Syntheses, crystal structures and Hirshfeld surface analysis of three salts of 1-(4-nitrophenyl)piperazine

Syntheses, crystal structures and Hirshfeld surface analysis of three salts of 1-(4-nitrophenyl)piperazine

The structures and Hirshfeld surface analysis of three salts of 1-(4-nitrophenyl)piperazine are discussed. In 4-(4-nitrophenyl)piperazin-1-ium salicylate (C10H14N3O2+·C7H5O3−), there are strong hydrogen bonds between cation and anion and the 4-nitrophenyl substituent occupies an equatorial position...

Full description

Bibliographic Details
Main Authors:	Sreeramapura D. Archana, Sabine Foro, Hemmige S. Yathirajan, Haruvegowda Kiran Kumar, Rishik Balerao, Ray J. Butcher
Format:	Article
Language:	English
Published:	International Union of Crystallography 2023-04-01
Series:	Acta Crystallographica Section E: Crystallographic Communications
Subjects:	crystal structure piperazinium salt hirshfeld surface analysis salicylate graph-set notation axial and equatorial substitution patterns in piperazinium rings
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2056989023002517

Similar Items

Syntheses and crystal structures of three salts of 1-(4-nitrophenyl)piperazine
by: Holehundi J. Shankara Prasad, et al.
Published: (2023-05-01)

Syntheses and crystal structures of four 4-(4-nitrophenyl)piperazinium salts with hydrogen succinate, 4-aminobenzoate, 2-(4-chlorophenyl)acetate and 2,3,4,5,6-pentafluorobenzoate anions
by: Vinaya, et al.
Published: (2023-03-01)

Syntheses and crystal structures of four 4-(4-methoxyphenyl)piperazin-1-ium salts: trifluoroacetate, 2,3,4,5,6-pentafluorobenzoate, 4-iodobenzoate, and a polymorph with 4-methylbenzoate
by: Vinaya, et al.
Published: (2023-04-01)

4-(2,3-Dichlorophenyl)piperazin-1-ium picrate
by: Udhayasuriyan Sathya, et al.
Published: (2021-04-01)

4-(3-Chlorophenyl)-1-(3-chloropropyl)piperazin-1-ium chloride redetermined at 100 K
by: Muzzaffar Ahmad Bhat, et al.
Published: (2016-02-01)

Crystal structure of 4-(2-methoxyphenyl)piperazin-1-ium 3,5-dintrosalicylate
by: Veerappan Subha, et al.
Published: (2022-08-01)

Syntheses, crystal structures and Hirshfeld surface analysis of 4-(4-nitrophenyl)piperazin-1-ium trifluoroacetate and 4-(4-nitrophenyl)piperazin-1-ium trichloroacetate
by: Holehundi J. Shankara Prasad, et al.
Published: (2023-01-01)

Synthesis and crystal structures of 1-benzoyl-4-(4-nitrophenyl)piperazine and 1-(4-bromobenzoyl)-4-phenylpiperazine at 90 K
by: Sreeramapura D. Archana, et al.
Published: (2022-10-01)

Crystal structures of six 4-(4-nitrophenyl)piperazin-1-ium salts
by: Ninganayaka Mahesha, et al.
Published: (2022-05-01)

Syntheses, crystal structures and Hirshfeld surface analyses of four molecular salts of amitriptynol
by: Vinaya, et al.
Published: (2023-05-01)

Synthesis, crystal structure and Hirshfeld surface analysis of N-(4-fluorophenyl)-N-isopropyl-2-(methylsulfonyl)acetamide
by: Doreswamy Geetha, et al.
Published: (2023-05-01)

Crystal structure and Hirshfeld surface analysis of N,N′-bis(2-nitrophenyl)glutaramide
by: Akshatha R. Salian, et al.
Published: (2018-10-01)

The structures of eleven (4-phenyl)piperazinium salts containing organic anions
by: Sreeramapura D. Archana, et al.
Published: (2022-10-01)

Crystal structure of (E)-N'-[1-(4-aminophenyl)ethylidene]-2-hydroxy-5-iodobenzohydrazide methanol monosolvate
by: Cong Nguyen Tien, et al.
Published: (2018-07-01)

Twelve 4-(4-methoxyphenyl)piperazin-1-ium salts containing organic anions: supramolecular assembly in one, two and three dimensions
by: Haruvegowda Kiran Kumar, et al.
Published: (2019-10-01)

Syntheses and crystal structures of 4-(4-nitrophenyl)piperazin-1-ium benzoate monohydrate and 4-(4-nitrophenyl)piperazin-1-ium 2-carboxy-4,6-dinitrophenolate
by: Holehundi J. Shankara Prasad, et al.
Published: (2022-08-01)

3-Methyl-5-(4-methylphenoxy)-1-phenyl-1H-pyrazole-4-carbaldehyde
by: Sreeramapura D. Archana, et al.
Published: (2022-09-01)

5-(4-Fluorophenyl)-1-[4-(4-methylphenyl)thiazol-2-yl]-3-[4-(prop-2-ynyloxy)phenyl]-4,5-dihydro-1H-pyrazole
by: Sreeramapura D. Archana, et al.
Published: (2022-10-01)

