Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i>
In this work, the production of a novel methodology for the application of natural corrosion inhibitors on steel, using an autoclave is presented. Tests were carried out using <i>Artemisia vulgaris</i>. The inhibitor was produced with a simple soxhlet extraction process using 15 g of <...
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2021-04-01
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Online Access: | https://www.mdpi.com/1996-1944/14/9/2234 |
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author | Daniel Alejandro Pineda Hernández Elisabeth Restrepo Parra Pedro José Arango Arango Belarmino Segura Giraldo Carlos Daniel Acosta Medina |
author_facet | Daniel Alejandro Pineda Hernández Elisabeth Restrepo Parra Pedro José Arango Arango Belarmino Segura Giraldo Carlos Daniel Acosta Medina |
author_sort | Daniel Alejandro Pineda Hernández |
collection | DOAJ |
description | In this work, the production of a novel methodology for the application of natural corrosion inhibitors on steel, using an autoclave is presented. Tests were carried out using <i>Artemisia vulgaris</i>. The inhibitor was produced with a simple soxhlet extraction process using 15 g of <i>Artemisia vulgaris</i> and 260 mL of Ether. Once the inhibitor was produced, the steel was immersed in it, to form a coating that protects the material against corrosion. Thermogravimetry analyzes (TGA) were performed on the inhibitor, to determine the degradation temperature; it was observed that, at 321 °C, the loss of organic mass begins. After applying the inhibitor to the steel, the Fourier Transform Infrared Spectroscopy (FTIR) technique was used to determine the vibrational bands and the difference between the spectra for the steels before and after the coating was applied. For the evaluation of the method efficiency, Electrochemical Impedance Spectroscopy (EIS) and polarization resistance tests were performed, where Nyquist diagrams and Tafel curves were obtained, for steels with and without treatment. In this case, an increase of 93% in the corrosion resistance, and an 88% decrease in the corrosion rate were observed, proving that this methodology can be used to protect steel against corrosion and extend the steel’s useful life. |
first_indexed | 2024-03-10T11:56:22Z |
format | Article |
id | doaj.art-ccf81cd620754f2984e2369ebb32a438 |
institution | Directory Open Access Journal |
issn | 1996-1944 |
language | English |
last_indexed | 2024-03-10T11:56:22Z |
publishDate | 2021-04-01 |
publisher | MDPI AG |
record_format | Article |
series | Materials |
spelling | doaj.art-ccf81cd620754f2984e2369ebb32a4382023-11-21T17:16:52ZengMDPI AGMaterials1996-19442021-04-01149223410.3390/ma14092234Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i>Daniel Alejandro Pineda Hernández0Elisabeth Restrepo Parra1Pedro José Arango Arango2Belarmino Segura Giraldo3Carlos Daniel Acosta Medina4Laboratorio de Física del Plasma, Unicversidad Nacional de Colombia sede Manizales, Manizales-Caldas 170003, ColombiaLaboratorio de Física del Plasma, Unicversidad Nacional de Colombia sede Manizales, Manizales-Caldas 170003, ColombiaLaboratorio de Física del Plasma, Unicversidad Nacional de Colombia sede Manizales, Manizales-Caldas 170003, ColombiaLaboratorio de Física del Plasma, Unicversidad Nacional de Colombia sede Manizales, Manizales-Caldas 170003, ColombiaCalculo Científico y Modelamiento Matemático, Universidad Nacional de Colombia sede Manizales, Manizales-Caldas 170003, ColombiaIn this work, the production of a novel methodology for the application of natural corrosion inhibitors on steel, using an autoclave is presented. Tests were carried out using <i>Artemisia vulgaris</i>. The inhibitor was produced with a simple soxhlet extraction process using 15 g of <i>Artemisia vulgaris</i> and 260 mL of Ether. Once the inhibitor was produced, the steel was immersed in it, to form a coating that protects the material against corrosion. Thermogravimetry analyzes (TGA) were performed on the inhibitor, to determine the degradation temperature; it was observed that, at 321 °C, the loss of organic mass begins. After applying the inhibitor to the steel, the Fourier Transform Infrared Spectroscopy (FTIR) technique was used to determine the vibrational bands and the difference between the spectra for the steels before and after the coating was applied. For the evaluation of the method efficiency, Electrochemical Impedance Spectroscopy (EIS) and polarization resistance tests were performed, where Nyquist diagrams and Tafel curves were obtained, for steels with and without treatment. In this case, an increase of 93% in the corrosion resistance, and an 88% decrease in the corrosion rate were observed, proving that this methodology can be used to protect steel against corrosion and extend the steel’s useful life.https://www.mdpi.com/1996-1944/14/9/2234EISorganic coatingtafelmild steelcorrosion |
spellingShingle | Daniel Alejandro Pineda Hernández Elisabeth Restrepo Parra Pedro José Arango Arango Belarmino Segura Giraldo Carlos Daniel Acosta Medina Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i> Materials EIS organic coating tafel mild steel corrosion |
title | Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i> |
title_full | Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i> |
title_fullStr | Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i> |
title_full_unstemmed | Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i> |
title_short | Innovative Method for Coating of Natural Corrosion Inhibitor Based on <i>Artemisia vulgaris</i> |
title_sort | innovative method for coating of natural corrosion inhibitor based on i artemisia vulgaris i |
topic | EIS organic coating tafel mild steel corrosion |
url | https://www.mdpi.com/1996-1944/14/9/2234 |
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