2-(3-Bromo-4-methoxyphenyl)-3-nitropyridine
The title compound, C12H9BrN2O3, was prepared in two steps from 2-chloro-3-nitropyridine. The nitrobiaryl unit is twisted, with dihedral angles of 35.4 (5)° between the nitro substituent and the pyridine ring to which it is bound, and 51.0 (5)° between the nitro group and the benzene ring. In the cr...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2017-11-01
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| Series: | IUCrData |
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| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314617013943 |
| _version_ | 1818541112617336832 |
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| author | Daniel Limbach Heiner Detert Dieter Schollmeyer |
| author_facet | Daniel Limbach Heiner Detert Dieter Schollmeyer |
| author_sort | Daniel Limbach |
| collection | DOAJ |
| description | The title compound, C12H9BrN2O3, was prepared in two steps from 2-chloro-3-nitropyridine. The nitrobiaryl unit is twisted, with dihedral angles of 35.4 (5)° between the nitro substituent and the pyridine ring to which it is bound, and 51.0 (5)° between the nitro group and the benzene ring. In the crystal, the molecules are connected via C—H...O hydrogen bonds, forming strands along the b-axis direction. |
| first_indexed | 2024-12-11T22:04:18Z |
| format | Article |
| id | doaj.art-cdc3e7b5860e4c6aacf63819115e704c |
| institution | Directory Open Access Journal |
| issn | 2414-3146 |
| language | English |
| last_indexed | 2024-12-11T22:04:18Z |
| publishDate | 2017-11-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | IUCrData |
| spelling | doaj.art-cdc3e7b5860e4c6aacf63819115e704c2022-12-22T00:49:00ZengInternational Union of CrystallographyIUCrData2414-31462017-11-01211x17139410.1107/S2414314617013943sj41322-(3-Bromo-4-methoxyphenyl)-3-nitropyridineDaniel Limbach0Heiner Detert1Dieter Schollmeyer2University of Mainz, Institut for Organic Chemistry, Duesbergweg 10-14, 55099 Mainz, GermanyUniversity of Mainz, Institut for Organic Chemistry, Duesbergweg 10-14, 55099 Mainz, GermanyUniversity of Mainz, Institut for Organic Chemistry, Duesbergweg 10-14, 55099 Mainz, GermanyThe title compound, C12H9BrN2O3, was prepared in two steps from 2-chloro-3-nitropyridine. The nitrobiaryl unit is twisted, with dihedral angles of 35.4 (5)° between the nitro substituent and the pyridine ring to which it is bound, and 51.0 (5)° between the nitro group and the benzene ring. In the crystal, the molecules are connected via C—H...O hydrogen bonds, forming strands along the b-axis direction.http://scripts.iucr.org/cgi-bin/paper?S2414314617013943crystal structurenitroheterocyclebiaryl |
| spellingShingle | Daniel Limbach Heiner Detert Dieter Schollmeyer 2-(3-Bromo-4-methoxyphenyl)-3-nitropyridine IUCrData crystal structure nitro heterocycle biaryl |
| title | 2-(3-Bromo-4-methoxyphenyl)-3-nitropyridine |
| title_full | 2-(3-Bromo-4-methoxyphenyl)-3-nitropyridine |
| title_fullStr | 2-(3-Bromo-4-methoxyphenyl)-3-nitropyridine |
| title_full_unstemmed | 2-(3-Bromo-4-methoxyphenyl)-3-nitropyridine |
| title_short | 2-(3-Bromo-4-methoxyphenyl)-3-nitropyridine |
| title_sort | 2 3 bromo 4 methoxyphenyl 3 nitropyridine |
| topic | crystal structure nitro heterocycle biaryl |
| url | http://scripts.iucr.org/cgi-bin/paper?S2414314617013943 |
| work_keys_str_mv | AT daniellimbach 23bromo4methoxyphenyl3nitropyridine AT heinerdetert 23bromo4methoxyphenyl3nitropyridine AT dieterschollmeyer 23bromo4methoxyphenyl3nitropyridine |