The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni Alloys

This research was conducted to determine the effect of solution variations, electrical current, thickness, weight, metal composition, and the characteristics of the Fe-Ni alloy synthesized using the electrodeposition method. The instruments used in this study were atomic absorption spectroscopy (AAS...

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Main Authors: Ghina Imani Rofi, Maria Paristiowati
Format: Article
Language:English
Published: The Center for Science Innovation 2022-06-01
Series:Chemistry and Materials
Subjects:
Online Access:https://piscience.org/index.php/cma/article/view/27
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author Ghina Imani Rofi
Maria Paristiowati
author_facet Ghina Imani Rofi
Maria Paristiowati
author_sort Ghina Imani Rofi
collection DOAJ
description This research was conducted to determine the effect of solution variations, electrical current, thickness, weight, metal composition, and the characteristics of the Fe-Ni alloy synthesized using the electrodeposition method. The instruments used in this study were atomic absorption spectroscopy (AAS) to determine the metal composition in the deposit, X-ray diffraction to determine the diffraction patterns, and scanning electron microscopy (SEM) to observe morphology and energy dispersive X-ray spectroscopy for elemental analysis. The SEM micrographs obtained showed that morphology of the Fe-Ni alloy was in the form of refined grains. The percentage of Fe in the deposit decreases with the increase in the used current. The AAS data also showed that a high Ni composition in solution will affect the atomic percent of each metal in the deposit. The formation of the alloy was confirmed by diffraction peaks at 2θ of 44°, 53°, and 76° that associated with reflection planes of the face centered cubic structure of Fe-Ni with the crystallite size range from 5 nm to 35 nm.
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spelling doaj.art-cde1450680434a5c8ab6a0ebcc578adc2023-07-19T02:26:46ZengThe Center for Science InnovationChemistry and Materials2828-271X2828-23102022-06-0112556010.56425/cma.v1i2.2727The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni AlloysGhina Imani Rofi0Maria ParistiowatiUniversitas Negeri JakartaThis research was conducted to determine the effect of solution variations, electrical current, thickness, weight, metal composition, and the characteristics of the Fe-Ni alloy synthesized using the electrodeposition method. The instruments used in this study were atomic absorption spectroscopy (AAS) to determine the metal composition in the deposit, X-ray diffraction to determine the diffraction patterns, and scanning electron microscopy (SEM) to observe morphology and energy dispersive X-ray spectroscopy for elemental analysis. The SEM micrographs obtained showed that morphology of the Fe-Ni alloy was in the form of refined grains. The percentage of Fe in the deposit decreases with the increase in the used current. The AAS data also showed that a high Ni composition in solution will affect the atomic percent of each metal in the deposit. The formation of the alloy was confirmed by diffraction peaks at 2θ of 44°, 53°, and 76° that associated with reflection planes of the face centered cubic structure of Fe-Ni with the crystallite size range from 5 nm to 35 nm.https://piscience.org/index.php/cma/article/view/27alloyfe-nielectrodeposition
spellingShingle Ghina Imani Rofi
Maria Paristiowati
The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni Alloys
Chemistry and Materials
alloy
fe-ni
electrodeposition
title The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni Alloys
title_full The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni Alloys
title_fullStr The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni Alloys
title_full_unstemmed The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni Alloys
title_short The Effect of Electrodeposition Current and Electrolyte Composition on Electrodeposition of Fe-Ni Alloys
title_sort effect of electrodeposition current and electrolyte composition on electrodeposition of fe ni alloys
topic alloy
fe-ni
electrodeposition
url https://piscience.org/index.php/cma/article/view/27
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