Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength

Objectives: To measure and compare the bond strength between three different types of ceramics and resin cement, as well as the degree of conversion of resin cement after using different light-curing units and curing modes. Methods: Three types of ceramics—Leucite-reinforced (Empress CAD), Lithium d...

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Main Authors: Evonne Mei Jing Phua, John Neil Waddell, Joanne Jung Eun Choi
Format: Article
Language:English
Published: MDPI AG 2022-02-01
Series:Oral
Subjects:
Online Access:https://www.mdpi.com/2673-6373/2/1/8
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author Evonne Mei Jing Phua
John Neil Waddell
Joanne Jung Eun Choi
author_facet Evonne Mei Jing Phua
John Neil Waddell
Joanne Jung Eun Choi
author_sort Evonne Mei Jing Phua
collection DOAJ
description Objectives: To measure and compare the bond strength between three different types of ceramics and resin cement, as well as the degree of conversion of resin cement after using different light-curing units and curing modes. Methods: Three types of ceramics—Leucite-reinforced (Empress CAD), Lithium disilicate (Emax CAD), and Zirconia (Emax ZirCAD)—of varying thicknesses (1.5 mm and 2.0 mm) were bonded to a light-cure resin cement (Variolink Esthetic LC). Light-curing was carried out using a monowave LCU (3M Elipar DeepCure-S LED Curing Light with irradiance of 1470 mW/cm<sup>2</sup>) and with polywave LCU (Ivoclar Bluephase PowerCure) using High, Turbo, and 3 s curing modes, respectively (1200, 2100, 3000 mW/cm<sup>2</sup>). A chevron-notch bond strength test (total n = 288) was conducted to calculate the fracture energy and interfacial bond strength (J/m<sup>2</sup>). The degree of cure (%DC) of the residual resin cement on debonded surfaces was measured using Fourier Transform Infrared Spectroscopy (FTIR). Collected data were statistically analysed under SPSS ver. 27 by conducting an ANOVA and Bonferroni post hoc test. The mode of failure was established using a scanning electron microscope (SEM). Results: A significant difference in interfacial bond strength was found between the three types of ceramic material groups (<i>p</i> < 0.01). Cement cured through Empress that was 2 mm thick showed the highest bond strength (1.36 ± 0.46 J/m<sup>2</sup>), while the lowest was observed (0.26 ± 0.07 J/m<sup>2</sup>) in 2 mm Emax CAD using the 3 s mode. The use of different LCUs and curing modes had a significant influence on the %DC of resin cement seen in all groups, except 2 mm Emax ZirCAD. The dominant mode of failure for Empress, EmaxCAD, and EmaxZirCAD were cohesive, adhesive, and mixed, respectively. Conclusions: The type of ceramic and its thickness can significantly affect bond strength, and the results showed that polywave LCU is more effective than monowave LCU when curing through ceramics.
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spelling doaj.art-ccdc89121dd04421a8b41bc62bb679f52023-11-30T21:51:35ZengMDPI AGOral2673-63732022-02-0121627410.3390/oral2010008Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond StrengthEvonne Mei Jing Phua0John Neil Waddell1Joanne Jung Eun Choi2Sir John Walsh Research Institute, Faculty of Dentistry, University of Otago, Dunedin 9016, New ZealandSir John Walsh Research Institute, Faculty of Dentistry, University of Otago, Dunedin 9016, New ZealandSir John Walsh Research Institute, Faculty of Dentistry, University of Otago, Dunedin 9016, New ZealandObjectives: To measure and compare the bond strength between three different types of ceramics and resin cement, as well as the degree of conversion of resin cement after using different light-curing units and curing modes. Methods: Three types of ceramics—Leucite-reinforced (Empress CAD), Lithium disilicate (Emax CAD), and Zirconia (Emax ZirCAD)—of varying thicknesses (1.5 mm and 2.0 mm) were bonded to a light-cure resin cement (Variolink Esthetic LC). Light-curing was carried out using a monowave LCU (3M Elipar DeepCure-S LED Curing Light with irradiance of 1470 mW/cm<sup>2</sup>) and with polywave LCU (Ivoclar Bluephase PowerCure) using High, Turbo, and 3 s curing modes, respectively (1200, 2100, 3000 mW/cm<sup>2</sup>). A chevron-notch bond strength test (total n = 288) was conducted to calculate the fracture energy and interfacial bond strength (J/m<sup>2</sup>). The degree of cure (%DC) of the residual resin cement on debonded surfaces was measured using Fourier Transform Infrared Spectroscopy (FTIR). Collected data were statistically analysed under SPSS ver. 27 by conducting an ANOVA and Bonferroni post hoc test. The mode of failure was established using a scanning electron microscope (SEM). Results: A significant difference in interfacial bond strength was found between the three types of ceramic material groups (<i>p</i> < 0.01). Cement cured through Empress that was 2 mm thick showed the highest bond strength (1.36 ± 0.46 J/m<sup>2</sup>), while the lowest was observed (0.26 ± 0.07 J/m<sup>2</sup>) in 2 mm Emax CAD using the 3 s mode. The use of different LCUs and curing modes had a significant influence on the %DC of resin cement seen in all groups, except 2 mm Emax ZirCAD. The dominant mode of failure for Empress, EmaxCAD, and EmaxZirCAD were cohesive, adhesive, and mixed, respectively. Conclusions: The type of ceramic and its thickness can significantly affect bond strength, and the results showed that polywave LCU is more effective than monowave LCU when curing through ceramics.https://www.mdpi.com/2673-6373/2/1/8photopolymerisationceramicadhesionresin cementsdegree of curebond strength
spellingShingle Evonne Mei Jing Phua
John Neil Waddell
Joanne Jung Eun Choi
Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength
Oral
photopolymerisation
ceramic
adhesion
resin cements
degree of cure
bond strength
title Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength
title_full Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength
title_fullStr Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength
title_full_unstemmed Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength
title_short Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength
title_sort curing through ceramics influence of different light curing units and curing modes on bond strength
topic photopolymerisation
ceramic
adhesion
resin cements
degree of cure
bond strength
url https://www.mdpi.com/2673-6373/2/1/8
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AT johnneilwaddell curingthroughceramicsinfluenceofdifferentlightcuringunitsandcuringmodesonbondstrength
AT joannejungeunchoi curingthroughceramicsinfluenceofdifferentlightcuringunitsandcuringmodesonbondstrength