Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanol

Abstract The active gamma alumina oxide catalyst was prepared by using the precipitation of mixing of aluminum nitrate and aqueous ammonia . The effect of calcinations temperature of aluminum hydroxide on the crystallography of the alumina oxide products were studied by means the thermal analysis an...

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Main Author: Khalid Hummadi
Format: Article
Language:English
Published: Unviversity of Technology- Iraq 2005-04-01
Series:Engineering and Technology Journal
Subjects:
Online Access:https://etj.uotechnology.edu.iq/article_181845_b6ea4975400e714825a73802925c29f5.pdf
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author Khalid Hummadi
author_facet Khalid Hummadi
author_sort Khalid Hummadi
collection DOAJ
description Abstract The active gamma alumina oxide catalyst was prepared by using the precipitation of mixing of aluminum nitrate and aqueous ammonia . The effect of calcinations temperature of aluminum hydroxide on the crystallography of the alumina oxide products were studied by means the thermal analysis and the X - Ray diffraction technique . The calcinations temperature were ( 300 , 500 , 600 , 650 , 700 , 800 , 900 , and 1000 ) " C. Also the surface area , pore volume , and mean pore radius were measured for all alumina oxide products . The activity of these alumina oxides for dehydration of ethanol was studied and comparable to that of commercial alumina oxide . The reaction was carried out in a tubular reactor under atmospheric pressure and 350 ° C.While the reaction products were analyzed by gas chromatography technique . The results show that the calcination temperature of 600-650 ° C gives the active crystal phase of gamma alumina oxide which is exhibit comparable dehydration activity to the commercial catalyst .
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spelling doaj.art-c978ebf09e054e5ca9f3ae6a46f3f5a22024-02-04T17:56:04ZengUnviversity of Technology- IraqEngineering and Technology Journal1681-69002412-07582005-04-0124436838310.30684/etj.24.4.3181845Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanolKhalid Hummadi0Dep. of Biochemical Engineering University of BaghdadAbstract The active gamma alumina oxide catalyst was prepared by using the precipitation of mixing of aluminum nitrate and aqueous ammonia . The effect of calcinations temperature of aluminum hydroxide on the crystallography of the alumina oxide products were studied by means the thermal analysis and the X - Ray diffraction technique . The calcinations temperature were ( 300 , 500 , 600 , 650 , 700 , 800 , 900 , and 1000 ) " C. Also the surface area , pore volume , and mean pore radius were measured for all alumina oxide products . The activity of these alumina oxides for dehydration of ethanol was studied and comparable to that of commercial alumina oxide . The reaction was carried out in a tubular reactor under atmospheric pressure and 350 ° C.While the reaction products were analyzed by gas chromatography technique . The results show that the calcination temperature of 600-650 ° C gives the active crystal phase of gamma alumina oxide which is exhibit comparable dehydration activity to the commercial catalyst .https://etj.uotechnology.edu.iq/article_181845_b6ea4975400e714825a73802925c29f5.pdfkeyword: calcinationsaluminum hydroxidegamma aluminaethanol dehydration
spellingShingle Khalid Hummadi
Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanol
Engineering and Technology Journal
keyword: calcinations
aluminum hydroxide
gamma alumina
ethanol dehydration
title Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanol
title_full Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanol
title_fullStr Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanol
title_full_unstemmed Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanol
title_short Influence of calcination temperature of prepared Aluminum hydroxide on the activity of active gamma Alumina oxide on the dehydration of ethanol
title_sort influence of calcination temperature of prepared aluminum hydroxide on the activity of active gamma alumina oxide on the dehydration of ethanol
topic keyword: calcinations
aluminum hydroxide
gamma alumina
ethanol dehydration
url https://etj.uotechnology.edu.iq/article_181845_b6ea4975400e714825a73802925c29f5.pdf
work_keys_str_mv AT khalidhummadi influenceofcalcinationtemperatureofpreparedaluminumhydroxideontheactivityofactivegammaaluminaoxideonthedehydrationofethanol