Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoate
The title compound was prepared by inducing amide bond formation between methyl 2-[(2-aminophenyl)ethynyl]benzoate and 2-[(2-acetamidophenyl)ethynyl]benzoic acid in the presence of dichlorotriphenylphosphorane. The structure of the synthesized compound was determined on the basis of its 1H-nuclear m...
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| Format: | Article |
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MDPI AG
2015-04-01
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| Series: | Molbank |
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| Online Access: | http://www.mdpi.com/1422-8599/2015/2/M854 |
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| author | Yosuke Demizu Takashi Misawa Nanako Yamagata Mitsunobu Doi Masaaki Kurihara |
| author_facet | Yosuke Demizu Takashi Misawa Nanako Yamagata Mitsunobu Doi Masaaki Kurihara |
| author_sort | Yosuke Demizu |
| collection | DOAJ |
| description | The title compound was prepared by inducing amide bond formation between methyl 2-[(2-aminophenyl)ethynyl]benzoate and 2-[(2-acetamidophenyl)ethynyl]benzoic acid in the presence of dichlorotriphenylphosphorane. The structure of the synthesized compound was determined on the basis of its 1H-nuclear magnetic resonance (NMR), 13C-NMR, and mass spectral data. Furthermore, the compound’s crystal structure is also reported. |
| first_indexed | 2024-12-13T13:13:42Z |
| format | Article |
| id | doaj.art-c9170689451b49feaa8b7044e84f94bf |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-12-13T13:13:42Z |
| publishDate | 2015-04-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-c9170689451b49feaa8b7044e84f94bf2022-12-21T23:44:37ZengMDPI AGMolbank1422-85992015-04-0120152M85410.3390/M854M854Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoateYosuke Demizu0Takashi Misawa1Nanako Yamagata2Mitsunobu Doi3Masaaki Kurihara4Division of Organic Chemistry, National Institute of Health Sciences, 1-18-1, Kamiyoga, Setagaya, Tokyo 158-8501, JapanDivision of Organic Chemistry, National Institute of Health Sciences, 1-18-1, Kamiyoga, Setagaya, Tokyo 158-8501, JapanDivision of Organic Chemistry, National Institute of Health Sciences, 1-18-1, Kamiyoga, Setagaya, Tokyo 158-8501, JapanOsaka University of Pharmaceutical Sciences, Osaka 569-1094, JapanDivision of Organic Chemistry, National Institute of Health Sciences, 1-18-1, Kamiyoga, Setagaya, Tokyo 158-8501, JapanThe title compound was prepared by inducing amide bond formation between methyl 2-[(2-aminophenyl)ethynyl]benzoate and 2-[(2-acetamidophenyl)ethynyl]benzoic acid in the presence of dichlorotriphenylphosphorane. The structure of the synthesized compound was determined on the basis of its 1H-nuclear magnetic resonance (NMR), 13C-NMR, and mass spectral data. Furthermore, the compound’s crystal structure is also reported.http://www.mdpi.com/1422-8599/2015/2/M854foldameraromatic amideX-ray crystallographic analysis |
| spellingShingle | Yosuke Demizu Takashi Misawa Nanako Yamagata Mitsunobu Doi Masaaki Kurihara Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoate Molbank foldamer aromatic amide X-ray crystallographic analysis |
| title | Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoate |
| title_full | Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoate |
| title_fullStr | Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoate |
| title_full_unstemmed | Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoate |
| title_short | Methyl 2-[(2-{2-[(2-acetamidophenyl)ethynyl]benzamido} phenyl)ethynyl]benzoate |
| title_sort | methyl 2 2 2 2 acetamidophenyl ethynyl benzamido phenyl ethynyl benzoate |
| topic | foldamer aromatic amide X-ray crystallographic analysis |
| url | http://www.mdpi.com/1422-8599/2015/2/M854 |
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