Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle Concentration

The tribological properties of nanofluids are influenced by multiple factors, and the interrelationships among the factors are deserving of further attention. In this paper, response surface methodology (RSM) was used to study the tribological behavior of reduced graphene oxide–Al<sub>2</su...

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Main Authors: Chenglong Wang, Jianlin Sun, Linghui Kong, Jiaqi He
Format: Article
Language:English
Published: MDPI AG 2022-07-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/15/15/5177
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author Chenglong Wang
Jianlin Sun
Linghui Kong
Jiaqi He
author_facet Chenglong Wang
Jianlin Sun
Linghui Kong
Jiaqi He
author_sort Chenglong Wang
collection DOAJ
description The tribological properties of nanofluids are influenced by multiple factors, and the interrelationships among the factors are deserving of further attention. In this paper, response surface methodology (RSM) was used to study the tribological behavior of reduced graphene oxide–Al<sub>2</sub>O<sub>3</sub> (rGO-Al<sub>2</sub>O<sub>3</sub>) nanofluid. The interaction effects of testing force, rotational speed and nanoparticle concentration on the friction coefficient (<i>μ</i>), wear rate (<i>W</i><sub>r</sub>) and surface roughness (<i>R</i><sub>a</sub>) of steel disks were investigated via the analysis of variance. It was confirmed that all the three input variables were significant for <i>μ</i> and <i>W</i><sub>r</sub> values, while testing force, nanoparticle concentration and its interaction with testing force and rotational speed were identified as significant parameters for <i>R</i><sub>a</sub> value. According to regression quadratic models, the optimized response values were 0.088, 2.35 × 10<sup>−7</sup> mm<sup>3</sup>·N<sup>−1</sup>·m<sup>−1</sup> and 0.832 μm for <i>μ</i>, <i>W</i><sub>r</sub> and <i>R</i><sub>a</sub>, which were in good agreement with the actual validation experiment values. The tribological results show that 0.20% was the optimum mass concentration which exhibited excellent lubrication performance. Compared to the base fluid, <i>μ</i>, <i>W</i><sub>r</sub> and <i>R</i><sub>a</sub> values had a reduction of approximately 45.6%, 90.3% and 56.0%. Tribochemical reactions occurred during the friction process, and a tribofilm with a thickness of approximately 20 nm was generated on the worn surface, consisting of nanoparticle fragments (rGO and Al<sub>2</sub>O<sub>3</sub>) and metal oxides (Fe<sub>2</sub>O<sub>3</sub> and FeO) with self-lubrication properties.
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spelling doaj.art-ca0aa8555439498eb5d1508ec947f6e72023-12-03T12:45:05ZengMDPI AGMaterials1996-19442022-07-011515517710.3390/ma15155177Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle ConcentrationChenglong Wang0Jianlin Sun1Linghui Kong2Jiaqi He3School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, ChinaSchool of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, ChinaThe Yellow River Institute of Hydraulic Research, the Yellow River Water Conservancy Commission, Zhengzhou 450003, ChinaSchool of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, ChinaThe tribological properties of nanofluids are influenced by multiple factors, and the interrelationships among the factors are deserving of further attention. In this paper, response surface methodology (RSM) was used to study the tribological behavior of reduced graphene oxide–Al<sub>2</sub>O<sub>3</sub> (rGO-Al<sub>2</sub>O<sub>3</sub>) nanofluid. The interaction effects of testing force, rotational speed and nanoparticle concentration on the friction coefficient (<i>μ</i>), wear rate (<i>W</i><sub>r</sub>) and surface roughness (<i>R</i><sub>a</sub>) of steel disks were investigated via the analysis of variance. It was confirmed that all the three input variables were significant for <i>μ</i> and <i>W</i><sub>r</sub> values, while testing force, nanoparticle concentration and its interaction with testing force and rotational speed were identified as significant parameters for <i>R</i><sub>a</sub> value. According to regression quadratic models, the optimized response values were 0.088, 2.35 × 10<sup>−7</sup> mm<sup>3</sup>·N<sup>−1</sup>·m<sup>−1</sup> and 0.832 μm for <i>μ</i>, <i>W</i><sub>r</sub> and <i>R</i><sub>a</sub>, which were in good agreement with the actual validation experiment values. The tribological results show that 0.20% was the optimum mass concentration which exhibited excellent lubrication performance. Compared to the base fluid, <i>μ</i>, <i>W</i><sub>r</sub> and <i>R</i><sub>a</sub> values had a reduction of approximately 45.6%, 90.3% and 56.0%. Tribochemical reactions occurred during the friction process, and a tribofilm with a thickness of approximately 20 nm was generated on the worn surface, consisting of nanoparticle fragments (rGO and Al<sub>2</sub>O<sub>3</sub>) and metal oxides (Fe<sub>2</sub>O<sub>3</sub> and FeO) with self-lubrication properties.https://www.mdpi.com/1996-1944/15/15/5177reduced graphene oxidetribologynanofluidlubrication mechanismresponse surface methodology
spellingShingle Chenglong Wang
Jianlin Sun
Linghui Kong
Jiaqi He
Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle Concentration
Materials
reduced graphene oxide
tribology
nanofluid
lubrication mechanism
response surface methodology
title Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle Concentration
title_full Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle Concentration
title_fullStr Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle Concentration
title_full_unstemmed Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle Concentration
title_short Tribological Behavior of Reduced Graphene Oxide–Al<sub>2</sub>O<sub>3</sub> Nanofluid: Interaction among Testing Force, Rotational Speed and Nanoparticle Concentration
title_sort tribological behavior of reduced graphene oxide al sub 2 sub o sub 3 sub nanofluid interaction among testing force rotational speed and nanoparticle concentration
topic reduced graphene oxide
tribology
nanofluid
lubrication mechanism
response surface methodology
url https://www.mdpi.com/1996-1944/15/15/5177
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AT linghuikong tribologicalbehaviorofreducedgrapheneoxidealsub2subosub3subnanofluidinteractionamongtestingforcerotationalspeedandnanoparticleconcentration
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