Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic Steel

Abstract Microstructure and mechanical properties of GN9 Ferritic/Martensitic steel for sodium- cooled fast reactors have been investigated through orthogonal design and analysis. Scanning electron microscopy (SEM), transmission electron microscopy (TEM), differential scanning calorimeter (DSC), ten...

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Main Authors: Tingwei Ma, Xianchao Hao, Ping Wang
Format: Article
Language:English
Published: SpringerOpen 2023-12-01
Series:Chinese Journal of Mechanical Engineering
Subjects:
Online Access:https://doi.org/10.1186/s10033-023-00984-5
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author Tingwei Ma
Xianchao Hao
Ping Wang
author_facet Tingwei Ma
Xianchao Hao
Ping Wang
author_sort Tingwei Ma
collection DOAJ
description Abstract Microstructure and mechanical properties of GN9 Ferritic/Martensitic steel for sodium- cooled fast reactors have been investigated through orthogonal design and analysis. Scanning electron microscopy (SEM), transmission electron microscopy (TEM), differential scanning calorimeter (DSC), tensile and impact tests were used to evaluate the heat treatment parameters on yield strength, elongation and ductile-to-brittle transition temperature (DBTT). The results indicate that the microstructures of GN9 steel after orthogonal heat treatments consist of tempered martensite, M23C6, MX carbides and MX carbonitrides. The average prior austenite grains increase and the lath width decreases with the austenitizing temperature increasing from 1000 °C to 1080 °C. Tempering temperature is the most important factor that influences the dislocation evolution, yield strength and elongation compared with austenitizing temperature and cooling methods. Austenitizing temperature, tempering temperature and cooling methods show interactive effects on DBTT. Carbide morphology and distribution, which is influenced by austenitizing and tempering temperatures, is the critical microstructural factor that influences the Charpy impact energy and DBTT. Based on the orthogonal design and microstructural analysis, the optimal heat treatment of GN9 steel is austenitizing at 1000 °C for 0.5 h followed by air cooling and tempering at 760 °C for 1.5 h.
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spelling doaj.art-ceda6c54bd744c00977e1edc57b885532023-12-24T12:11:27ZengSpringerOpenChinese Journal of Mechanical Engineering2192-82582023-12-0136111210.1186/s10033-023-00984-5Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic SteelTingwei Ma0Xianchao Hao1Ping Wang2Key Laboratory of Electromagnetic Processing of Materials, Ministry of Education, Northeastern UniversityCAS Key Laboratory of Nuclear Materials and Safety Assessment, Institute of Metal Research, Chinese Academy of SciencesKey Laboratory of Electromagnetic Processing of Materials, Ministry of Education, Northeastern UniversityAbstract Microstructure and mechanical properties of GN9 Ferritic/Martensitic steel for sodium- cooled fast reactors have been investigated through orthogonal design and analysis. Scanning electron microscopy (SEM), transmission electron microscopy (TEM), differential scanning calorimeter (DSC), tensile and impact tests were used to evaluate the heat treatment parameters on yield strength, elongation and ductile-to-brittle transition temperature (DBTT). The results indicate that the microstructures of GN9 steel after orthogonal heat treatments consist of tempered martensite, M23C6, MX carbides and MX carbonitrides. The average prior austenite grains increase and the lath width decreases with the austenitizing temperature increasing from 1000 °C to 1080 °C. Tempering temperature is the most important factor that influences the dislocation evolution, yield strength and elongation compared with austenitizing temperature and cooling methods. Austenitizing temperature, tempering temperature and cooling methods show interactive effects on DBTT. Carbide morphology and distribution, which is influenced by austenitizing and tempering temperatures, is the critical microstructural factor that influences the Charpy impact energy and DBTT. Based on the orthogonal design and microstructural analysis, the optimal heat treatment of GN9 steel is austenitizing at 1000 °C for 0.5 h followed by air cooling and tempering at 760 °C for 1.5 h.https://doi.org/10.1186/s10033-023-00984-5Ferritic/Martensitic steelOrthogonal designM23C6 carbideDuctile-to-brittle transition temperature
spellingShingle Tingwei Ma
Xianchao Hao
Ping Wang
Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic Steel
Chinese Journal of Mechanical Engineering
Ferritic/Martensitic steel
Orthogonal design
M23C6 carbide
Ductile-to-brittle transition temperature
title Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic Steel
title_full Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic Steel
title_fullStr Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic Steel
title_full_unstemmed Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic Steel
title_short Effects of Orthogonal Heat Treatment on Microstructure and Mechanical Properties of GN9 Ferritic/Martensitic Steel
title_sort effects of orthogonal heat treatment on microstructure and mechanical properties of gn9 ferritic martensitic steel
topic Ferritic/Martensitic steel
Orthogonal design
M23C6 carbide
Ductile-to-brittle transition temperature
url https://doi.org/10.1186/s10033-023-00984-5
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AT pingwang effectsoforthogonalheattreatmentonmicrostructureandmechanicalpropertiesofgn9ferriticmartensiticsteel