Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOx

With TEMPO oxidation, it was possible to incorporate iron nanostructures into a cellulose nanofiber matrix. FTIR spectra showed the functional groups present in the films. The combination of both iron and CNF confers to the films good electrochemical activity; the electrochemical characterization (C...

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Main Authors: Araceli G. Gomez-Rojas, Luis Alejandro Macclesh del Pino-Perez, Carlos Fernando Castro-Guerrero, Claudia Esmeralda Ramos-Galvan, Ana Beatriz Morales-Cepeda
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Fibers
Subjects:
Online Access:https://www.mdpi.com/2079-6439/11/1/8
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author Araceli G. Gomez-Rojas
Luis Alejandro Macclesh del Pino-Perez
Carlos Fernando Castro-Guerrero
Claudia Esmeralda Ramos-Galvan
Ana Beatriz Morales-Cepeda
author_facet Araceli G. Gomez-Rojas
Luis Alejandro Macclesh del Pino-Perez
Carlos Fernando Castro-Guerrero
Claudia Esmeralda Ramos-Galvan
Ana Beatriz Morales-Cepeda
author_sort Araceli G. Gomez-Rojas
collection DOAJ
description With TEMPO oxidation, it was possible to incorporate iron nanostructures into a cellulose nanofiber matrix. FTIR spectra showed the functional groups present in the films. The combination of both iron and CNF confers to the films good electrochemical activity; the electrochemical characterization (CV) showed that they present stability in the reduction process at a potential of 0–1 V, with the materials with 5% and 10% being the most active. The Pb reduction process shows that the 5% film is the material with the highest oxidizing capacity.
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spelling doaj.art-cb9348016d33472199679f605ec2f08f2023-11-30T22:11:18ZengMDPI AGFibers2079-64392023-01-01111810.3390/fib11010008Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOxAraceli G. Gomez-Rojas0Luis Alejandro Macclesh del Pino-Perez1Carlos Fernando Castro-Guerrero2Claudia Esmeralda Ramos-Galvan3Ana Beatriz Morales-Cepeda4Petrochemical Research Center, Technological Institute of Madero City—National Technological Institute of Mexico, Altamira 89600, MexicoPetrochemical Research Center, Technological Institute of Madero City—National Technological Institute of Mexico, Altamira 89600, MexicoCONACyT, Technological Institute of Madero City—National Technological Institute of Mexico, Altamira 89600, MexicoPetrochemical Research Center, Technological Institute of Madero City—National Technological Institute of Mexico, Altamira 89600, MexicoPetrochemical Research Center, Technological Institute of Madero City—National Technological Institute of Mexico, Altamira 89600, MexicoWith TEMPO oxidation, it was possible to incorporate iron nanostructures into a cellulose nanofiber matrix. FTIR spectra showed the functional groups present in the films. The combination of both iron and CNF confers to the films good electrochemical activity; the electrochemical characterization (CV) showed that they present stability in the reduction process at a potential of 0–1 V, with the materials with 5% and 10% being the most active. The Pb reduction process shows that the 5% film is the material with the highest oxidizing capacity.https://www.mdpi.com/2079-6439/11/1/8nanocelluloseelectrodeFeOxPbII
spellingShingle Araceli G. Gomez-Rojas
Luis Alejandro Macclesh del Pino-Perez
Carlos Fernando Castro-Guerrero
Claudia Esmeralda Ramos-Galvan
Ana Beatriz Morales-Cepeda
Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOx
Fibers
nanocellulose
electrode
FeOx
PbII
title Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOx
title_full Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOx
title_fullStr Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOx
title_full_unstemmed Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOx
title_short Electrochemical Oxidation of Pb II Using Carbon Electrodes Doped with Nanocellulose-FeOx
title_sort electrochemical oxidation of pb ii using carbon electrodes doped with nanocellulose feox
topic nanocellulose
electrode
FeOx
PbII
url https://www.mdpi.com/2079-6439/11/1/8
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