Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization Process

In the context of the growing interest in biopolymer-based materials for various applications, this study aimed to enhance the properties of chitosan (CS, a derivative of chitin) films by incorporating caffeic acid, a polyphenol compound known for its multiple health benefits. The objective was to i...

Full description

Bibliographic Details
Main Authors: Marta Szulc, Katarzyna Lewandowska
Format: Article
Language:English
Published: MDPI AG 2023-07-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/14/5038
_version_ 1797588519651115008
author Marta Szulc
Katarzyna Lewandowska
author_facet Marta Szulc
Katarzyna Lewandowska
author_sort Marta Szulc
collection DOAJ
description In the context of the growing interest in biopolymer-based materials for various applications, this study aimed to enhance the properties of chitosan (CS, a derivative of chitin) films by incorporating caffeic acid, a polyphenol compound known for its multiple health benefits. The objective was to improve the mechanical parameters of the resulting films, including surface roughness and elasticity. CS was combined with caffeic acid and then underwent a neutralization process. The modified films exhibited potential for use in soft tissue engineering, where increased elasticity and surface roughness are desirable characteristics. The main methods employed to evaluate the structure and properties of the films included mechanical analysis, infrared spectroscopy, scanning electron microscopy, atomic force microscopy, thermogravimetric analysis, contact angle measurement, and swelling behavior. The study’s main findings revealed significant alterations in the mechanical properties and surface morphology of the films. The main conclusions drawn from the study suggest that interactions between caffeic acid and CS hold promise for the development of advanced biomaterials in medicine, tissue engineering, and cosmetic formulations. However, a deeper understanding of these interactions is necessary to optimize the material properties and unlock their full potential.
first_indexed 2024-03-11T00:53:13Z
format Article
id doaj.art-ca6988da6a4e4488bc862c75806bbb08
institution Directory Open Access Journal
issn 1996-1944
language English
last_indexed 2024-03-11T00:53:13Z
publishDate 2023-07-01
publisher MDPI AG
record_format Article
series Materials
spelling doaj.art-ca6988da6a4e4488bc862c75806bbb082023-11-18T20:17:04ZengMDPI AGMaterials1996-19442023-07-011614503810.3390/ma16145038Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization ProcessMarta Szulc0Katarzyna Lewandowska1Department of Biomaterials and Cosmetic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Toruń, Gagarin 7, 87-100 Toruń, PolandDepartment of Biomaterials and Cosmetic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Toruń, Gagarin 7, 87-100 Toruń, PolandIn the context of the growing interest in biopolymer-based materials for various applications, this study aimed to enhance the properties of chitosan (CS, a derivative of chitin) films by incorporating caffeic acid, a polyphenol compound known for its multiple health benefits. The objective was to improve the mechanical parameters of the resulting films, including surface roughness and elasticity. CS was combined with caffeic acid and then underwent a neutralization process. The modified films exhibited potential for use in soft tissue engineering, where increased elasticity and surface roughness are desirable characteristics. The main methods employed to evaluate the structure and properties of the films included mechanical analysis, infrared spectroscopy, scanning electron microscopy, atomic force microscopy, thermogravimetric analysis, contact angle measurement, and swelling behavior. The study’s main findings revealed significant alterations in the mechanical properties and surface morphology of the films. The main conclusions drawn from the study suggest that interactions between caffeic acid and CS hold promise for the development of advanced biomaterials in medicine, tissue engineering, and cosmetic formulations. However, a deeper understanding of these interactions is necessary to optimize the material properties and unlock their full potential.https://www.mdpi.com/1996-1944/16/14/5038chitosancross-linkingsurface propertiesalkali treatment
spellingShingle Marta Szulc
Katarzyna Lewandowska
Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization Process
Materials
chitosan
cross-linking
surface properties
alkali treatment
title Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization Process
title_full Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization Process
title_fullStr Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization Process
title_full_unstemmed Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization Process
title_short Characterization of Chitosan Films Modified Using Caffeic Acid and a Neutralization Process
title_sort characterization of chitosan films modified using caffeic acid and a neutralization process
topic chitosan
cross-linking
surface properties
alkali treatment
url https://www.mdpi.com/1996-1944/16/14/5038
work_keys_str_mv AT martaszulc characterizationofchitosanfilmsmodifiedusingcaffeicacidandaneutralizationprocess
AT katarzynalewandowska characterizationofchitosanfilmsmodifiedusingcaffeicacidandaneutralizationprocess