Synthesis and characterization of apatite silicated powders with wet precipitation method

The synthesis of apatite silicated Ca10(PO4)6-x(SiO4)x(OH)2-x (SiHA) with 0≤x≤2 was investigated using a wet precipitation method followed by heat treatment using calcium carbonate CaCO3 and phosphoric acid H3PO4 and silicon tetraacetate SiC8H20O4 (TEOS) in medium of water ethanol, with three differ...

Full description

Bibliographic Details
Main Authors: Labjar Houda, Chaair Hassan
Format: Article
Language:English
Published: EDP Sciences 2021-01-01
Series:E3S Web of Conferences
Online Access:https://www.e3s-conferences.org/articles/e3sconf/pdf/2021/10/e3sconf_icies2020_00106.pdf
_version_ 1828728397340082176
author Labjar Houda
Chaair Hassan
author_facet Labjar Houda
Chaair Hassan
author_sort Labjar Houda
collection DOAJ
description The synthesis of apatite silicated Ca10(PO4)6-x(SiO4)x(OH)2-x (SiHA) with 0≤x≤2 was investigated using a wet precipitation method followed by heat treatment using calcium carbonate CaCO3 and phosphoric acid H3PO4 and silicon tetraacetate SiC8H20O4 (TEOS) in medium of water ethanol, with three different silicate concentrations. After drying, the samples are ground and then characterized by different analytical techniques like X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR) and Scanning electron Microscopy (SEM) and chemical analysis.
first_indexed 2024-04-12T14:14:37Z
format Article
id doaj.art-ccbfa0a09ff24c818e0db126c1b0e59d
institution Directory Open Access Journal
issn 2267-1242
language English
last_indexed 2024-04-12T14:14:37Z
publishDate 2021-01-01
publisher EDP Sciences
record_format Article
series E3S Web of Conferences
spelling doaj.art-ccbfa0a09ff24c818e0db126c1b0e59d2022-12-22T03:29:45ZengEDP SciencesE3S Web of Conferences2267-12422021-01-012340010610.1051/e3sconf/202123400106e3sconf_icies2020_00106Synthesis and characterization of apatite silicated powders with wet precipitation methodLabjar HoudaChaair HassanThe synthesis of apatite silicated Ca10(PO4)6-x(SiO4)x(OH)2-x (SiHA) with 0≤x≤2 was investigated using a wet precipitation method followed by heat treatment using calcium carbonate CaCO3 and phosphoric acid H3PO4 and silicon tetraacetate SiC8H20O4 (TEOS) in medium of water ethanol, with three different silicate concentrations. After drying, the samples are ground and then characterized by different analytical techniques like X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR) and Scanning electron Microscopy (SEM) and chemical analysis.https://www.e3s-conferences.org/articles/e3sconf/pdf/2021/10/e3sconf_icies2020_00106.pdf
spellingShingle Labjar Houda
Chaair Hassan
Synthesis and characterization of apatite silicated powders with wet precipitation method
E3S Web of Conferences
title Synthesis and characterization of apatite silicated powders with wet precipitation method
title_full Synthesis and characterization of apatite silicated powders with wet precipitation method
title_fullStr Synthesis and characterization of apatite silicated powders with wet precipitation method
title_full_unstemmed Synthesis and characterization of apatite silicated powders with wet precipitation method
title_short Synthesis and characterization of apatite silicated powders with wet precipitation method
title_sort synthesis and characterization of apatite silicated powders with wet precipitation method
url https://www.e3s-conferences.org/articles/e3sconf/pdf/2021/10/e3sconf_icies2020_00106.pdf
work_keys_str_mv AT labjarhouda synthesisandcharacterizationofapatitesilicatedpowderswithwetprecipitationmethod
AT chaairhassan synthesisandcharacterizationofapatitesilicatedpowderswithwetprecipitationmethod