The effect of preparation method and presence of impurity on structural properties and morphology of iron oxide

In this paper, the effect of the structural properties and morphology of iron oxide product, have been studied in co-precipitation and hydrothermal methods. Also, the effect of adding CCl4 impurities and final annealing of the materials is taken into account. The more homogeneous particle size in hy...

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Main Authors: Maryam Mahdavi Matin, Mohsen Hakimi, M . Mazloum-Ardakani
Format: Article
Language:English
Published: Islamic Azad University, Marvdasht Branch 2017-01-01
Series:Journal of Optoelectronical Nanostructures
Subjects:
Online Access:https://jopn.marvdasht.iau.ir/article_2195_53c324065a22d87f49373f7ca13e4f95.pdf
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author Maryam Mahdavi Matin
Mohsen Hakimi
M . Mazloum-Ardakani
author_facet Maryam Mahdavi Matin
Mohsen Hakimi
M . Mazloum-Ardakani
author_sort Maryam Mahdavi Matin
collection DOAJ
description In this paper, the effect of the structural properties and morphology of iron oxide product, have been studied in co-precipitation and hydrothermal methods. Also, the effect of adding CCl4 impurities and final annealing of the materials is taken into account. The more homogeneous particle size in hydrothermal method has been explained by the effect of adding CCl4 as impurities to prevent the continuation of nucleation. It has also been observed that in co-precipitation sample additive has a key role for providing the bar shape particles by mediating of the anisotropic connection of nuclei. The difference in the crystal structure of the anneal samples has been related to the oxygen content.
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spelling doaj.art-cb145378cf77477eb4173d21744dc77f2023-04-11T05:28:31ZengIslamic Azad University, Marvdasht BranchJournal of Optoelectronical Nanostructures2423-73612538-24892017-01-0121182195The effect of preparation method and presence of impurity on structural properties and morphology of iron oxideMaryam Mahdavi Matin0Mohsen Hakimi1M . Mazloum-Ardakani2Master student, Research and Technology of Magnetizm lab physics Department Yazd University, YazdAssistant Professor, Research and Technology of Magnetizm lab physics Department Yazd University, YazdProfessor, Department of Chemistry, Yazd University, YazdIn this paper, the effect of the structural properties and morphology of iron oxide product, have been studied in co-precipitation and hydrothermal methods. Also, the effect of adding CCl4 impurities and final annealing of the materials is taken into account. The more homogeneous particle size in hydrothermal method has been explained by the effect of adding CCl4 as impurities to prevent the continuation of nucleation. It has also been observed that in co-precipitation sample additive has a key role for providing the bar shape particles by mediating of the anisotropic connection of nuclei. The difference in the crystal structure of the anneal samples has been related to the oxygen content.https://jopn.marvdasht.iau.ir/article_2195_53c324065a22d87f49373f7ca13e4f95.pdfiron oxideco-precipitationhydrothermalccl4 additivebar structure shape
spellingShingle Maryam Mahdavi Matin
Mohsen Hakimi
M . Mazloum-Ardakani
The effect of preparation method and presence of impurity on structural properties and morphology of iron oxide
Journal of Optoelectronical Nanostructures
iron oxide
co-precipitation
hydrothermal
ccl4 additive
bar structure shape
title The effect of preparation method and presence of impurity on structural properties and morphology of iron oxide
title_full The effect of preparation method and presence of impurity on structural properties and morphology of iron oxide
title_fullStr The effect of preparation method and presence of impurity on structural properties and morphology of iron oxide
title_full_unstemmed The effect of preparation method and presence of impurity on structural properties and morphology of iron oxide
title_short The effect of preparation method and presence of impurity on structural properties and morphology of iron oxide
title_sort effect of preparation method and presence of impurity on structural properties and morphology of iron oxide
topic iron oxide
co-precipitation
hydrothermal
ccl4 additive
bar structure shape
url https://jopn.marvdasht.iau.ir/article_2195_53c324065a22d87f49373f7ca13e4f95.pdf
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