RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATA

Rietveld method was used to conduct a texture refinement analysis for Linde type A zeolite prepared by hydrothermal conditions of 100 ºC for 4 h. Material Analysis Using Diffraction software, which is an open access/user-friendly software, was used to accomplish the analysis using the observed X-ray...

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Main Authors: SAMA M. AL-JUBOURI, BASMA I. WAISI, STUART M. HOLMES
Format: Article
Language:English
Published: Taylor's University 2018-12-01
Series:Journal of Engineering Science and Technology
Subjects:
Online Access:http://jestec.taylors.edu.my/Vol%2013%20issue%2012%20December%202018/13_12_13.pdf
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author SAMA M. AL-JUBOURI
BASMA I. WAISI
STUART M. HOLMES
author_facet SAMA M. AL-JUBOURI
BASMA I. WAISI
STUART M. HOLMES
author_sort SAMA M. AL-JUBOURI
collection DOAJ
description Rietveld method was used to conduct a texture refinement analysis for Linde type A zeolite prepared by hydrothermal conditions of 100 ºC for 4 h. Material Analysis Using Diffraction software, which is an open access/user-friendly software, was used to accomplish the analysis using the observed X-ray diffraction data. This study shows the feasibility of using Material Analysis Using Diffraction software for zeolite analysis because it has not been applied for zeolite before. Implementation of this software for the texture refinement analysis for zeolite can contributes to the field of zeolite preparation in term of adding more reliability to the experimental results. The X-ray diffraction results of the prepared zeolite concur well with the standard Linde type A zeolite. All parameters calculated by Rietveld refinement method for the prepared zeolite were close enough to those for the standard zeolite A. Also, ImageJ software was used for image analysis to obtain the average particle size for zeolite A sample.
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spelling doaj.art-cbbd872183314529b26ff6aa6d32693b2022-12-22T03:58:25ZengTaylor's UniversityJournal of Engineering Science and Technology1823-46902018-12-01131240664077RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATASAMA M. AL-JUBOURI0 BASMA I. WAISI1STUART M. HOLMES2Department of Chemical Engineering, College of Engineering, University of Baghdad, Aljadria, Baghdad, P. O. Box 47024, IraqDepartment of Chemical Engineering, College of Engineering, University of Baghdad, Aljadria, Baghdad, P. O. Box 47024, IraqSchool of Chemical Engineering and Analytical Science, The University of Manchester, Manchester M13 9PL, United KingdomRietveld method was used to conduct a texture refinement analysis for Linde type A zeolite prepared by hydrothermal conditions of 100 ºC for 4 h. Material Analysis Using Diffraction software, which is an open access/user-friendly software, was used to accomplish the analysis using the observed X-ray diffraction data. This study shows the feasibility of using Material Analysis Using Diffraction software for zeolite analysis because it has not been applied for zeolite before. Implementation of this software for the texture refinement analysis for zeolite can contributes to the field of zeolite preparation in term of adding more reliability to the experimental results. The X-ray diffraction results of the prepared zeolite concur well with the standard Linde type A zeolite. All parameters calculated by Rietveld refinement method for the prepared zeolite were close enough to those for the standard zeolite A. Also, ImageJ software was used for image analysis to obtain the average particle size for zeolite A sample.http://jestec.taylors.edu.my/Vol%2013%20issue%2012%20December%202018/13_12_13.pdfCharacterizationCrystal structureLinde type A zeoliteRietveld methodTexture analysisX-ray diffraction
spellingShingle SAMA M. AL-JUBOURI
BASMA I. WAISI
STUART M. HOLMES
RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATA
Journal of Engineering Science and Technology
Characterization
Crystal structure
Linde type A zeolite
Rietveld method
Texture analysis
X-ray diffraction
title RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATA
title_full RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATA
title_fullStr RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATA
title_full_unstemmed RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATA
title_short RIETVELD TEXTURE REFINEMENT ANALYSIS OF LINDE TYPE A ZEOLITE FROM X-RAY DIFFRACTION DATA
title_sort rietveld texture refinement analysis of linde type a zeolite from x ray diffraction data
topic Characterization
Crystal structure
Linde type A zeolite
Rietveld method
Texture analysis
X-ray diffraction
url http://jestec.taylors.edu.my/Vol%2013%20issue%2012%20December%202018/13_12_13.pdf
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AT stuartmholmes rietveldtexturerefinementanalysisoflindetypeazeolitefromxraydiffractiondata