Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites

To improve the interfacial performance of carbon fiber (CF) and epoxy resin, the surface of CF was modified using magnetron sputtering technology, and a CF epoxy resin (CFER) composite was prepared using injection molding technology. The influence of magnetron sputtering technology on the surface pr...

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Main Authors: Li Yang, Hong Xia, Zhenzhen Xu, Zou Lihua, Qingqing Ni
Format: Article
Language:English
Published: IOP Publishing 2020-01-01
Series:Materials Research Express
Subjects:
Online Access:https://doi.org/10.1088/2053-1591/abbc90
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author Li Yang
Hong Xia
Zhenzhen Xu
Zou Lihua
Qingqing Ni
author_facet Li Yang
Hong Xia
Zhenzhen Xu
Zou Lihua
Qingqing Ni
author_sort Li Yang
collection DOAJ
description To improve the interfacial performance of carbon fiber (CF) and epoxy resin, the surface of CF was modified using magnetron sputtering technology, and a CF epoxy resin (CFER) composite was prepared using injection molding technology. The influence of magnetron sputtering technology on the surface properties of CF was investigated by scanning electron microscopy (SEM), atomic force microscopy (AFM), and dynamic contact angle analysis (DCAA). The influence of the surface modification of the CFs by magnetron sputtering on the mechanical and interfacial properties of CF composites was analyzed by testing the tensile and bending properties of the CFER composites. The results indicated that the surface morphology of CF can be modified by magnetron sputtering, and a nano sized carbon film was deposited on the surface of the CFs. The morphology of the carbon film on the surface of the CFs was different from that on the silicon pellet. The surface roughness of the CF increased after it was modified by magnetron sputtering. The surface wettability of the CFs may be improved by increasing the surface free energy of the fiber owing to the deposition of the carbon film. Tests of the tensile and bending properties of the CFER composites showed that the surface modification of CFs by magnetron sputtering can effectively improve the mechanical properties of the CFER composites, which not only improves the tensile strength and bending strength, but also increases the tensile modulus and bending modulus. The SEM images showed that the interfacial adhesion between the modified CF and the epoxy resin was significantly improved. The stress–strain curves showed that the failure mode of the CFER composite modified by magnetron sputtering CF surface changed, and a stress yield phenomenon was observed.
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spelling doaj.art-cec3ae8b30134cf58355d26512b71a702023-08-09T15:50:36ZengIOP PublishingMaterials Research Express2053-15912020-01-0171010560210.1088/2053-1591/abbc90Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber compositesLi Yang0https://orcid.org/0000-0002-7731-8602Hong Xia1Zhenzhen Xu2Zou Lihua3Qingqing Ni4https://orcid.org/0000-0001-9362-2148Department of Mechanical Engineering & Robotics, Shinshu University , Ueda 386-8567, Japan; College of Textile and Garments, Anhui Polytechnic University , Wuhu, Anhui, 241000, People’s Republic of ChinaDepartment of Mechanical Engineering & Robotics, Shinshu University , Ueda 386-8567, JapanCollege of Textile and Garments, Anhui Polytechnic University , Wuhu, Anhui, 241000, People’s Republic of ChinaCollege of Textile and Garments, Anhui Polytechnic University , Wuhu, Anhui, 241000, People’s Republic of ChinaDepartment of Mechanical Engineering & Robotics, Shinshu University , Ueda 386-8567, JapanTo improve the interfacial performance of carbon fiber (CF) and epoxy resin, the surface of CF was modified using magnetron sputtering technology, and a CF epoxy resin (CFER) composite was prepared using injection molding technology. The influence of magnetron sputtering technology on the surface properties of CF was investigated by scanning electron microscopy (SEM), atomic force microscopy (AFM), and dynamic contact angle analysis (DCAA). The influence of the surface modification of the CFs by magnetron sputtering on the mechanical and interfacial properties of CF composites was analyzed by testing the tensile and bending properties of the CFER composites. The results indicated that the surface morphology of CF can be modified by magnetron sputtering, and a nano sized carbon film was deposited on the surface of the CFs. The morphology of the carbon film on the surface of the CFs was different from that on the silicon pellet. The surface roughness of the CF increased after it was modified by magnetron sputtering. The surface wettability of the CFs may be improved by increasing the surface free energy of the fiber owing to the deposition of the carbon film. Tests of the tensile and bending properties of the CFER composites showed that the surface modification of CFs by magnetron sputtering can effectively improve the mechanical properties of the CFER composites, which not only improves the tensile strength and bending strength, but also increases the tensile modulus and bending modulus. The SEM images showed that the interfacial adhesion between the modified CF and the epoxy resin was significantly improved. The stress–strain curves showed that the failure mode of the CFER composite modified by magnetron sputtering CF surface changed, and a stress yield phenomenon was observed.https://doi.org/10.1088/2053-1591/abbc90magnetron sputteringcarbon fibercompositesinterfacial modification
spellingShingle Li Yang
Hong Xia
Zhenzhen Xu
Zou Lihua
Qingqing Ni
Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites
Materials Research Express
magnetron sputtering
carbon fiber
composites
interfacial modification
title Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites
title_full Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites
title_fullStr Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites
title_full_unstemmed Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites
title_short Influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites
title_sort influence of surface modification of carbon fiber based on magnetron sputtering technology on mechanical properties of carbon fiber composites
topic magnetron sputtering
carbon fiber
composites
interfacial modification
url https://doi.org/10.1088/2053-1591/abbc90
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AT zhenzhenxu influenceofsurfacemodificationofcarbonfiberbasedonmagnetronsputteringtechnologyonmechanicalpropertiesofcarbonfibercomposites
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