4,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one
The synthesis of previously unknown 4,5-dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one has been proposed and structurally characterized via a single-crystal X-ray diffraction analysis, <sup>1</sup>H, <sup>13</sup>C–{<sup>1</sup>H}, &l...
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| Language: | English |
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MDPI AG
2024-02-01
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| Online Access: | https://www.mdpi.com/1422-8599/2024/1/M1776 |
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| author | Kirill A. Gomonov Vasilii V. Pelipko Igor A. Litvinov Ruslan I. Baichurin Sergey V. Makarenko |
| author_facet | Kirill A. Gomonov Vasilii V. Pelipko Igor A. Litvinov Ruslan I. Baichurin Sergey V. Makarenko |
| author_sort | Kirill A. Gomonov |
| collection | DOAJ |
| description | The synthesis of previously unknown 4,5-dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one has been proposed and structurally characterized via a single-crystal X-ray diffraction analysis, <sup>1</sup>H, <sup>13</sup>C–{<sup>1</sup>H}, <sup>1</sup>H–<sup>13</sup>C HMQC, and <sup>1</sup>H–<sup>13</sup>C HMBC NMR spectroscopy, and IR spectroscopy. |
| first_indexed | 2024-04-24T17:59:48Z |
| format | Article |
| id | doaj.art-cf2412243754430ea1917f0d5c23b840 |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-04-24T17:59:48Z |
| publishDate | 2024-02-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-cf2412243754430ea1917f0d5c23b8402024-03-27T13:56:37ZengMDPI AGMolbank1422-85992024-02-0120241M177610.3390/M17764,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-oneKirill A. Gomonov0Vasilii V. Pelipko1Igor A. Litvinov2Ruslan I. Baichurin3Sergey V. Makarenko4Laboratory of Nitrocompounds, Department of Organic Chemistry, Faculty of Chemistry, Herzen State Pedagogical University of Russia, 48 Moika Embankment, 191186 St. Petersburg, RussiaLaboratory of Nitrocompounds, Department of Organic Chemistry, Faculty of Chemistry, Herzen State Pedagogical University of Russia, 48 Moika Embankment, 191186 St. Petersburg, RussiaA. E. Arbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of the Russian Academy of Sciences, 420088 Kazan, RussiaLaboratory of Nitrocompounds, Department of Organic Chemistry, Faculty of Chemistry, Herzen State Pedagogical University of Russia, 48 Moika Embankment, 191186 St. Petersburg, RussiaLaboratory of Nitrocompounds, Department of Organic Chemistry, Faculty of Chemistry, Herzen State Pedagogical University of Russia, 48 Moika Embankment, 191186 St. Petersburg, RussiaThe synthesis of previously unknown 4,5-dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one has been proposed and structurally characterized via a single-crystal X-ray diffraction analysis, <sup>1</sup>H, <sup>13</sup>C–{<sup>1</sup>H}, <sup>1</sup>H–<sup>13</sup>C HMQC, and <sup>1</sup>H–<sup>13</sup>C HMBC NMR spectroscopy, and IR spectroscopy.https://www.mdpi.com/1422-8599/2024/1/M1776furo[3,4-<i>d</i>]pyridazinfuranspyridazinonescyclocondensationcrystal structureX-ray diffraction analysis |
| spellingShingle | Kirill A. Gomonov Vasilii V. Pelipko Igor A. Litvinov Ruslan I. Baichurin Sergey V. Makarenko 4,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one Molbank furo[3,4-<i>d</i>]pyridazin furans pyridazinones cyclocondensation crystal structure X-ray diffraction analysis |
| title | 4,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one |
| title_full | 4,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one |
| title_fullStr | 4,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one |
| title_full_unstemmed | 4,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one |
| title_short | 4,5-Dimethylfuro[3,4-<i>d</i>]pyridazin-1(2<i>H</i>)-one |
| title_sort | 4 5 dimethylfuro 3 4 i d i pyridazin 1 2 i h i one |
| topic | furo[3,4-<i>d</i>]pyridazin furans pyridazinones cyclocondensation crystal structure X-ray diffraction analysis |
| url | https://www.mdpi.com/1422-8599/2024/1/M1776 |
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