3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid
In the title compound, C24H25N3O5, the ethoxy group is disordered over two orientations in a 0.853 (14):0.147 (14) ratio. The benzimadazole ring system (r.m.s. deviation = 0.016 Å) makes a dihedral angle of 35.47 (7)° with the attached benzen...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2013-02-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536813001116 |
| _version_ | 1818083359618760704 |
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| author | Yeong Keng Yoon Mohamed Ashraf Ali Soo Choon Tan Mohd Mustaqim Rosli Ibrahim Abdul Razak |
| author_facet | Yeong Keng Yoon Mohamed Ashraf Ali Soo Choon Tan Mohd Mustaqim Rosli Ibrahim Abdul Razak |
| author_sort | Yeong Keng Yoon |
| collection | DOAJ |
| description | In the title compound, C24H25N3O5, the ethoxy group is disordered over two orientations in a 0.853 (14):0.147 (14) ratio. The benzimadazole ring system (r.m.s. deviation = 0.016 Å) makes a dihedral angle of 35.47 (7)° with the attached benzene ring. The pyrrolidine ring adopts an envelope conformation with a methylene C atom as the flap. In the crystal, inversion dimers linked by pairs of O—H...N hydrogen bonds generate R22(16) loops. C—H...O interactions link the dimers into a three-dimensional network. |
| first_indexed | 2024-12-10T19:36:45Z |
| format | Article |
| id | doaj.art-cfaaa8fafe2f48039f09c3699cd6b544 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-10T19:36:45Z |
| publishDate | 2013-02-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-cfaaa8fafe2f48039f09c3699cd6b5442022-12-22T01:36:07ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682013-02-01692o304o30410.1107/S16005368130011163-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acidYeong Keng YoonMohamed Ashraf AliSoo Choon TanMohd Mustaqim RosliIbrahim Abdul RazakIn the title compound, C24H25N3O5, the ethoxy group is disordered over two orientations in a 0.853 (14):0.147 (14) ratio. The benzimadazole ring system (r.m.s. deviation = 0.016 Å) makes a dihedral angle of 35.47 (7)° with the attached benzene ring. The pyrrolidine ring adopts an envelope conformation with a methylene C atom as the flap. In the crystal, inversion dimers linked by pairs of O—H...N hydrogen bonds generate R22(16) loops. C—H...O interactions link the dimers into a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S1600536813001116 |
| spellingShingle | Yeong Keng Yoon Mohamed Ashraf Ali Soo Choon Tan Mohd Mustaqim Rosli Ibrahim Abdul Razak 3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid Acta Crystallographica Section E |
| title | 3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_full | 3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_fullStr | 3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_full_unstemmed | 3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_short | 3-{5-Ethoxycarbonyl-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazol-2-yl}benzoic acid |
| title_sort | 3 5 ethoxycarbonyl 1 3 2 oxopyrrolidin 1 yl propyl 1h benzimidazol 2 yl benzoic acid |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536813001116 |
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