering and solution treatment process parameters were screened out for reference in actual production.
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spelling doaj.art-c83e277bdb8f475e95a6202121d2d94d2023-11-18T02:17:03ZengMDPI AGMaterials1996-19442023-05-011610384510.3390/ma16103845Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder MetallurgyAmy X. Y. Guo0Bin Cao1Zihan Wang2Xiao Ma3Shan Cecilia Cao4Materials Genome Institute, Shanghai University, Shanghai 200444, ChinaMaterials Genome Institute, Shanghai University, Shanghai 200444, ChinaMaterials Genome Institute, Shanghai University, Shanghai 200444, ChinaInstitute for the Conservation of Cultural Heritage, Shanghai University, Shanghai 200444, ChinaMaterials Genome Institute, Shanghai University, Shanghai 200444, ChinaWith the huge demands of an aging society, it is urgent to develop a new generation of non-toxic titanium alloy to match the modulus of human bone. Here, we prepared bulk Ti2448 alloys by powder metallurgy technology, and focused on the influence of the sintering process on the porosity, phase composition, and mechanical properties of the initial sintered samples. Furthermore, we performed solution treatment on the samples under different sintering parameters to further adjust the microstructure and phase composition, so as to achieve strength enhancement and reduction of Young’s modulus. Solution treatment can effectively inhibit the continuous α phase precipitated along the grain boundaries of the β matrix, which is beneficial to the fracture resistance. Therefore, the water-quenched sample exhibits good mechanical properties due to the absence of acicular α-phase. Samples sintered at 1400 °C and subsequently water quenched have excellent comprehensive mechanical properties, which benefit from high porosity and the smaller feature size of microstructure. To be specific, the compressive yield stress is 1100 MPa, the strain at fracture is 17.5%, and the Young’s modulus is 44 GPa, which are more applicable to orthopedic implants. Finally, the relatively mature sintering and solution treatment process parameters were screened out for reference in actual production.https://www.mdpi.com/1996-1944/16/10/3845Ti2448 alloymicrostructure analysisporositymechanical properties
spellingShingle Amy X. Y. Guo
Bin Cao
Zihan Wang
Xiao Ma
Shan Cecilia Cao
Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder Metallurgy
Materials
Ti2448 alloy
microstructure analysis
porosity
mechanical properties
title Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder Metallurgy
title_full Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder Metallurgy
title_fullStr Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder Metallurgy
title_full_unstemmed Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder Metallurgy
title_short Fabricated High-Strength, Low-Elastic Modulus Biomedical Ti-24Nb-4Zr-8Sn Alloy via Powder Metallurgy
title_sort fabricated high strength low elastic modulus biomedical ti 24nb 4zr 8sn alloy via powder metallurgy
topic Ti2448 alloy
microstructure analysis
porosity
mechanical properties
url https://www.mdpi.com/1996-1944/16/10/3845
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