5-(4-Methoxyphenyl)-1-[4-(4-methoxyphenyl)thiazol-2-yl]-3-[4-(prop-2-ynyloxy)phenyl]-4,5-dihydro-1H-pyrazole
by: Sreeramapura D. Archana, et al.
Published: (2022-11-01)

Crystal structure and Hirshfeld surface analysis of (E)-1-[2,2-dichloro-1-(4-nitrophenyl)ethenyl]-2-(4-fluorophenyl)diazene
by: Zeliha Atioğlu, et al.
Published: (2019-02-01)

New Zinc Coordination Compound with Simple Salicylato and Pyridine Ligands: Synthesis, Crystal Structure and Hirshfeld Surface Analysis
by: Nives Kitanovski, et al.
Published: (2021-06-01)

Crystal structures of the recreational drug N-(4-methoxyphenyl)piperazine (MeOPP) and three of its salts
by: Haruvegowda Kiran Kumar, et al.
Published: (2020-04-01)

3-(3-Nitrophenyl)-1-[4-(prop-2-ynyloxy)phenyl]prop-2-en-1-one
by: Vinaya, et al.
Published: (2022-10-01)

Six 1-aroyl-4-(4-methoxyphenyl)piperazines: similar molecular structures but different patterns of supramolecular assembly
by: Haruvegowda Kiran Kumar, et al.
Published: (2019-08-01)

Crystal structure and Hirshfeld-surface analysis of a monoclinic polymorph of 2-amino-5-chlorobenzophenone oxime at 90 K
by: Doreswamy Geetha, et al.
Published: (2023-07-01)

Structural Characterization of 4-(4-Nitrophenyl)thiomorpholine, a Precursor in Medicinal Chemistry
by: Paul R. Palme, et al.
Published: (2024-03-01)

Bis[N-(2-hydroxyethyl)-N-isopropyldithiocarbamato-κ2S,S′](piperazine-κN)cadmium: crystal structure and Hirshfeld surface analysis
by: Siti Artikah M. Safbri, et al.
Published: (2016-02-01)

Crystal structure and Hirshfeld surface analysis of 2-(4-nitrophenyl)-2-oxoethyl 2-chlorobenzoate
by: S. N. Sheshadri, et al.
Published: (2019-11-01)

Syntheses, crystal structures and Hirshfeld surface analyses of N-arylsulfonyl derivatives of cytisine
by: Rasul Ya. Okmanov, et al.
Published: (2023-04-01)

Crystal structure and Hirshfeld surface analysis of a chalcone derivative: (E)-3-(4-fluorophenyl)-1-(4-nitrophenyl)prop-2-en-1-one
by: Qin Ai Wong, et al.
Published: (2019-01-01)

Crystal structure and Hirshfeld surface analysis of 1-[(E)-2-(3-nitrophenyl)diazen-1-yl]naphthalen-2-ol
by: Mohamed Amine Benaouida, et al.
Published: (2023-03-01)

Crystal structure and Hirshfeld surface analysis of 2-(4-nitrophenyl)-2-oxoethyl benzoate
by: S. N. Sheshadri, et al.
Published: (2019-11-01)

Crystal structure and Hirshfeld surface analysis of the hydrated 2:1 adduct of piperazine-1,4-diium 3,5-dinitro-2-oxidobenzoate and piperazine
by: Veerappan Subha, et al.
Published: (2022-02-01)

Crystal Structure Determination and Hirshfeld Analysis of a New Alternariol Packing Polymorph
by: Kelly L. Rue, et al.
Published: (2022-04-01)

Crystal structure and Hirshfeld surface analysis of (Z)-4-chloro-N′-(4-oxothiazolidin-2-ylidene)benzenesulfonohydrazide monohydrate
by: Nikhila Pai, et al.
Published: (2018-11-01)

Fragmentation and transferability in Hirshfeld atom refinement
by: Michał Chodkiewicz, et al.
Published: (2022-03-01)

Crystal structure and Hirshfeld surface analysis of N-[2-(5-methylfuran-2-yl)phenyl]-3-nitro-N-[(3-nitrophenyl)sulfonyl]benzenesulfonamide
by: Gunay Z. Mammadova, et al.
Published: (2023-05-01)

Synthesis, crystal structure and Hirshfeld surface analysis of 2-({5-[(naphthalen-1-yl)methyl]-4-phenyl-4H-1,2,4-triazol-3-yl}sulfanyl)-1-(4-nitrophenyl)ethanone
by: Trong Duc Le, et al.
Published: (2024-02-01)

Crystal structures and Hirshfeld surface analyses of the two isotypic compounds (E)-1-(4-bromophenyl)-2-[2,2-dichloro-1-(4-nitrophenyl)ethenyl]diazene and (E)-1-(4-chlorophenyl)-2-[2,2-dichloro-1-(4-nitrophenyl)ethenyl]diazene
by: Mehmet Akkurt, et al.
Published: (2019-08-01)

Crystal structure and Hirshfeld surface analysis of a new polymorph of (E)-2-(4-bromophenyl)-1-[2,2-dibromo-1-(3-nitrophenyl)ethenyl]diazene
by: Zeliha Atioğlu, et al.
Published: (2022-08-01)