Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSM

In this study, the behavior of hydrodynamic parameters was investigated in agitated columns including Asymmetric rotating disc contactor (ARDC), Perforated rotating disc contactor (PRDC), Oldshue–Rushton column (ORC), and Kuhni. The effects of various parameters, including rotor speed (rpm), dispers...

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Main Authors: Shaparak Mirzaei, Fatemeh Ardestani, Ahad Ghaemi, Alireza Hemmati, Mansour Shirvani
Format: Article
Language:English
Published: Elsevier 2023-11-01
Series:Chemical Engineering Journal Advances
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2666821123001126
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author Shaparak Mirzaei
Fatemeh Ardestani
Ahad Ghaemi
Alireza Hemmati
Mansour Shirvani
author_facet Shaparak Mirzaei
Fatemeh Ardestani
Ahad Ghaemi
Alireza Hemmati
Mansour Shirvani
author_sort Shaparak Mirzaei
collection DOAJ
description In this study, the behavior of hydrodynamic parameters was investigated in agitated columns including Asymmetric rotating disc contactor (ARDC), Perforated rotating disc contactor (PRDC), Oldshue–Rushton column (ORC), and Kuhni. The effects of various parameters, including rotor speed (rpm), dispersed and continuous phase velocities, interfacial parameters, and type of RDCs on the dispersed phase holdup and Sauter mean drop diameter were studied. The response surface methodology (RSM) based on the central composite design (CCD) approach was applied for the experimental modeling of three standard systems including toluene-water, butyl acetate-water, and butanol-water. Results showed that the enhancement of rotor speed and dispersed and continuous phase velocities would enhance the dispersed phase holdup. PRDC showed the least enhancement of dispersed phase holdup compared to the other three columns. Our investigation demonstrated that Sauter mean droplet diameter decreased with the rotor speed increase, and this declining trend is more appreciable in ORC and Kuhni columns. Additionally, by increasing dispersed phase velocity in the four columns, the droplet size in the ORC column is larger than the columns. However, by increasing continuous phase velocity, subtle changes in droplet size was observed. Based on the experimental data, new correlations have been presented to predict Sauter mean drop diameter and dispersed phase holdup for agitated columns by analysis of variance (ANOVA). The coefficient of determination (R2) was obtained to be 0.9612 and 0.9495 for Sauter mean drop diameter and dispersed phase holdup, respectively, indicating a good correlation between the predicted and observed values of the models.
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spelling doaj.art-ced40effbc7f4d51818c3f5c8e80bdff2023-12-17T06:42:18ZengElsevierChemical Engineering Journal Advances2666-82112023-11-0116100555Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSMShaparak Mirzaei0Fatemeh Ardestani1Ahad Ghaemi2Alireza Hemmati3Mansour Shirvani4School of Chemical, Petroleum and Gas Engineering, Iran University of Science and Technology, Narmak, Tehran, IranSchool of Chemical, Petroleum and Gas Engineering, Iran University of Science and Technology, Narmak, Tehran, IranCorresponding author.; School of Chemical, Petroleum and Gas Engineering, Iran University of Science and Technology, Narmak, Tehran, IranSchool of Chemical, Petroleum and Gas Engineering, Iran University of Science and Technology, Narmak, Tehran, IranSchool of Chemical, Petroleum and Gas Engineering, Iran University of Science and Technology, Narmak, Tehran, IranIn this study, the behavior of hydrodynamic parameters was investigated in agitated columns including Asymmetric rotating disc contactor (ARDC), Perforated rotating disc contactor (PRDC), Oldshue–Rushton column (ORC), and Kuhni. The effects of various parameters, including rotor speed (rpm), dispersed and continuous phase velocities, interfacial parameters, and type of RDCs on the dispersed phase holdup and Sauter mean drop diameter were studied. The response surface methodology (RSM) based on the central composite design (CCD) approach was applied for the experimental modeling of three standard systems including toluene-water, butyl acetate-water, and butanol-water. Results showed that the enhancement of rotor speed and dispersed and continuous phase velocities would enhance the dispersed phase holdup. PRDC showed the least enhancement of dispersed phase holdup compared to the other three columns. Our investigation demonstrated that Sauter mean droplet diameter decreased with the rotor speed increase, and this declining trend is more appreciable in ORC and Kuhni columns. Additionally, by increasing dispersed phase velocity in the four columns, the droplet size in the ORC column is larger than the columns. However, by increasing continuous phase velocity, subtle changes in droplet size was observed. Based on the experimental data, new correlations have been presented to predict Sauter mean drop diameter and dispersed phase holdup for agitated columns by analysis of variance (ANOVA). The coefficient of determination (R2) was obtained to be 0.9612 and 0.9495 for Sauter mean drop diameter and dispersed phase holdup, respectively, indicating a good correlation between the predicted and observed values of the models.http://www.sciencedirect.com/science/article/pii/S2666821123001126Sauter mean drop diameterDispersed phase holdupAgitated columnsRotating disc contactors (RDCs)Response surface methodology (RSM)
spellingShingle Shaparak Mirzaei
Fatemeh Ardestani
Ahad Ghaemi
Alireza Hemmati
Mansour Shirvani
Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSM
Chemical Engineering Journal Advances
Sauter mean drop diameter
Dispersed phase holdup
Agitated columns
Rotating disc contactors (RDCs)
Response surface methodology (RSM)
title Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSM
title_full Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSM
title_fullStr Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSM
title_full_unstemmed Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSM
title_short Experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors, using RSM
title_sort experimental modeling of mean drop size and dispersed phase holdup in rotating disc contactors using rsm
topic Sauter mean drop diameter
Dispersed phase holdup
Agitated columns
Rotating disc contactors (RDCs)
Response surface methodology (RSM)
url http://www.sciencedirect.com/science/article/pii/S2666821123001126
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