Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites

The effect of thermal exposure at 1000 ℃ to 1200 ℃ on the properties of porous matrix Al2O3/Al2O3 ceramic matrix composites was studied. The results show that the thermal exposure at 1000 ℃ for 100 h has no effect on the tensile strength of the composites. After 100 h at 1100 ℃, the tensile strength...

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Main Authors: YANG Rui, CHEN Yicheng, DENG Yangfang, SUN Shijie, ZHAO Wenqing, YANG Jinhua, JIAO Jian
Format: Article
Language:zho
Published: Journal of Aeronautical Materials 2023-04-01
Series:Journal of Aeronautical Materials
Subjects:
Online Access:http://jam.biam.ac.cn/article/doi/10.11868/j.issn.1005-5053.2023.000006
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author YANG Rui
CHEN Yicheng
DENG Yangfang
SUN Shijie
ZHAO Wenqing
YANG Jinhua
JIAO Jian
author_facet YANG Rui
CHEN Yicheng
DENG Yangfang
SUN Shijie
ZHAO Wenqing
YANG Jinhua
JIAO Jian
author_sort YANG Rui
collection DOAJ
description The effect of thermal exposure at 1000 ℃ to 1200 ℃ on the properties of porous matrix Al2O3/Al2O3 ceramic matrix composites was studied. The results show that the thermal exposure at 1000 ℃ for 100 h has no effect on the tensile strength of the composites. After 100 h at 1100 ℃, the tensile strength of the composites decreases slightly, and after 100 h at 1200 ℃, the tensile strength of the composites decreases obviously. The effects of different thermal exposure durations at 1200 ℃ on the properties of Al2O3/Al2O3 composites, alumina fibers and alumina matrix are further studied, and the micro morphologies of the samples are characterized by optical microscopy and SEM. The results show that the thermal exposure at 1200 ℃ for 100 h has little effect on the performance of alumina fiber, but has a great effect on the alumina matrix. After the thermal exposure at 1200 ℃ for only 10 h, the porosity of alumina matrix is significantly reduced and the density is significantly increased. It can be seen from the SEM morphology of the matrix fracture that with the increase of thermal exposure time at 1200 ℃, the alumina grain size of the matrix gradually increases and the matrix is further sintered. Correspondingly, it can be seen from the fracture morphology of the Al2O3/Al2O3 composite that the length and number of fibers pulled out also decrease significantly. The degradation of the properties of the composites after high temperature thermal exposure is mainly due to the further sintering of alumina matrix, and the densification of porous matrix reduces the toughening effect of the composites.
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spelling doaj.art-cc2ccbeac6ba4e8eb4f0002bc0c5621d2023-04-03T09:47:48ZzhoJournal of Aeronautical MaterialsJournal of Aeronautical Materials1005-50532023-04-014321810.11868/j.issn.1005-5053.2023.0000062023-0006Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix compositesYANG Rui0CHEN Yicheng1DENG Yangfang2SUN Shijie3ZHAO Wenqing4YANG Jinhua5JIAO Jian6National Key Laboratory of Advanced Composites, AECC Beijing Institute of Aeronautical Materials, Beijing 100095,ChinaAECC Sichuan Gas Turbine Establishment, Chengdu 610500,ChinaAECC Sichuan Gas Turbine Establishment, Chengdu 610500,ChinaNational Key Laboratory of Advanced Composites, AECC Beijing Institute of Aeronautical Materials, Beijing 100095,ChinaNational Key Laboratory of Advanced Composites, AECC Beijing Institute of Aeronautical Materials, Beijing 100095,ChinaNational Key Laboratory of Advanced Composites, AECC Beijing Institute of Aeronautical Materials, Beijing 100095,ChinaNational Key Laboratory of Advanced Composites, AECC Beijing Institute of Aeronautical Materials, Beijing 100095,ChinaThe effect of thermal exposure at 1000 ℃ to 1200 ℃ on the properties of porous matrix Al2O3/Al2O3 ceramic matrix composites was studied. The results show that the thermal exposure at 1000 ℃ for 100 h has no effect on the tensile strength of the composites. After 100 h at 1100 ℃, the tensile strength of the composites decreases slightly, and after 100 h at 1200 ℃, the tensile strength of the composites decreases obviously. The effects of different thermal exposure durations at 1200 ℃ on the properties of Al2O3/Al2O3 composites, alumina fibers and alumina matrix are further studied, and the micro morphologies of the samples are characterized by optical microscopy and SEM. The results show that the thermal exposure at 1200 ℃ for 100 h has little effect on the performance of alumina fiber, but has a great effect on the alumina matrix. After the thermal exposure at 1200 ℃ for only 10 h, the porosity of alumina matrix is significantly reduced and the density is significantly increased. It can be seen from the SEM morphology of the matrix fracture that with the increase of thermal exposure time at 1200 ℃, the alumina grain size of the matrix gradually increases and the matrix is further sintered. Correspondingly, it can be seen from the fracture morphology of the Al2O3/Al2O3 composite that the length and number of fibers pulled out also decrease significantly. The degradation of the properties of the composites after high temperature thermal exposure is mainly due to the further sintering of alumina matrix, and the densification of porous matrix reduces the toughening effect of the composites.http://jam.biam.ac.cn/article/doi/10.11868/j.issn.1005-5053.2023.000006thermal exposurealuminaceramic matrix compositetensile strength
spellingShingle YANG Rui
CHEN Yicheng
DENG Yangfang
SUN Shijie
ZHAO Wenqing
YANG Jinhua
JIAO Jian
Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites
Journal of Aeronautical Materials
thermal exposure
alumina
ceramic matrix composite
tensile strength
title Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites
title_full Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites
title_fullStr Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites
title_full_unstemmed Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites
title_short Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites
title_sort effect of high temperature thermal exposure on properties of al2o3 al2o3 ceramic matrix composites
topic thermal exposure
alumina
ceramic matrix composite
tensile strength
url http://jam.biam.ac.cn/article/doi/10.11868/j.issn.1005-5053.2023.000006
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